2-((6‚8-dibromo-2-(4-chlorophenyl)quinazolin-4-yloxy)methyl)-5-methyl-1‚3‚4-oxadiazole (IX) : A mixture of the hydrazide VII (0.01 mol) and acetic anhydride (30mL) was refluxed for 6h. The precipitated solid formed upon cooling‚ was filtered and recrystallized from ethanol‚ m.p. 155oC‚ 80% yield. Analysis calculated for C18H11Br2ClN4O2; Calcd.: %C‚ 42.34; H‚ 2.17; N‚ 10.97‚ Found: % C‚ 42.30; H‚ 2.14; N‚ 10.90. IR: υmax./cm-1 3000 (C-H aromatic)‚ 1610 (C=N) and at 1600 (C=C). 1H-NMR (DMSO-d6‚ ppm):
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used (ml) | 30.6 | 30.2 | 30.0 | | | | | Acid to Base Ratio | 0.87 | 0.86 | 0.86 | Average acid/base ratio | 0.86 | | | | | Base to Acid Ratio | 1.14 | 1.16 | 1.17 | Average base/acid Ratio | 1.16 | Name: Jared Philip Condez Date Performed: June 28‚ July 2 & 5‚ 2013 Partner: Shiela Mae Molina Date Submitted: July 12‚ 2013 Experiment 3 ACID – BASE TITRATION I. Objectives * Determine the purity of Potassium Acid Phthalate * To titrate effectively
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Experiment 1 mass determinations Objective: The purpose of this experiment is to see the difference of precision of different balances. When doing experiments we determine the mass my measuring the sample with a balance. There are many kinds of balances that measure to different precisions. This experiment shows the different results that two balances can give. Summary of Procedures Determine the mass with the triple beam scale to the most precise measurement possible for the scale.
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Lab: Electrostatic Coulomb Constant Rylee Rose Date: 1/28/13 Abstract: This experiment was done to study electrostatic and Coulomb’s law. Objective: The objective was to demonstrate the veracity of Coulomb’s Law. This was done by observing different equilibrium conditions of two pith balls that were equally charged. They were then constructed into a pendulum using strings. Calculations were done to determine the charge on pith balls‚ calculate the mass of the pith balls and to calculate
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Phuong Pham Prof. Johnson Lab 3 Gravimetric determination of Calcium as CaC2O4.H2O Feb‚ 27‚ 2014 I. Objective: The purpose of this lab is to determine how well gravimetric method measures the calcium level in a solution of known calcium concentration. II. Method: a) Overview: In this lab we will prepare 25 mL known concentration Calcium solutions. Then we will use Gravimetric method to determine the concentration of Calcium in each solution to figure out how well this method is. As we know
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the sum of the components of the series. In this experiment‚ you will measure the temperature change of two reactions‚ and use Hess’s law to determine the enthalpy change‚ ΔH of a third reaction. You will use a Styrofoam cup nested in a beaker as a calorimeter‚ as shown in Figure 1. For purposes of this experiment‚ you may assume that the heat loss to the calorimeter and the surrounding air is negligible. OBJECTIVES In this experiment‚ you will • Use Hess’s law to determine the enthalpy
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EXPERIMENT 2: Recrystallization and Melting Point Recrystallization (or Crystallization) is a technique used to purify solids. This procedure relies on the fact that solubility increases as temperature increases (you can dissolve more sugar in hot water than in cold water). As a hot‚ saturated solution cools‚ it becomes supersaturated and the solute precipitates (crystallizes) out. In a recrystallization procedure‚ an impure (crude) solid is dissolved in a hot solvent. As this solution is cooled
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EXPERIMENT 1 DETERMINATION OF ASCORBIC ACID CONTENT IN VITAMIN C TABLETS INTRODUCTION To calculate the mass of the ascorbic acid and hence the mass percentage of ascorbic acid in the vitamin C tablet. PROCEDURES (Refer to Lab Manual) 1. Accurately weight vitamin C (effervescent type) in a 50 ml beaker. Add about 30 ml of deionised water to dissolve the vitamin C tablet. Once the tablet has dissolved completely‚ transfer the solution into a 250 ml volumetric flask via a plastic filter
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______________________ Evaluation of the Gas Law Constant Objectives In this experiment‚ we will determine the Ideal Gas Constant‚ R‚ which relates the number of moles of gas present to its volume‚ pressure and absolute temperature. Background To see how "R" was derived‚ we must look at the proportionalities defined by the other fundamental gas laws. For example‚ Charles’ Law showed us that the volume of a gas sample is proportional to its absolute temperature at constant pressure. Thus V ∝ T abs . In addition
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Experiment 2 Lab Report: Calculating the Spring Constant and Verifying that Energy is Conserved Within a System Abstract: An experiment was conducted to determine the spring constant of a spring in the cart by measuring the force required to compress a spring as well as the distance the spring compressed relative to the equilibrium position. A cart was placed onto a slanted track and speed and force censors were used to record appropriate data. The spring constant was determined
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