The progress of the reaction was monitored in my case using two TLC plate. It first started off with the spotting of Standard benzoin and benzil which were provided in the lab and followed by the addition of the reaction mixture at once it starts changing colour/boiling‚ then at 10 and 20 mins into the reflux. Once all the necessary steps were spotted‚ the TLC plate was placed in in a beaker containing CH₂Cl₂(methylene chloride)‚ which was used as the developing solvent in this experiment. To check
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details Results and Discussion: Voltaic Cell Reactions | | | Overall Cell Reaction | Observed Voltage | Theoretical Voltage | Cu2+(aq)+Zn(s) Cu(s)+Zn2+(aq) | 0.947 V | 1.10 V | Cu2+(aq)+Sn(s)Cu(s)+Sn2+(aq) | 0.571 V | 0.473 V | Cu2+(aq)+Fe(s) Cu(s)+Fe2+(aq) | 0.512 V | 0.777 V | Cu2+(aq)+Mg(s) Cu(s)+Mg2+(aq) | 1.598 V | 2.707 V | Cu2+(aq)+Pb(s) Cu(s)+Pb2+(aq) | 0.651 V | 0.463 V | Concentration Cell | Based on Cu2+ - Cu | Cell Reaction | | [Cu2+] anode | [Cu2+] cathode | Observed
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ADULT ELECTROLYTE REPLACEMENT PROTOCOLS Standing electrolyte replacement protocols are available for use in adult patients admitted to King Khaled Hospital. Najran‚ Saudi Arabia. The protocols are listed below. SPECIFIC REQUIREMENTS: • Intravenous infusions of electrolytes must be administered with free-flow protected infusion devices (i.e. infusion pump). • Patients must meet the following criteria prior to initiation of the Potassium‚ Magnesium‚ or Phosphorus protocols: o SCr < 2 mg/dL
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Substitution Reactions of 3-phenyl-1-phenol‚ 2-pentanol‚ and 2‚4-dimethyl-3-pentanol Samantha Sparks‚ Isi Nosegbe and Sabrina Becker. Department of Chemistry‚ IUPUI‚ 402 N. Blackford St.‚ Indianapolis‚ IN 46202 This project was collaborated on by three different organic chemistry students‚ who individually synthesized and researched each of the three substitution reactions in this experiment.. The first reaction was an Sn2 reaction of 3-phenyl-1-propanol with NaBr and H2SO4 to create1-bromo-3-phenylpropane
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a chemical reaction will occur spontaneously or non-spontaneously is an important aspect of thermodynamics. Spontaneity is determined from free energy‚ or Gibbs free energy. The equation (1) gives the relationship of how entropy (∆S) and enthalpy (∆H) along with temperature affects the amount of free energy‚ and henceforth the spontaneity. A spontaneous process may be quick or slow‚ and it is only affected by temperature and energy‚ therefore it is not related to kinetics or reaction rate. equation
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Edward Dickson CHE101 DS-01 Experiment Date 7/21/2013 Report Submitted 7/21/2013 Title: Experiment #8: Ionic Reactions Purpose: In this lab we will work with aqueous solutions of ionic substances and determine if they are soluble. If the solution appears milky than it is known as a precipitate reaction‚ meaning it is soluble‚ and that the ions separated and became surrounded by water. Precipitates in this experiment are electrically uncharged. To identify which compounds are
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Kinetics of a Reaction I. List of reagents & products 1. 1.0 M Copper(II) nitrate (Cu(NO3)2‚ 0.10 M Hydrochloric Acid (HCl)‚ 0.010 M Potassium Iodide (KI)‚ 0.040 M Potassium Bromate (KBrO3)‚ 0.0010 M Sodium Thiosulfate (N2S2O3)‚ 2% Starch solution‚ Water (H2O) II. Summary of Procedure. Part 1: Find the Volume of One Drop of Solution 2. Fill pipet with 3ml of distilled water 3. Mass a beaker and record 4. Put 5 drops of water into beaker and record
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The Grignard Reaction Abstract Through the use of the Grignard reaction‚ a carbon-carbon bond was formed‚ thereby resulting in the formation of triphenylmethanol from phenyl magnesium bromide and benzophenone. A recrystallization was performed to purify the Grignard product by dissolving the product in methanol. From here‚ a melting point range of 147.0 °C to 150.8 °C was obtained. The purified product yielded an IR spectrum with major peaks of 3471.82 cm-1‚ 3060.90 cm-1‚ 1597.38 cm-1‚ and 1489
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214 MEMORY MANAGEMENT CHAP. 4 4.4 PAGE REPLACEMENT ALGORITHMS When a page fault occurs‚ the operating system has to choose a page to remove from memory to make room for the page that has to be brought in. If the page to be removed has been modified while in memory‚ it must be rewritten to the disk to bring the disk copy up to date. If‚ however‚ the page has not been changed (e.g.‚ it contains program text)‚ the disk copy is already up to date‚ so no rewrite is needed. The page to be
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Diels-Alder Reaction Heather Jost Lab Partner: Jasmina Salcinovic CHEM2642L Luise Strange de Soria Georgia Perimeter College September 29‚ 2004 Diels-Alder Reaction Resources: Mayo‚ Pike‚ Trumper‚ Strange de Soria. Microscale Organic Laboratory. New York: John Wiley and Sons‚ 2002. Strange de Soria‚ Luise. “Student Survival Guide”. http://www.gpc.edu/~lstrange/2642lab/survivalguide/grignard2.pdf. 2004. Purpose: The purpose of these experiments
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