THE HIGHFIELD LEVEL 3 Health & Safety TRAINING PACK Lecture programme designed and written by Kirstie Trasler and Ian Fisher Disclaimer The information provided in this training package has been carefully compiled to ensure its relevance and accuracy. However‚ no liability or legal responsibility is accepted for the content or any errors or omissions. ©Highfield.co.uk Ltd Apart from any fair dealing for the purpose of private study or the purpose permitted under the UK Copyright‚ Designs
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Copper Complex 1. Place 10mL of N‚N-dimethylformamide (DMF) in a 25mL Erlenmeyer flask with boiling chips and heat on hotplate until slight boil. 2. Add 100 mg (0.16 mmol) TPP to the hot DMF‚ and dissolve 3. Add ~40 mg (0.20 mmol) of Copper (II) acetate‚ continue to heat at reflux for 5 min.
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degeneration‚most prominently in the striatum. The mechanism of neuronal degeneration is uncertainbut mitochondrial dysfunction may be one of the importantcontributors to neuronal dysfunction and finally neurodegeneration in HD.(5-7) Ethyl-eicosapentaenoate (ethyl-EPA) is a semisynthetic‚highly
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The Preparation of Methyl Salicylate Introduction: Esters have various smells that differ due to the types of carboxylic acids and alcohols one mixes together. This is called esterfication. The reaction is catalyzed by an inorganic acid usually H2SO4 Purpose: In this lab Methanol alcohol and Salicylic acid were reacted together to form Methyl Salicylate. This was done to determine the characteristic odour of the Methyl Salicylate. Safety: Safety goggles must be worn at all times. Methanol: Toxic
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Wars have been fought for thousands of years with different fighting styles and varying tactics. Fighting styles have been evolving since the dawn of time‚ as men have been learning how to defend themselves better and how to produce superior weapons. The weapons that were used in battle have become more deadly at an increasing rate. In World War I alone‚ more than 16 million people died‚ which made it one of the highest ranking wars in death total a war ever. Trench warfare was used extensively in
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Chapter 3 3.1 Identify the functional groups in each of the following molecules: O C NH2 H N O C OH H C CH2 (a) (b) O (c) Solutions: a. b. c. d. Amide‚ double bond Amine‚ carboxylic acid Double bond‚ ketone‚ ester O OCH3 (d) CH2OH Aromatic ring‚ double bond‚ alcohol (a) Alcohol (d) Amine (b) Aromatic ring (e) both ketone and amine (c) Carboxylic acid (f) two double bonds 3.2 Propose structures for simple molecules that contain the following functional groups:
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brown color with the addition of the remaining bromobenzene and ether added at a dropwise rate. The reaction vessel became warm at this point. The mixture then turned a reddish‚ pink color with the addition of 9.1g benzophenone in 100mL anhydrous ethyl ether. During the reflux the reaction mixture first turned a “pepto bismal” pink color then became a thick white liquid/solid. When the sulfuric acid was added the solution turned a yellow
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Abstract: The purpose of this lab is to prepare phenylmagnesium bromide‚ a Grignard reagent‚ and react it with benzophenone to give triphenylmethanol. Once made‚ the Grignard reagent will do a nucleophilic attack on the carbonyl carbon of the ketone‚ benzophenone. The result is an alkoxide that is then protonated to give the alcohol‚ triphenylmethanol. The purity of the final product will then be considered by melting point and IR spectroscopy. Final purified triphenylmethanol weighed 8.02 grams
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transition metal ion of Nickel(II)‚ that further more react with nickel acetate to form red crystals through condensation‚ the colour being constituded by the congugated bonds. These series of reactions synthesize the Schiff Base ligand and Nickel(II) complex of the Schiff base ligand. 0.36g of the Schiff base ligand is yielded and 0.1g of the nickel complex is yielded from the 0.36g Schiff base ligand and 0.5g nickel acetate. Introduction We perform two separate reactions in this experiment
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Introduction: In this experiment‚ when vinyl strip and acetate strip is rubbed by tissue‚ it will charge the vinyl strip negatively and acetate strip positively caused by the transfer of electron between the strip and tissue. If molecules have non zero bond dipole‚ because polar molecule must have a non-zero molecular dipole where electron spend more of their time closer to one atomic nucleus than the other and make one end partially positive or negative than the other end. Different charge will
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