Arranged a fractional distillation apparatus used a 100mL round-bottomed flask for the solution and used a 50mL round- bottomed flask cooled in ice an ice bath as the receiver of the reaction. The 65% sulfuric solution was prepared in a clean 125mL Erlenmeyer flask it contained 20.0 mL of deionized water and 20mL of concentrated sulfuric acid was added carefully with some swirling in between. The diluted acid was cooled with an ice water bath to 20-25ºC. to the cooled sulfuric acid cyclohexanol was
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8.2.1 (iv) Fractional Distillation of Crude Oil By Blake Turner – Year 11 Fractional Distillation of Crude Oil Introduction Crude oil is the term for "unprocessed" oil‚ the stuff that comes out of the ground. It is also known as petroleum. Crude oil is a fossil fuel‚ meaning that it was made naturally from decaying plants and animals living in ancient seas millions of years ago -- most places you can find crude oil were once sea beds. Crude oils vary in colour‚ from clear to tar-black‚
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this separation in crude oil is known as fractional distillation. Fractional distillation is carried out by heating the petroleum to 400 °C. As every hydrocarbon in petroleum has it a particular boiling point‚ by doing so‚ they will separate out and then be collected. The portion that remains thick at 400 °C falls to the bottom of the tower is removed and forms bitumen or asphalt. The mixture of vapours that enters the fractional distillation tower starts to condense as the temperature cools the
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phosphoric acid‚ and one boiling chip‚ were all added to a 10 mL round bottom flask that would be attached to the end of an assembled simple distillation set up. A sand bath was placed atop a hot plate‚ and the simple distillation mechanism was lowered into the sand bath with the bottom most piece (the 10 mL round bottom flask) submerged about half way. The distillation process was completed after a sufficient amount of liquid distillate had accumulated within the Hickman Still Head. Smaller volumes were
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students to familiarize and perfect the simple distillation method to produce 4-Methylcyclohexene and to gain experience using an IR spectroscopy to characterize the product of the reaction in favor of equilibrium. B. Results and Discussion: C. Experimental: 24 mL of 4-methylcyclohexanol‚ 5mL of phosphoric acid‚ and 1mL of concentrated sulfuric acid was added to a 250 mL round bottom flask and mixed thoroughly with a magnetic stirrer. A simple distillation set up was installed with a 250mL round
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In experiment 5‚ distillation method was used to divide hexane and toluene from a mixture (50:50) of hexane and toluene. Hexane was separated from toluene and was observed from the gas chromatography‚ it showed that hexane increased from 0.0.873 to 0.886 moles. Once the mixture of toluene and hexane hit 70 degrees in the experiment‚ the distillate was used for the gas chromatography. Hexane was higher in the distillate stage. The first drop of condensation appeared at 79°C. The volume of the distillate
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four days‚ before moving half of the rats to a new location and injecting them with a larger amount of ethanol. The rats that stayed in the same location remained relatively healthy‚ while nearly two-thirds of the rats in the new location died of alcohol poisoning. A similar experiment involving rats and morphine showed that the body can overcompensate for the expected effects of a drug when presented with a smaller dose. Rats were given relatively large doses of morphine for several days‚ and when
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Alcohol and Fetal Alcohol Syndrome Alcohol plays a major role in society today. It is constantly being . ...... in our minds through advertisements‚ whether its commercials or billboards‚ holidays‚ or even just at the popular social scene. Alcohol is consumed for many purposes‚ such as celebrations‚ to increase romance‚ out of boredom‚ or a way to relax. Alcohol is a drug that is depended upon by the majority of our society. Nonetheless‚ alcohol has very damaging effects‚ not only
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Theory: Distillation is the conversion of a mixture of substance into vapors which is afterwards condensed to the liquid form. It cans separation or purification of substances by taking advantage of differences in volatility. The purpose of this lab is comparing the efficiency of two distillation methods with the mixture of ethanol and 1-butanol. in theory the fractional distillation should be more efficient because of the steel sponge. The sponge acted as surface area for gas to condense on. This
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Organic Chemistry I Simple and Fractional Distillation The Simple and Fractional distillation experiment was divided into two parts. We split up the procedure in this experiment. My group did the simple distillation and we received the Fractional distillation from another group in class. In this experiment‚ we examined the effectiveness of fractional and simple distillation to determine which is more successful at extracting a pure sample. This experiment was very successful. We are able to
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