INVESTIGATION #2 DETERMINATION OF THE WATER OF CRYSTALLISATION April 4‚ 2012 OBJECTIVE: Chemical compounds that contain discrete water molecules as part of their crystalline structure are called hydrates. Hydrates occur quite commonly among chemical substances‚ especially among ionic substances. More often than not‚ such compounds are either prepared in‚ or are recrystallized from‚ aqueous solutions. Hydrates exist for ionic compounds most commonly‚ but hydrates of polar and non polar covalent molecules
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Abstract The objective of this experiment was to observe multi-step purification of benzoic acid after performing the extraction from a mixture containing benzoic acid‚ cellulose‚ and methyl orange. Recrystallization was done to remove impurities from the sample. The amount of BA recovered during recrystallization is much less than the extracted amount of BA. The difference between the pure and impure samples was observed by comparison of melting points. It was found that impure samples will have
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1 UDEC1164 ORGANIC CHEMISTRY Name: Cheong Wai See Student ID: 1404057 Practical Group: 1 Title of Experiment: Name of Tutor: Dr. Mohammod Aminuzzaman Date: 24 February 2016 Tiltle: Nitration of Methyl Benzoate Objectives: -To prepare methyl-3-nitrobenzoate from nitration of methyl benzoate by electropilic aromatic substitution. -To calculate the percentage yield and get the melting point of methyl-3-nitrobenzoate. Introduction: Benzene contains compounds have special properties that make them
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Tittle: Determination of moisture Objectives: 1. To determine the moisture content of selected food samples using drying oven method 2. To determine the moisture content of selected food samples using moisture analyzer. Introduction: Moisture content is one of the most commonly measured properties of food materials. The choice of an analytical procedure for a particular application depends on the nature of the food being analyzed and the reason the information is needed. In this experiment‚ cookies
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ICSE Class X Chapter 5 Hydrogen Chloride and Hydrochloric Acid Hydrogen chloride (HCl) : Formula : HCl Nature : Covalent. Molecular Mass : 36·5u [i.e. HCl = 1 + 35·5 = 36·5] Occurrence : (i) Present in gastric juices. (ii) Present in volcanic gases. Laboratory preparation of HCl gas : Hydrogen chloride gas is prepared in laboratory by heating conc. H2SO4 with NaCl. NaCl + H2SO4 Heat → NaCl + NaHSO4 Heat → NaHSO4 + HCl Sodium hydrogen sulphate Na2SO4 + HCl
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Gravimetric Determination of Calcium ABSTRACT Determining the mass of a pure compound is a method of a gravimetric analysis. One of the gravimetric analyses is the precipitation; it is a method of separating the analyte from the unknown sample as a precipitate where it will be filtered and converted into a known composition that can be weighed to determine its mass (Skoog et al‚ 2013). Determining the mass of calcium by using gravimetric analysis was the objective of the experiment. A 25 mL of
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PRACTICAL 7 TITLE : DETERMINATION OF ERYTHROSINE CONCENTRATION USING UV- VISIBLE SPECTROPHOTOMETER INTRODUCTION In chemistry‚ spectrophotometry is the quantitative measurement of the reflection or transmission properties of a material as a function of wavelength. It is more specific than the general term electromagnetic spectroscopy in that spectrophotometry deals with visible light‚ near-ultraviolet‚ and near-infrared‚ but does not cover time-resolved spectroscopic techniques. Spectrophotometry
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CHM 3120L ANALYTICAL CHEMISTRY I LABORATORY REPORT EXPERIMENT: SPECTROPHOTOMETRIC DETERMINATION OF IRON IN DRINKING WATER Name: Steven Adrien Section: 3 Date Experiment Completed: Wednesday‚ July 17‚ 2013 1. Complete the following table Fe(II) stock solution | mass‚ g | 0.1756 | volume‚ mL | 500.0 | MW(Fe(NH4)2(SO4)2 x 6H2O)‚ g/mol | 392.14 | AW(Fe)‚ g/mol | 55.85 | conc. Fe(II)‚ ppm | 50.0 | Use Equation Editor to show how you calculated the concentration of Fe(II)
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Introduction The purpose of this experiment is to practice common organic laboratory techniques inside the lab to get one oriented to the basic methods of procedure that can be used for later experiments. This experiment involves the separation of benzoic acid from a more crude form‚ consisting of benzoic acid‚ methyl orange‚ a common acid/base indicator‚ and cellulose‚ a natural polymer of glucose (Huston‚ and Liu 17-24). The technique that is used to perform this separation is called extraction
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Introduction Extraction is a purification technique used in organic chemistry to separate compounds from a mixture of two or more compounds. There are three different extraction techniques: liquid-liquid extraction‚ solid-liquid extraction and chemically active extraction. All three types of extraction follow the same principle. Organic molecules dissolve in organic solvents and polar molecules dissolve in aqueous solvents. This phenomenon is observed because of the intermolecular forces between
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