A simple‚ rapid‚ specific and highly sensitive spectrofluorimetric method has been developed for the quantification of dabigatran etexilate mesylate (DAB) in bulk and capsule dosage form. A linear relationship was found between fluorescence intensity and DAB concentration in the range of 0.01-1.0 μg/ml in DMSO as solvent at an emission wavelength of 391 nm after excitation at 334 nm‚ with a good correlation coefficient (0.989). The detection and quantification limits were found to be 0.005 and 0
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In the reaction mechanism‚ a carboxylic acid‚ m-toluic acid is used to synthesize N‚N-diethyl-m-toluamide‚ also know as DEET‚ through a nucleophilic acyl substitution reaction. The reaction begins by first converting the m-toluic carboxylic acid into an acyl chlorosulfite through a reaction using thionyl chloride. The carboxylic acid is converted into an acyl chloride because the acyl chloride is more reactive. In this step‚ hydrochloric acid is formed from a hydrogen on the carboxylic acid and a
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FOUNDATION CHEMISTRY II CHM096 CHAPTER 1 ORGANIC CHEMISTRY PART I PREPARED BY SYED ABDUL ILLAH ALYAHYA BIN SYED ABD KADIR 1 TOPICS PART I 1.1 1.2 1.3 1.4 1.5 Introduction to Hydrocarbon and Functional Groups Alkanes and Cycloalkanes Isomerism and Overview of Organic Reaction Alkenes and Alkynes Alkyl Halides 2 TOPIC INTRODUCTION TO HYDROCARBON AND FUNCTIONAL GROUPS 3 1.1 Introduction to Hydrocarbon and Functional Groups What is Organic Chemistry?
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CHAPTER 10 Liquids and Solids 1. Order the intermolecular forces (dipole-dipole‚ London dispersion‚ ionic‚ and hydrogen-bonding) from weakest to strongest . a) dipole-dipole‚ London dispersion‚ ionic‚ and hydrogen-bonding b) London dispersion‚ dipole-dipole‚ hydrogen-bonding‚ and ionic c) hydrogen-bonding‚ dipole-dipole‚ London dispersion‚ and ionic d) dipole-dipole‚ ionic‚ London dispersion‚ and hydrogen-bonding e) London dispersion‚ ionic‚ dipole-dipole‚ and hydrogen-bonding Ans: b 2. Hydrogen
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Chapter 18 Ethers & Epoxides; Thiols and Sulfides Assigned Reading from McMurry: Read Sections 18.1 through 18.9; not responsible for “Focus on … Epoxy Resins & Adhesives‚ pp. 697-698). Recommended Problems from McMurry: 18.1a-e;18.18.2;18.3a-d; 18.4; 18.5a-d; 18.6a-b; 18.7a-b; 18.8; 18.9; 18.10; 18.11; 18.12a‚b; 18.13a‚b; 18.14a-c; 18.16a-f; 18.17; 18.18; 18.19a-c; 18.20; 18.21; 18.22; 18.23a-e; 18.24a-I; 18.25a-f; 18.26a-d; 18.27; 18.28; 18.29ad; 18.30a-e; 18.31; 18.32; 18.33; 18.34; 18
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immediate amperometric response toward the addition of 0.2 mΜ OA‚ whereas no remarkable effect was observed for the 50-fold excess concentration of possible interferrants such as ethylene glycol (E.G) (CH2OH-CH2OH)‚ glyoxylic acid (GA) (CHO-COOH)‚ dimethyl oxalate (DO) (CH3OOC-COOCH3) and glycolic acid (CH2OH-COOH) (Fig. 8A). However‚ a considerable response was observed after further addition of 0.2 mM OA into the solution containing of interferences. These results show that this sensor has high selectivity
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|Thesis Summary | | | | | |
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Celecoxib (CLX) is a nonsteroidal anti-inflammatory drug (NSAID) used as a positive control for the antiangiogenesis assay Dimethyl sulfoxide (DMSO) an organosulfur compound with the formula (CH₃)₂SO which is capable of dissolving polar and nonpolar compounds. DPPH is also known as 2‚2-diphenyl-1-picrylhydrazyl. It is a stable free radical commonly used to evaluate the ability
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1. This name describes the chemical structure of the drug and is generally not used due to its long and complicated name. Answer A a. Chemical Name b. Generic Name c. Official Name d. Trade Name 2. This name is established by the USAN (United States Adopted Names Council). Answer B a. Chemical Name b. Generic Name c. Official Name d. Trade Name 3. This name is “owned” by a drug company. Answer D a. Chemical Name b. Generic Name c. Official
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Effects of curing condition of solution cast Nafion® membranes on PEMFC performance Korean J. Chem. Eng.26(3)‚ 679-684 (2009) Thickness of membrane ~ 50µm There are some disadvantages of the solution casting method that the cold cast films are generally mechanically weak‚ susceptible to crack formation and soluble in many polar solvents‚ especially in water at room temperature. Generally‚ the annealed films undergo morphological changes when heated above the glass transition temperature (Tg=109oC
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