"Esterification of methyl benzoate from benzoic acid" Essays and Research Papers

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    Also known as "benzoate of soda‚" sodium benzoate is an FDA-approved‚ polyunsaturated fat that has been used by food manufacturers for over 80 years to inhibit microbial growth. As a food additive it is used as a preservative‚ effectively killing most yeasts‚ bacteria and fungi. Sodium benzoate is effective only in acidic conditions (pH < 3.6) making its use most prevalent in foods such as preserves‚ salad dressings (vinegar)‚ carbonated drinks (carbonic acid)‚ jams (citric acid)‚ fruit juices (citric

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    Methyl Orange

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    In this experiment the initial mass of the sodium carbonate used was 2.69g. In each titration‚ 3 drops of methyl orange was added to the sodium carbonate solution. With this information the titration can begin‚ and the results obtained are shown below: Titration readings Titration Rough 1 2 3 4 5 Initial 0.00 4.30 22.00 21.00 15.00 25.90 Final 4.30 22.00 38.60 37.60 32.60 42.20 Titre (cm3) 4.30 17.70 16.60 16.60 17.60 16.30 Therefore‚ the average titre would be calculated as follows;

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    extraction‚ crystallization and melting point determination‚ preparations of organic compound and separation of mixtures. The Techniques Students are REQUIRED to read and understand the various techniques that will be covered in the laboratory sessions from the textbook. | Techniques | Page | 1 | Laboratory Safety | 6 | 2 | Laboratory Glassware | 31 | 3 | Measurement of Volume and Weight | 39 | 4 | Heating and Cooling Methods | 58 | 5 | Reaction methods (eg: distillation‚ reflux) | 68 |

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    Fischer Esterification is a reaction between a carboxylic acid and an alcohol to form an ester. Refluxing the two reactants with an acid catalyst forms the ester. Fischer Esterification was discovered in 1895 by the German chemist‚ Emily Fischer and Arthur Speier. The reaction is also sometimes known as Fischer-Speier Esterification. The major components of almost all natural flavors and odors are esters. These fragrant esters are formed by the Fischer Esterification reaction. Saponification

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    Recrystallization of Methyl 3-nitrobenzoate Santiago Horta‚ Daniella I School of Chemistry and Biochemistry‚ Georgia Institute of Technology Atlanta‚ GA 30332 Submitted: 18 February 2015 In this experiment‚ the product of a nitration will be purified by recrystallization using a selected solvent. Methyl benzoate is treated with nitric acid and sulfuric acid to obtain methyl 3-benzoate‚ which will be mixed with a solvent that will dissolve the product at its boiling temperature but not at

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    Organic Chem Esterification

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    EXPERIMENT 5- A FISCHER ESTERIFICATION SYNTHESIS OF PEAR OIL One of the major uses of Esterification (C(=O)-C-R) is forming compounds with different odors which can be used to make different synthetic and natural flavorings.  Using the chemical and physical properties of organic compounds‚ an ester was catalyzed from the reaction of a carboxylic acid with an alcohol‚ producing an odor similar to that of pear oil. The mechanism of this Fischer- Esterification process is outlined as follows:

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    RECRYSTALLIZATION AND MELTING POINT DETERMINATION OF BENZOIC ACID ANSWERS TO QUESTIONS 1. How does the use of fluted filter paper hasten filtration? Why is it advisable to place a small piece of wire between the funnel and the mouth of the flask during hot filtration? Fluted filter paper is effective in preventing crystal formation in the filter paper. It is also often used in filtering hot saturated solution used during crystallization. One major advantage of a fluted filter is that it increases

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    To synthesis methyl orange by coupling diazotised sulphanilic acid with N‚N-dimethylaniline. Materials (Chemicals) Sulfanilic acid‚ 2.5% aqueous sodium carbonate solution‚ sodium nitrite‚ concentrated hydrochloric acid‚ N‚N-dimethylaniline‚ glacial acetic acid‚ 10% aqueous sodium hydroxide‚ saturated sodium chloride solution Apparatus 50 mL Erlemeyer flask‚ 250 mL beaker‚ test tube‚ hot plate‚ Buchner funnels Procedure In a 50 mL Elermenyer flask 1.2 g of sulfanilic acid and 12.5 mL of

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    Synthesis of Methyl Stearate The purpose of this lab was the convert liquid methyl oleate to solid methyl stearate by catalytic hydrogenation. Firstly‚ we produced hydrogen gas using solid mossy zinc and sulfuric acid. Using the hydrogen produced in the previous reaction‚ we were able to convert the liquid methyl oleate to solid crystals of methyl stearate. A mineral oil was also used to bubbler was used to maintain the hydrogen pressure slightly above the atmospheric pressure and to prevent back-diffusion

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    Methyl Salicylate Lab

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    began by weighing 4.0ml of methyl salicylate into a flask—a stir bar was added. While stirring‚ 40ml of 6M sodium hydroxide was added and the solution was heated and boiled for about 15 minutes. After the 15 minutes‚ a bit of water was used to wash down the sides of the flask and the solution was cooled. It was boiled for another 15 minutes‚ after this the solution was cooled for 5 minutes in an ice water bath. While the flaks was in the ice bath‚ 50ml of 6M hydrochloric acid was added in 5ml increments

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