Reuven Ilyayev Lab Instructor: Maciej Domaradzki Labs 3 & 4 09/19/11 Objective: In steam distillation lab (lab 3)‚ we must obtain pure Eugenol from cloves through the process of steam distillation. In the crystallization lab (lab 4) part 1‚ we must acquire the best possible pure crystallization of acetylsalicylic acid from aspirin and in part 2 we must obtain a similar pure crystallization of benzil from an impure mixture of benzil. Materials: In lab 3‚ we used 75 g of cloves from
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SUMMARY The aim is to observe distillation process of ethanol-water solution and to measure the alcohol content after process in this experiment. 500 ml of solution with an alcohol content of 32% (v/v) is used for this experiment. Temperature values are recorded for every 10 ml alcohol obtained in the flask. The process is repeated in our experiment and for the first process‚ the data collection process continues until the distillate reaches to 200 ml. The concentration of alcohol is measured for
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Standardization of Solution and Titration Lab Report‚ Preparing a Dilute HCl Solution from a Concentrated One Titrating NAOH Solution with HCl Solution (of Known Concentration) Chemistry lab report(by abdazino abdalla) International College Objective preparing a dilute HCl solution from a concentrated one titrating NAOH solution with HCl solution (of known concentration) Procedure Section A: Preparation of 100.0cm3 0.480 mol/dm3 HCl solution a)Determine the volume of the concentrated acid
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The lab was to include a purpose‚ procedure‚ data/observations‚ all reactions and side reactions written out with qualitative data beneath each product and reactant except H20‚ and a summary. The purpose of this experiment is to observe the qualitative aspects of a series of reactions involving copper. Procedure 1.Measure about 1g of solid copper. 2.Place Cu in Erlenmeyer flask and place flask under fume hood. 3.Add dropwise 15M HNO3 until solid copper is completely reacted. 4.Place flask
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ANALYTICAL AND ORGANIC CHEMISTRY LECTURER’S NAME : DR.RAPIDAH OTHMAN COD SUBJECT : NKB 10103 NAME : NUR NADIRAH BINTI BAHARUDEAN ID NUMBER : 55220114255 CHAPTER : ORGANIC CHEMISTRY CONTENTS 1‚4-BENZENEDICARBOXYLIC ACID Introduction The organic compound’s group that I’ve chosen in this assignment is 1‚4-benzenedicarboxylic acid. 1‚4-benzenedicarboxylic acid and also called as Terephthalic acid containing the carboxyl group and benzene group. Sometimes it simply referred to as a acid group
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Steam distillation of cloves produced 0.53g of an oil which contained in its IR spectrum the functional groups O-H (at 3520 cm-1)‚ sp2 C-H (3080 – 3000 cm-1)‚ aliphatic C-H (2980 – 2940 cm-1)‚ and both alkene C=C (at 1640 cm-1) and aromatic C=C (at 1514 cm-1). The IR spectrum is attached to this report. These data are consistent with the structure of eugenol‚ shown in Figure 2 below: In addition‚ the IR of the product from the steam distillation of cloves closely corresponds with that of an
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Steam Distillation – Clove Oil Abstract: In this experiment‚ a situ method steam distillation was performed and essential oils were isolated from cloves. Once the oils were obtained‚ extraction techniques were used to extract a crude‚ eugenol‚ and acetyleugenol product sample. These samples were submitted for GC analysis and the normalization area percents were calculated to confirm their purity; for the crude sample it was 93.95% eugenol and 6.05% acetyleugenol‚ for the eugenol sample it
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Identifying Organic Compounds Problem: Based on the color of the indicator‚ which type of organic compound will be found in each type of food? Hypothesis: If Benedict solution is added to honey‚ then it will turn. If Biuret solution is added to egg whites‚ then it will turn. If Benedict solution is added to corn oil‚ then it will turn. If Benedict solution is added to glucose‚ then it will turn. If Benedict solution is added to gelatin‚ then it will turn. If Benedict solution is added to butter
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Mona Vaidya 02/04/2014 CHE 317 Laboratory Experiment #1: Simple Distillation of Two Volatile Liquids Containing Non-Volatile Impurities Introduction: Simple distillation is a commonly used method to separate and purify the mixtures of organic liquids into their original components. Mixtures of two miscible liquids with two different boiling points were separated. Therefore‚ it can be said that the two organic compounds are separated by exploiting the different boiling temperatures of the liquids
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Determination of Melting and Boiling Point of different Organic Compounds Bakare‚ Abimbola Kristine‚ C. Professor Miranda Marilyn‚ school of chemical engineering and biotechnology‚ Mapua Institute of Technology‚ CHM145L-B11 ABSTRACT A melting point of a solid is the temperature at which the first crystal just starts to melt until the temperature at which the last crystal just disappears. Thus‚ the melting point (m.p.) is actually a melting range. The melting point of a substance depends
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