Experiment 2 Title: Determination of Quinine in Tonic Water Objective: To Determine the Concentration of Quinine Hydrochloride in Sample (Schweppers) given‚ by plotting a Calibration Curve of Fluorescent Intensity against Concentration of Quinine Hydrochloride in ppm‚ after Fluorescence Intensity of a series of Standard Solution prepared and the Sample solution by Fluorescence Spectrometer. Data: Brand name of tonic water sample: Schweppes Dilution factor = 1000 Concentration of
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the percent composition of each product for both of the NMR spectra shown in this content area. Provide the average percent composition. Discussion: Discuss what the major product was in each case‚ and why‚ (thermo vs kinetic) Describe how NMR spectroscopy worked to determine the product concentration. Speculate how the opposite product composition might be obtained. Describe the reaction mechanism for the the two condensation reactions that were done. Predict the product that you would expect
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David Kennedy CHE 235 Lab 10/30/14 Scale-up Synthesis and Characterization of Butyl 2-Cyano-3-(3‚5-dichloro-phenyl)-2-propenoate‚ TSE Project #131 Introduction: This report describes the steps taken to create the scale-up of targeted trisubstituted ethylene‚ Butyl 2-Cyano-3-(3‚5-dichloro-phenyl)-2-propenoate compound (#131)‚ and also the characterization methods deployed to the results. This report serves as a critical step in the overall objective of the project; the synthesis of the copolymer
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Mass Determination of Ca‚ Fe and Zn in a multivitamin using Atomic Absorbance Spectroscopy (AAS) and X-Ray Fluorescence Spectroscopy (XRF) ABSTRACT: The purpose of this project was to determine the amount of calcium‚ iron and zinc present in an over the counter multivitamin. This mass was determined using atomic absorption spectroscopy (AAS) and X-ray fluorescence spectroscopy (XRF). For both analytical techniques‚ the method of standard additions was used to compensate for matrix effects.
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The technique by the name of Raman Spectroscopy was used (2013). This method detects laser light allowing for investigators to analyze lipstick marks left at the crime scene (2013). “Analyzing lipstick traces can be used to establish physical contact between two individuals‚ such as a victim and a suspect” (2013). This advancement is significant because current lipstick tracing relies on destructive forensic techniques or human opinion (2013). “Raman spectroscopy is ideal as it can be performed through
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of the alkene formed in a Wittig Reaction. The nitro group is substituted in the ortho‚ meta‚ and para positions‚ and benzaldehyde serves as a control. The ylide used is (carbethoxymethylene) triphenylphosphorane. Through the utilization of NMR spectroscopy‚ the products of the reactions will be analyzed to gain a ratio of E /Z isomers. Reaction Equations:Ethyl cinnamate from BenzaldehydeEthyl-3-(2-nirophenyl)acrylate from O-nitrobenzaldehydeEthyl-3-(3-nitrophenyl)acrylate from M-nitrobenzaldehydeEthyl-3-(4-nitrophenyl)acrylate
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Epoxidation Reactions Lab Report 2 Abstract An oxygen atom is transferred from a peroxy acid to the carbon=carbon double bond thus forming an epoxide. Scheme 1. Oxone Epoxidation. Scheme 2. mCPBA Epoxidation. The percent yield for the Oxone epoxidation reaction was 65% yield and the mCPBA epoxidation reaction was 70% yield. Oxone is the greener alternative because using mCPBA is twice as expensive as Oxone and leaves behind the epoxide plus m-chlorobenzoic acid while Oxone creates non-toxic
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Qualitative Analysis Lab Report Organic Chemistry Laboratory II ABSTRACT: The purpose of this lab was to separate and purify two unknown compounds‚ one solid and one liquid‚ from an ethereal solution using the techniques of chemically active extraction‚ vacuum filtration‚ simple distillation‚ and recrystallization. Then identifying information was compiled about these unknowns by obtaining experimental melting/boiling point ranges‚ and analyzing IR and proton/carbon NMR spectrums It was determined
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hydride addition is that product is entirely a racemic mixture (McMurry 696). After the initial reaction the product was isolated using a series of vacuum filtrations‚ ether extractions‚ and rotorary evaporations‚ before being analyzed via proton NMR spectroscopy. Results and Discussion: The table listed below as Table 1 lists the starting amounts of each of the chemicals present in the reaction flask‚ along with their formula mass. Compound: Moleculear Mass (g/ mol) Mass
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Abstract Chemically active extraction was used to separate two unknown compounds from each other and to determine what compound class each compound belongs. The solid unknown was purified by recrystallization and its melting point range was determined to be 109-111°C. The liquid unknown was purified by simple distillation and its boiling point was determined to be 95°C. An IR spectrum was collected for each of the purified compounds; the solid was determined to be 3-toluic acid and the liquid was
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