CP4001: ANALYTICAL & PHYSICAL CHEMISTRY | | Formal Report of the Quantitative Determination of Sulphate by Gravimetric Analysis (Experiment 4) | Maryjo Lee Wei Min 1111107 DBS/FT/1A/01 | (A) Synopsis The amount of sulphate is determined quantitatively as barium sulphate by gravimetric analysis. This determination consists of slowly adding a dilute solution of barium chloride to a hot‚ unknown sulphate solution which is slightly acidified with concentrated hydrochloric acid. A white precipitate
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Mass of crucible Mass with cuSO4 Mass after heating Difference in mass 29.50 34.50 32.66 1.84 30.40 35.40 33.56 1.84 26.37 31.37 29.54 1.83 29.50 34.50 32.66 1.84 Moles of water = mass/mr = 1.84/18 =0.102 CuSo4 moles = mass/mr = (5 - 1.84)
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Chemistry Internal Assessment 2011 Candy Au Introduction The reaction between zinc and copper (II) sulphate is endothermic. If an excess of zinc powder is added to a measured amount of aqueous copper (II) sulphate in a calorimeter and the temperature change is recorded over a period of time‚ the enthalpy change of the reaction can be experimentally determined. Assumption 1. Mass of H2O in 100cm3 of CuSO4 solution is 100g 2. Specific heat of solution is 4.18 kJ kg-1 K-1 which is the
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Determination of the Enthalpy for Decomposition of Hydrogen Peroxide Objective: To construct a coffee cup calorimeter‚ measure its calorimeter constant‚ and determine the enthalpy of decomposition and formation of hydrogen peroxide. Background: This experiment is a classic thermodynamics lab. In it‚ we attempt to measure the enthalpy (H) of a chemical reaction. The main obstacle is that this is a quantity that cannot be measured directly. It instead is observed as heat from one substance is transferred
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Thermochemistry: An Ice Calorimeter Determination of Reaction Enthalpy D. F. Nachman 6/23/2010 Abstract: An ice calorimeter was used to study the reaction of magnesium metal and 1.00M sulfuric acid solution: Mg(s) + H2SO4(aq) →MgSO4(aq) + H2(g). We found the experimental molar enthalpy of reaction to be ΔH = –355 ± 17 kJ/mol at 0°C‚ 24% lower than the textbook value of ΔH° = –466.9 kJ/mol‚ reported at 25°C. Introduction Whether a chemical reaction occurs spontaneously or is driven by an outside
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F6/7 Chemistry Practical: Enthalpy of hydration of copper(II) sulphate Objective: To determine the enthalpy of hydration of copper(II) sulphate Group size: Individual Introduction This experiment enables an approximate determination of the enthalpy of hydration of copper(II) sulphate to be made. The enthalpy change when one mole of anhydrous copper(II) sulphate is dissolved in water is first determined. Secondly‚ the enthalpy of solution of copper(II) sulphate pentahydrate in water is determined
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DETERMINATION OF COPPER BY COMPLEXATION‚ SOLVENT-EXTRACTION AND SPECTROPHOTOMETRY ABSTRACT To determine the concentration of copper in an unknown solution by using copper complexation‚ solvent extraction and spectrophotometry. Standards are used to create a calibration curve and the unknown concentration of copper is then calculated by using the linear equation from the calibration curve. The concentration of copper in the unknown solution 201 was found to be 12.57± 0.25 μg/mL. INTRODUCTION Copper
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Determining the Percent Copper and Zinc in Pennies from Density Lab Report Procedure: For pre-1982 pennies- Mass 10 pennies‚ record data. Fill a 100mL graduated cylinder to 40mL or enough to fully submerge the pennies with water‚ record the volume in data table. Carefully place the pennies into the graduated cylinder‚ record the final volume of the water in data table. To find the volume of the pennies‚ subtract the final volume from the initial‚ record the data. Repeat this procedure twice more
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Gravimetric determination of sulphate in fertiliser Question: The proportion of sulphate present in a brand of commercial fertiliser under a range of temperatures. Fertilisers provide plants with a number of sources necessary for them to grow‚ as follows‚ nitrogen‚ phosphorus‚ potassium and finally the one I will be concentrating on Sulfur. To cater for the varying plants‚ you wouldn’t require all these elements to the same extent as the necessities for each plant differ. The composition of different
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Thermochemistry: An Ice Calorimeter Determination of Reaction Enthalpy Shannon Wedepohl 9/17/13 Abstract: During this experiment‚ an ice calorimeter was used to measure the change in volume in milliliters of magnesium metal and 1.00 M of sulfuric acid. We found the experimental molar enthalpy of the reaction to be ∆H = -370 ± 1 kJ/mol at 0˚C. This compares with an expected value of -466.9 kJ/mol at 25 ˚C‚ a 20.75% difference. Introduction: Many chemical reactions truly only
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