Preparation of methyl m-nitrobenzoate by nitration using methyl benzoate‚ nitric acid‚ and sulfuric acid Aileen Quintana TA: Sijie Tues/Thurs 11:50 42067 Introduction: The purpose of this lab was to explore the concepts of electrophilic aromatic substitution‚ specifically nitration by synthesizing methyl m-nitrobenzoate using methyl benzoate‚ nitric acid and sulfuric acid. This nitration is a type of electrophilic aromatic substitution. A
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April 04‚ 2014 Fisher Esterification Introduction: Esters are one of the most common derivatives of carboxylic acids and are widely distributed in both nature and industry. A Fischer Esterification is the formation of an ester and water from alcohol and an acid. It is the simplest means of synthesizing an ester and requires the reaction of a carboxylic acid and an alcohol. The general reaction of Fischer esterification is‚ CH3CO2H + ROH ↔ CH3CO2R + H2O (reaction1) CH3COOH + ROH ↔
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Energies 2008‚ 1‚ 79-92; DOI: 10.3390/en1020079 energies ISSN 1424-8220 www.mdpi.org/energies Article Esterification of Oleic Acid for Biodiesel Production Catalyzed by SnCl2: A Kinetic Investigation Abiney L. Cardoso‚ Soraia Cristina Gonzaga Neves and Marcio J. da Silva * Departament of Chemistry‚ Federal University of Viçosa‚ Viçosa‚ Minas Gerais‚ Brazil‚ 36570-000. * Author to whom correspondence should be addressed; E-Mail:silvamj2003@ufv.br Received: 5 August 2008; in revised form:
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To prepare isopentyl acetate from isopentyl alcohol and acetic acid by the Fischer esterification reaction. Materials: West condenser‚ 250 mL round bottomed flask‚ two 250 mL flasks‚ heating mantle‚ boiling chips‚ graduated cylinder‚ sodium bicarbonate‚ isopentyl alcohol‚ glacial acetic acid‚ concentrated sulfuric acid‚ separatory funnel Procedure: 1. Place 50 mL of isopentyl alcohol in a 250 mL round bottom flask and add 60 mL of glacial acetic acid. Add the acid very slowly. 2. Swirl the
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Fischer Esterification is when an carboxylic acid and an alcohol reacts to produce an ester‚ catalyzed by a strong acid to protonate the -OH of the carboxylic acid‚ so it leave as water (Ketcha‚ 58). For Fischer Esterification to occur‚ the reaction must be heated up‚ without boiling away‚ for a prolong amount of time by refluxing the mixture (Ketcha‚ 57). Refluxing is the process in which the boiled solution’s vapors are condense back to a liquid and return to the boiled solution (Ketcha‚ 60). The
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Barry Allahyar Dr. Dodd CHEM 2122 2010-09-16 Experiment 19: Fischer Esterification‚ Conclusion The objective in this experiment was to efficiently perform an Fischer esterification of 1-butanol and acetic acid to form water and n-butyl acetate‚ and to confirm the esterification using IR spectroscopy analysis. It was found that 0.734 grams of n-butyl acetate was formed with a percent yield of 61%. The product was confirmed using IR spectroscopy and boiling point confirmation. The reaction mechanism
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Process Intensification – B51GD Esterification and Polymerisation in PET production Process Overview Polyethylene terephthalate is a polymer with broad applications worldwide‚ and one of the most produced polymers manufactured globally each year. It main application is the bottling industry where approximately 14.7 Mt in 2009. PET resin is produced conventionally in a two - step process displayed in figure 1.9. The first stage is the esterification of Terephthalic acid (PTA) with Ethylene glycol (EG)
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Esterification Lab Introduction Esterification is an important part of organic chemistry that has many practical applications. Esterification can be used to make polymers. In most cases‚ esters are used for scents – they often smell fruity and sweet. In general‚ an esterification reaction results from a condensation reaction between a carboxylic acid and an alcohol. The carboxylic acid group loses an OH group‚ and the alcohol loses and H. For instance‚ the reaction between methanoic acid and methanol
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family‚ a group of compounds that possess antibacterial and antifungal properties. These agents are esters of para-hydroxybenzoic acid‚ which is why they are collectively called parabens. However‚ in contrast to its cousins‚ ethylparaben‚ butylparaben‚ and propylparaben‚ methylparaben receives its specific name owing to the fact that its chemical structure contains the methyl alkyl group. Methylparaben is found in several fruits‚ in particular blueberries‚ where it acts as an antimicrobial agent. Methylparaben
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Title: Esterification Objective: To synthesis acetylsalicylic acid by esterification. Introduction: A pleasant‚ often fruity‚ odor is characteristic of some of the simpler esters. Ethyl butyrate smells similar to pineapples‚ the odor of n-propyl acetate is reminiscent of pears and isopentyl acetate has a strong banana fragrance. Esters are derivatives of the carboxylic acids and contain the following functional group: The synthesis of an ester can be accomplished in one of several ways. An esterification
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