bottom and sides of the flask so a spatula will probably be needed to scrape them out. Washing the flask and crystals with ice- cold xylenes completes this process. The resulting dried product was recrystalized using hot ethyl acetate. A hot plate was used to boil ethyl acetate to be poured into a heating beaker with a mixture of EtoAc and adduct until the product dissolved. A sequential suction filtration completed this
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reduced pressure. b) Hot extraction : In this extraction also 100gm powdered root was subjected to hot extraction. In this extraction the solvents are used polarity wise such as‚ Sl no: Solvents Polarity 1 Pet. Ether 0.1 2 Chloroform 4.81 3 Ethyl acetate 6.02 4 Ethanol 24.55 For 100gram of plant material yield (g) of the Leaves extract is as
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Chapter 1 INTRODUCTION Wine is an alcoholic beverage produced through the partial or total fermentation of grapes‚ other fruits and plants such as berries‚ apples‚ cherries‚ dandelions elder berries ‚ palm and rice can also be fermented. Grapes belong to the botanical family vitaceae of which there are many species. The species that are most widely used in wine production are Vitislabrusca and specially Vitisvinefara‚ which has long been the most widely used wine grape throughout the world
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Reminder: These notes are meant to supplement‚ not replace‚ the laboratory manual. A Diels-Alder Reaction History and Application: The 1950 Nobel prize in chemistry was awarded to Otto Paul Hermann Diels and Kurt Alder for their breakthrough work on the discovery and development of [4 + 2] cycloaddition reactions i. This set of reactions are enormously useful in the synthesis of six membered rings in a single stepii. These are used in many pharmaceutical applications. Tamiflu® is a drug which
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useful to make cinnamic acid. Experimental Section This experiment was performened on a 40 mmol scale. The materials we will use will be salicylaldehyde‚ Ethyl acetoacetane‚ Piperidine and Ethanol. In a 150ml single-neck round bottom flask equipped with a stir bar‚ add salicylaldehyde. We used 4.89g or one equivalent. Then add ethyl acetate to the round bottom flask. We added 5.47g or 1.05 equivalent. Add 40 mL of ethanol to the round bottom flask make sure to stir. While stirring add the piperidine
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Vallejos*‚ Ellis Mika C. Trino‚ Jahn Camille B. Valdez‚ Ariza Yamashita Department of Biological Sciences‚ College of Science Group 11 Corresponding author: gerome_911@yahoo.com Abstract The purpose of this experiment was to synthesize isopentyl acetate via Fischer esterification reaction between acetic anhydride and isoamyl alcohol‚ using concentrated sulfuric acid as a catalyst. This reaction is characterized by the combining of an alcohol and an acid (with an acid catalyst) to yield and ester
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as well as spotting the standard spinach extract. A beaker was used with the developing solvent‚ filter paper‚ and TLC plate inside and a watch glass over top of the beaker to perform the thin layer chromatography. After the solvent front (30% ethyl acetate in hexane) reached about an inch from the top‚ the TLC plate was removed from the beaker and the developing spots were marked. After implementing the column and thin layer chromatography‚ the Rf value for component one was .95‚ for component two
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The column fractions were collected in 25 ml test tubes. In that‚ fraction number 271-275th showed identical clear spot which were loaded on the activated silica gel TLC plates (20 cm × 20 cm). The plates were developed using methanol: ethyl acetate (60:40) solvent system. The single spot was located by exposing the plate to iodine fumes. Thus‚ it may indicate the presence of single
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Nitration of Methyl Benzoate Purpose: The purpose of this experiment was to synthesize methyl m-Nitrobenzoate from methyl benzoate‚ concentrated HNO3‚ and concentrated H2 SO4 by an electrophilic substitution reaction. The H2 SO4 and the HNO3 were initially combined to form nitronium ion which was then used as an electrophile in the reaction. Crystals that were collected after the formation of the methyl m-Nitrobenzoate were collected by vacuum filtration and the product was isolated and purified
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molecule This project will count as one lab grade. A sample grade sheet is on the back. Some possible molecules: Caffeine Theobromine Acetylsalicylic Acid (aspirin) Acetaminophen Ibuprofen Naproxen (Aleve) DEET Octyl acetate Isopentyl acetate Ethyl butyrate Methyl butyrate Methyl salicylate Isobutyl formate Citral Cinnamon aldehyde Vanillin Testosterone Estradiol Cholesterol Dopamine Serotonin Norepinephrine Pseudophedrine Methamphetamine AZT Nonoxynol-9 Nicotine
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