(+)- and (-) – Carvones Purpose Compare (+)- carvone from caraway oil to (-)- carvone from spearmint oil‚ using gas chromatography. Experimental Odor: Smell containers of spearmint and caraway oil and two carvones. Analytical Gas Chromatography: Put five individual samples by different group members into Gas Chromatograph to calculate the percent composition. Claudia tested S- (+)- carvone and R- (+) – Limonene‚ Daniel tested Spearmint oil (pure)‚ Greg tested R- (-)- carvone and I tested Caraway
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Jacobsen’s Method of Epoxidation of an Alkene | | Abstract Various types of reactions were completed to first create and then use Jacobsen’s catalyst in the asymmetric epoxidation of an unknown alkene with bleach in the laboratory. The chiral epoxide synthesized was then characterized with GC/MS and NMR. With this information the unknown alkene was able to be identified as 4-chlorostyrene. Introduction Organisms have evolved with mechanisms that use specific enantiomers of molecules
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Asymmetric Epoxidation of Dihydronaphthalene with a Synthesized Jacobsen’s Catalyst Justin Lindsey 12/08/96 Chem 250 GG Professor Tim Hoyt TA: Andrea Egans Abstract. 1‚2 diaminocyclohexane was reacted with L-(+)-tartaric acid to yield (R‚R)-1‚2-diaminocyclohexane mono-(+)-tartrate salt. The tartrate salt was then reacted with potassium carbonate and 3‚5-di-tert-butylsalicylaldehyde to yield (R‚R)-N‚N’-Bis(3‚5-di-tert-butylsalicylidene)-1‚2-cyclohexanediamine‚ which was then reacted with Mn(OAc)2*4H2O
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Activity of Carvones Kyle Peterson Chem. 243a Matt Judd‚ Sec. 25 Date Performed: 10/29/03 Abstract: The objective of this experiment is to use Gas Chromatography to distinguish between two enantiomers of carvone from caraway oil and spearment oil and to find the 2 carvone’s optical activity as well as percent carvone in spearment and caraway oil. It was found that S-carvone had an optical activity of 0.0047 and R-carvone had an optical activity of 0.516 and that spearment oil is 59% carvone and caraway
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Lab #2 (Part A‚B) Due date: Oct 5‚ 2010 1 - Theory and mechanism Epoxidation is a reaction of an alkene with a peroxycarboxylic acid (also called peracid) to produce an epoxide product‚ generally performed in inert solvents‚ such as dichloromethane. The epoxide product is a cyclic ether in which the ring contains three atoms. The alkene gains an oxygen from the peracid in a syn fashion. In this experiment‚ R-(－)-carvone is reacting with MCPBA‚ a peracid‚ to produce the epoxide product. Balanced
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Epoxidation Reactions Lab Report 2 Abstract An oxygen atom is transferred from a peroxy acid to the carbon=carbon double bond thus forming an epoxide. Scheme 1. Oxone Epoxidation. Scheme 2. mCPBA Epoxidation. The percent yield for the Oxone epoxidation reaction was 65% yield and the mCPBA epoxidation reaction was 70% yield. Oxone is the greener alternative because using mCPBA is twice as expensive as Oxone and leaves behind the epoxide plus m-chlorobenzoic acid while Oxone creates non-toxic
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Clays are one of the important natural materials‚ which have been examined for catalytic applications. Clays are characterized by a layered structure and hence they are slippery when wet. They are broadly classified as cationic or smectite type (having layer lattice structure in which two-dimensional oxyanions are separated by layers of hydrated cations) and anionic or brucite type (in which the charge on the layer and the gallery ion is reversed complimentary to smectite type). Anionic clays are
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P. Stonebraker Organic Chemistry II lecture UCB Extension Spring 2013 Extra Credit Report Papers Paper is strictly optional. Write a 4-6 page paper on a subject approved by the instructor (either picked from the list below or picked by yourself). Emphasis in the paper should be on the organic chemistry associated with the subject (how it is synthesized‚ uses‚ etc.). No two students can research the same subject. Maximum value of the paper will likely in the 20-40 point range‚ depending
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Hamdiya Mumade Partner: Isabella CHEM 253 TA: Pinky Chowdhury Oct 15‚ 2024 Lab 9: Stereochemistry and Polarimetry Purpose: To determine the concentration of three different vitamins by making a series of serial dilutions and using HPLC. Theory: Here?s a theory section for your lab report on stereochemistry and polarimetry. Theory Stereochemistry involves the study of how the spatial arrangement of atoms in a molecule influences its chemical and physical properties. Molecules with the same molecular
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