EXPERIMENT 1: REACTIONS OF ENOLATE IONS WITH CARBONYL GROUPS Aims In this experiment we used two techniques for the reactions of enolate ions with carbonyl groups. One technique used was Doebner reaction and the other technique used was Claisen-Schmidt reaction. Therefore the aim of this experiment is to synthesize trans p-methoxycinnamic acid and to synthesize dibenzalacetone via an aldol condensation reaction between acetone and benzaldehyde. The products would be recrystallized using ethanol
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Determination of Reaction Enthalpy Shannon Wedepohl 9/17/13 Abstract: During this experiment‚ an ice calorimeter was used to measure the change in volume in milliliters of magnesium metal and 1.00 M of sulfuric acid. We found the experimental molar enthalpy of the reaction to be ∆H = -370 ± 1 kJ/mol at 0˚C. This compares with an expected value of -466.9 kJ/mol at 25 ˚C‚ a 20.75% difference. Introduction: Many chemical reactions truly only encompass changes by exchanging heat energy
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conduct the experiment. 25 ml of The Bar Vodka was used and 7 ml of distillate was collected before a temperature of 95 degrees Celsius was reached. Collected distillate was then subjected to a flammability test to confirm ethanol content. The percent ethanol was computed to be 24%. Introduction Distillation is a method of separation for homogenous mixtures‚ which are composed of both volatile and nonvolatile substances [1]. It involves the volatile substance to undergo a phase change from a liquid
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its temperature remains constant until it is completely frozen. However‚ in order to melt a substance must go through a energy change‚ creating the problem‚ “What energy changes occur when a liquid solidifies?”. To solve the problem‚ a hypothesis was proposed‚ stating “When a substance begins to solidify‚ it releases heat energy‚ because a substance
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The Experiment Gloria Isham Central Texas College Twenty- six men are chosen to participate in the roles of guards and prisoners in a psychological study led by a Doctor Archaleta for which each participant is to receive $14‚000 after two weeks. Travis has just lost his part time job and is a peace protester who wants to travel to India with his girlfriend. Barris is a 42-year-old who lives alone with a domineering mother‚ who has made him join the experiment to raise money for her hip operation
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Internal Assessment: Enthalpy Change Design Lab Experiment: Reaction of distilled water and solid sodium hydroxide RESEARCH QUESTION How does the heat released during the reaction between distilled water and Group 1 elements (lithium‚ sodium and potassium) vary as one goes down the group? OBJECTIVE The objective of the experiment is to measure the heat change during the reactions with minimal heat loss to the surroundings. MATERIALS The materials to be used in this experiment are: • Lithium‚
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Experiment 2: IDENTIFICATION OF UNKNOWNS BY TLC AND MP IN COMBINATION Introduction: Thin layer chromatography (TLC) is one of the most valuable techniques in organic chemistry. This is a best method of separating and identifying mixtures of two or more compounds. The separation is accomplished by the distribution of the mixture between two phases: one that is stationary and one that is moving or mobile. Chromatography works on the principle that different compounds will have different
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Experiments in physics lab report Department of Electrical Engineering Isabela State University Ilagan Campus‚ Calamagui 2nd‚ City of Ilagan‚ Isabela baccaljoemel@yahoo.com Submitted to: Engr. Rafael S. Ramos Physics12 Professor Submitted by: Joemel L. Baccal BSEE IIA Experiments in Physics Lab Report Joemel L. Baccal Department of Electrical Engineering Isabela State University - Ilagan Campus‚ Calamagui 2nd‚ City of Ilagan‚ Isabela baccaljoemel@yahoo.com Abstract In
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EXPERIMENT 5 REDOX TITRATION: TITRATION USING SODIUM THIOSULPHATE Objectives 1. 2. To prepare a standard solution of potassium iodate for use to determine the concentration of sodium thiosulphate solution accurately. To acquire the proper techniques of carrying out a titration. Introduction Redox titrations using sodium thiosulphate as a reducing agent is known as iodometric titration since it is used specifically to titrate iodine. The reaction involved is: I2 + 2Na2S2O3 I2 + 2S2O322NaI + Na2S4O6
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gerati Laboratory report Vapour-Compression Refrigeration Experiment Thermodynamics Date of experiment: 26 June 2012 Group D2: Introduction The laboratory session for refrigeration system was performed in order to investigate the main concepts of the vapour-compression refrigeration cycle. Simple refrigeration system studied in the laboratory is a prototype for a variety of engineering applications utilized in industrial‚ domestic and scientific purposes. The detailed goals include the study
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