Distillation Purpose: To conduct the distillation process‚ simple or fractional. Procedure: 1. Add 5ml of 20% ethanol: water mix to the distillation flask. 2. Add 23 stir bar 3. Make sure that the thermometer bulb is just below the Claisen Head‚ carefully. Be very gentle with the thermometers and take care not to break them. 4. Label 3 vials‚ 1‚2‚ and 3. 5. Place receiving vial 1 on ice to collect the distillate 6. Start the distillation by piling up hot sand around the distillation flask with
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Comparing between the simple and fractional distillation‚ the fractional distillations for both n-propanol and acetone provided a better distillation. The data and graphs support the statement since the fractional graphs provided a steeper slope than the simple distillation. The steeper slope represent how fast the mixture are separated throughout the distillations. For example‚ the simple distillation for acetone the slope initially started at about 20 mL at about 65.5℃ and ended at about 30 mL
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Chemistry Lab: Experiment 1 Section 2 – 12:30 to 2:20 Distillation and Fractional Distillation Distillation and Fraction Distillations Purpose: The purpose of distillation is to purify a liquid. Distillations are use to purify contaminates out of water to obtain clean pure water‚ as well as‚ to separate mixtures of liquids into their individual components; e.g. methanol and water. Objective: Distill methanol from water using a simple distillation apparatus and fractional distillation apparatus
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Experiment 1: Simple Distillation and Boiling Points- Separation of Liquids February 24‚ 2014 Analysis In this experiment‚ the distillation of three groups of two miscible liquids was performed. First‚ Ethanol and 2-Propanol were distilled. The boiling points of ethanol and 2-propanol had a difference of 5°C. The percent recovery for both ethanol and 2-propanol were both 0%. The percent recovery of the intermediate was 96%. The percent efficiency calculated of ethanol and 2-propanol was 0% efficient
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Fractional distillation was used in this experiment. This is one of two ways for distillation‚ the other being simple distillation. However‚ with a simple distillation‚ the difference of boiling points between the substances must be more than 40 to 50 degrees C. A fractional distillation column is needed in a fractional distillation. The column in a fractional distillation column provides a temperature gradient where the temperature is lower at the top of the column and the temperature is greater
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SIMPLE DISTILLATION OF VODKA (ANTONOV) Kristel Joy M. Tan‚ Joshua Michael L. Torres‚ Pauleen Anne S. Vanadero‚ Paulene Arielle P. Ynzon and Rachel Pauline E. Zaballero Group 10‚ 2D Medical Technology‚ Faculty of Pharmacy‚ University of Santo Tomas ABSTRACT Distillation is the most common technique‚ it is a process wherein the liquid is separated from the solution by boiling the liquid solution and condensing the vapor in order to get the distillate. There are four kind of distillation: simple distillation
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Both the graph and the table represent the same thing‚ the temperature of the solution during fractional distillation. At the start of the fractional distillation‚ before we started the fire‚ it was 25° celcius. At the end of the fractional distillation‚ when all of the liquid was gone‚ it was 99.3 degrees. This set of data is not the first time we did the fractional distillation‚ it’s actually probably the 3rd or 4th. The first time we didn’t actually record the temperature‚ we just looked for the
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Arranged a fractional distillation apparatus used a 100mL round-bottomed flask for the solution and used a 50mL round- bottomed flask cooled in ice an ice bath as the receiver of the reaction. The 65% sulfuric solution was prepared in a clean 125mL Erlenmeyer flask it contained 20.0 mL of deionized water and 20mL of concentrated sulfuric acid was added carefully with some swirling in between. The diluted acid was cooled with an ice water bath to 20-25ºC. to the cooled sulfuric acid cyclohexanol was
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In experiment 5‚ distillation method was used to divide hexane and toluene from a mixture (50:50) of hexane and toluene. Hexane was separated from toluene and was observed from the gas chromatography‚ it showed that hexane increased from 0.0.873 to 0.886 moles. Once the mixture of toluene and hexane hit 70 degrees in the experiment‚ the distillate was used for the gas chromatography. Hexane was higher in the distillate stage. The first drop of condensation appeared at 79°C. The volume of the distillate
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Distillation Objective: To illustrate the use of distillation for separating a mixture of two volatile liquids with different boiling points. Background: Distillation consists of heating a liquid until it vaporizes‚ and then condensing the vapor and collecting it in a separate container. Distillation is used to separate mixtures of liquids that either have different boiling points‚ or that have one component that does not distill. There are many types of distillation‚ each of which has a distinct
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