Organic Chemistry II Laboratory (ABCT357/ABCT3757) Lab Manual 2014-2015 Lee Hang Wai‚ Alston (alston.lee@polyu.edu.hk) Dr. Lee Cheng Hao‚ Samuel (chenghao.lee@polyu.edu.hk) Organic Chemistry II Laboratory (ABCT357‚ ABCT3757) (Group one) Contact: Alston Lee (alston.lee@polyu.edu.hk) Tuesday 8:30-11:30 ‚ Laboratory: Y1315 Lab supporting staffs: YK Au / Kan Chan/Arnold Demonstrators: Dr. Samuel Lee‚ Alston Lee‚ Fu Wai Chung‚ Guo Shuai‚ Yuen On Ying‚ Sep 16 Tue Acetylation of α-D-glucopyranose (Expt
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Ellen Grant Honors Bio I Organic Compounds Problems and Objectives: The purpose of this lab was to select the suitable test for an organic molecule and define the safe process for that test. An organic molecule is normally found in or produced by living systems. (Unknown Author‚ 2014‚ www.biology-online.org/organic_molecule)In this lab one was supposed to infer the results of the test and be able to identify if major biomolecules are present. You were to analyze a variety of tests including
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Panther ID: NAME: FLORIDA INTERNATIONAL UNIVERSITY Department of Chemistry CHM 2211-U02– ORGANIC CHEMISTRY II PRACTICE EXAM I CHM 2211-U01 SAMPLE EXAM I‚ Page 2 Type of Vibration C-H Frequency (cm-1) 3000-2850 1450 and 1375 1465 3100-3000 1700-1000 3150-3050 1000-700 ca. 3300 2900-2800 2800-2700 1680-1600 1600-1400 2250-2100 1740-1720 1725-1705 1725-1700 1750-1730 1700-1640 1810 and 1760 1300-1000 Intensity s m m m s s s m w w m-w m-w m-w s s s s s s s Alkanes -CH3 -CH2Alkenes
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Discussion The purpose of the Density Lab was to determine the identity of four unknown solids and two unknown liquids by calculating their densities and comparing them to a density chart‚ taking into account error analysis and finally classifying the substances. In order to calculate this density‚ we first found the mass of the container that was to be holding the substances. We then found the volume of the substance‚ and lastly determined the mass of the container and substance. We subtracted
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phosphoric acid‚ and one boiling chip‚ were all added to a 10 mL round bottom flask that would be attached to the end of an assembled simple distillation set up. A sand bath was placed atop a hot plate‚ and the simple distillation mechanism was lowered into the sand bath with the bottom most piece (the 10 mL round bottom flask) submerged about half way. The distillation process was completed after a sufficient amount of liquid distillate had accumulated within the Hickman Still Head. Smaller volumes were
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One major observation made throughout this experiment was during the steam distillation. As the steam distillation started and the solution in the flask began heating‚ it was clear that too much stopcock grease was used around the glassware. The grease from the connecting ends of the three way connecting tube was melting and seeping into the clove and water solution in the two necked round bottom flask. The solution in the flask was immediately discarded and repeated with clean glassware and a very
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Chemistry 3373F Lab Manual 2008 Modified 11/07 Table of Contents Chem 3373 Laboratory Schedule for Fall 2008.............................................................................2 The Benzoin Condensation of Benzaldehyde ..............................................................................3 Synthesis of Dilantin and Related Compounds (two weeks).........................................................6 Synthesis of an Alkaloid: Pseudopelletierine (two weeks) .............
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Name Lab Section GTA Station # 5. Extraction Pre-lab questions Complete the following questions and submit before beginning the experiment. 1. Which layer will be the aqueous layer when using dichloromethane (methylene chloride) as the solvent (i.e.‚ top or bottom)? Which layer will be the aqueous layer when using ether as the solvent? 2. When everything has been separated in Part D‚ which compounds will be in test tubes 1‚ 2‚ and 3?
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Department of Chemistry Extraction and Sublimation Experiment #4 10/02/13 Introduction Caffeine is a stimulant found in tea‚ coffee‚ cocoa‚ OTC medication‚ and cola drinks.It stimulates the brain and the central nervous system‚ so that a person feels less tired and more alert. The purpose of this lab is to determine the amount of caffeine in tea. The major component of tea is cellulose which is a polymer of glucose. Materials Lab coat Goggles Graduated cylinder 1 tea
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ions Reagent/ Condition; Reaction | Explanation | Oxygen supply; Combustion | Limited supply of oxygen: CO formed.Even less Oxygen: C is deposited as soot. Excess Oxygen: Complete combustion (giving CO2 and H2O) | Al2 O3 and vaporisation of alkane at 500°C; Cracking of Alkanes | Al2 O3 is used as a catalyst. Heat provides energy for breakage of C-C bonds. | UV light; Initiation step of FRS of alkanes by halogens * Not required for electrophilic addition reaction btw Halogens and alkenes
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