CHM 3120L ANALYTICAL CHEMISTRY I LABORATORY REPORT EXPERIMENT: DETERMINATION OF ASCORBIC ACID BY REDOX TITRATION Name: Section: Date Experiment Completed: 2.0008 g KIO3 x (1 mol/214 g KIO3) = 0.0093495327 mol KIO3 0.0093495327 mol KIO3 / 0.500 L = 0.0186990654 M KIO3 6 Na2S2O3 + KIO3 + 6 H+ → I-+ 3 H2O + 3 S4O62- + K+ + 12 Na+ 0.0187 M KIO3 × 0.025 L = 4.675 x 10-4 mol KIO3 4.675 x 10-4 mol KIO3 x (6 mol Na2S2O3 / 1 mol KIO3) = 0.002805 mol Na2S2O3 0.002805 mol Na2S2O3
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Discussion The acid neutralising capacity (ANC) of 3 brands of calcium carbonate (CaCO3) tablets was determined by reacting the tablets in excess standardized hydrochloric acid (HCl) and then back-titrating with a standardized sodium hydroxide (NaOH) solution. Back titration was required for two reasons. Firstly‚ CaCO3 tablets are poorly water-soluble but dissolve rapidly in acid. Secondly‚ CaCO3 is a weak base so it is difficult to determine the end point of the reaction if titrated directly. Assuming
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techniques are created. In chemical analysis‚ the amount of an object is determined using a process called titration. According to Petrucci et al.‚ titration is a reaction carried out by the carefully controlled addition of one solution to another. It has several types like acid-base titrations and redox titrations. This experiment focuses on the latter type‚ the redox titration. A redox titration is based on an oxidation-reduction reaction between analyte and titrant (Harris‚2009). It involves the
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Nathalie Dagmang Co-workers: Annjaneth Briones and groups 5‚ 6‚ 7 and 9 Group 8 Date Performed: February 3‚ 2011 Results and Discussion Report 9: Redox Titration: Winkler Method for Dissolved Oxygen Determination The three main objectives of the experiment are to (1) determine dissolved oxygen (DO) in water using the classical method (redox titration)‚ (2) discuss the chemistry behind the Winkler method for DO analysis and (3) describe the sampling technique for the analysis of DO in water sample
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OXIDATION-REDUCTION TITRATIONS REDOX TITRATION • involves oxidizing agents and reducing agents titrants and analytes • oxidizing agents used as standard solutions: potassium permanganate‚ KMnO4 potassium dichromate‚ K2Cr2O7 iodine‚ I2 ceric sulfate‚ Ce(SO4) 2 potassium iodate‚ KIO3 REDOX TITRATION • reducing agents used as standard solutions: ferrous sulfate‚ FeSO4 oxalic acid‚ H2C2O4 sodium oxalate‚ Na2C2O4 sodium thiosulfate‚ Na2S2O3 titanous chloride
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Redox Problem Set 1: Reactions and Stoichiometry (All of these questions are no calculator friendly) 1) Give the oxidation number of carbon in each of the following: a) b) c) d) CF2Cl2 Na2C2O4 HCO3-1 C2H6 2) Give the oxidation number of sulphur in each of the following: a) b) c) d) SOCl2 H2S2 H2SO3 Na2S 3) Identify the oxidizing and reducing agents in each of the following: a) b) c) d) 8H+(aq) + 6Cl-1(aq) + Sn(s) + 4NO3-1(aq) SnCl6 -2(aq) + 4NO2(g) + 4H2O(l) 2MnO4-1(aq) + 10Cl-1(aq) + 16H+(aq)
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------------------------------------------------- Titration From Wikipedia‚ the free encyclopedia (Redirected from Back titration) Not to be confused with the mathematical notion of tetration. This article is about volumetric titration. For other uses‚ see Titration (disambiguation). A Winkler titration to determine the concentration of dissolved oxygen in a water sample Titration‚ also known as titrimetry‚[1] is a common laboratory method of quantitative chemical analysis that is used
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Titration KMnO4+ FeSO4 12/2/2013 At Alsadek Scientific Association Prepared by: Zainab Alfakih & Jinan Krayem Teacher: Dr. Hiba Nassar Contents Introduction 2 Objectives 3 Theoretical Study 3 Definitions 3 Derivations 3 Equipment 4 Setup 5 Procedures 5 Results 6 Discussion 7 Conclusion 8 References 9 I. Introduction: Oxidation Reduction reactions are chemical reactions in which substances undergo changes in oxidation state. Oxidation is defined as the
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Redox Titration Analysis of a Commercial Bleach A. Purpose ! ! ! To review oxidation-reduction reactions and their stoichiometry. To learn the concept and technique of redox titration. To determine the percent (m/v) of an active ingredient‚ sodium hypochlorite (NaOCl)‚ in a commercial bleaching agent. B. Theoretical Background Whereas acid-base reactions involve the transfer of a proton‚ oxidation-reduction or redox reactions involve the transfer of electrons from one substance to
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Experiment 1 : Redox Titration Using Sodium Thiosulphate Abstract This experiment is to determine the concentration of oxidizing solution using the iodine/ thiosulphate titration where the reducing solution is potassium iodate solution and the oxidizing solution is sodium thiosulphate solution. Potassium iodate solution which is an oxidizing agent is added into an excess solution of acidified potassium iodide. This reaction will release iodine. Potassium iodide is acidified with sulphuric acid
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