Acetylsalicylic Acid (Aspirin) Synthesis Telow‚ AJV Sumicad‚ CJ‚ Tavanlar‚ EMMT‚ Chem 40.1‚ Institute of Chemistry‚ University of the Philippines Los Baños I. Introduction Organic synthesis is the process where a desired organic compound is constructed or prepared from commercially available materials. The objective of organic synthesis is to design the simplest synthetic routes to a molecule. Aspirin‚ also known as acetylsalicylic acid is as salicylate drug often used as analgesic
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The synthesized product‚ SnI4 was found to have a yield of 0.0227 g which corresponded to a 4.63 % yield. The synthesizing process of SnI4 showed distinctive changes. After the addition of dichloromethane the solution turned to a purple color‚ this then turned into a purple-burgundy colour after gravity filtration; the desired colour was observed only when vacuum filtration was applied. The purple solution turned into damp orange crystals and after thorough drying the crystals were a bright‚ dry
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a solution. This lab should prove that Beer’s law and the equation A=a x b x c‚ is a linear relationship. Procedure: The only deviations in the lab procedure was that the stock solution was made before arrival to the lab with 0.570 g of KMnO4 in 0.500 L. The diluted solutions and the Spec 20 were used as directed in the lab manual. The same cuvette was used each time to eliminate error. Cuvettes are all made differently and have a difference in how they measure. If a new cuvette was used
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Procedures for Part A: For Activity A‚ we first tested enzyme activity. First‚ we used an H2O2 syringe to transfer 10 mL of H2O2 into an unlabeled 60-mL cup. Then‚ we used a transfer pipet to add one mL of catalase solution into the unlabeled 60-mL cup that we put H2O2 in. After that‚ we observed the solution for one minute. Then we tested the effect of boiling on enzyme activity. First we used a transfer pipet to transfer 4 mL of catalase into a test tube. After that‚ we placed the test tube filled
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Comparison of Three Isomers of Butanol SCH 4UI Abstract The Hydroxyl group on alcohols relates to their reactivity. This concept was explored by answering the question “Does each alcohol undergo halogenation and controlled oxidation?” . Using three isomers of butanol; the primary 1-butanol‚ the secondary 2-butanol and the tertiary 2-methyl-2-propanol‚ also referred to as T-butanol‚ two experiments were performed to test the capabilities of the alcohols. When mixed with hydrochloric acid in
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IntroductionA dehydration reaction of an alcohol results in an alkene. This type of reaction requires an alcohol‚ an acid catalyst and heat. Generally strong concentrated acids‚ like sulfuric acid and phosphoric acid‚ are used as the acid catalyst.The acid catalyst protonates the alcohol‚ to make a much better leaving group. Weakest bases make the best leaving groups‚ so once the alcohol is protonated the leaving group leaves and produces in a carbocation and water. In order to form the double bond
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http://foricseandbeyond.blogspot.in/ DE’S FOUNDATION BISTUPUR‚ JSR ACTION OF HEAT ON CHEMICAL COMPOUNDS “Analytical chemistry -I” http://foricseandbeyond.blogspot.in/ metal oxide “Oxides of metals are generally stable to heat and they are considered to be most stable form of compound found in nature.” Oxides of potassium‚sodium‚calcium‚magnesium‚ aluminum ‚ zinc‚iron‚lead and copper are stable to heat uO C PbO Zn O http://foricseandbeyond.blogspot.in/ MERCURIC OXIDE
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Determination of Cobalt Oxalate Hydtrate Introduction The objective of this lab is for students to determine the percentage of cobalt oxalate hydrate using the gravimetric analysis. They will also do a redox titration to determine the percentage of oxalate in the compound. After the percentages are calculated‚ you will determine the percent water by the difference of Oxalate and Cobalt from %100. Procedure Determination of Cobalt 1. Weigh 0.3 g of solid cobalt oxalate hydrate (from lab 8)
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Ashley Esparza Stallings Period 2 January 26‚ 2013 Enzyme Catalysis Lab Report Background: Enzymes are catalyst‚ which affect the rate of a chemical reaction. One consequence includes the cell to carry out complex chemical activities at relatively low temperatures. In these reactions the substrate binds reversibly to the active site. The cause of this is a decrease in the energy needed to activate the reaction of the substrate molecule to from products. Every enzyme is particular for a
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Abstract: After reviewing the basics of enzymes and catalysis‚ we take a dive into the wonderful world of catalase. Beginning with establishing a base line of just how much hydrogen peroxide there is in 5.0mL of the reacted solution; to figuring out exactly how much actually reacted after 300 seconds of catalyzed reaction. Follow the experiment from the beginning steps right to the end as you see where the students went wrong‚ interpretation of the results‚ and great answers to work sheet
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