The Grignard Synthesis of 3-methyl-3-heptanol In this experiment‚ an example of an organometallic compound which has a carbon magnesium bond will be utilized to form a tertiary alcohol. Grignard reagents have been extremely useful in the synthesis of a large number of classes of organic functional groups. Although Grignard reagents are unstable and decompose in air and moisture‚ they can be prepared and used immediately with moderate difficulty in the undergraduate organic chemistry laboratory
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Joelle Calugay______ An experiment to obtain and compare the spring constants of 3 strings (soft‚ medium‚ and hard) obtained in 2 ways (using the energy chapter and the dynamics chapter)‚ to confirm that Hooke’s Law is valid over a range of initial displacements‚ and to find the acceleration due to gravity on unknown Planet X. Problem: What are the spring constants of 3 strings (soft‚ medium‚ and hard) and how do they compare? Theory: To find the spring constants of each string‚ we can calculate
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transported to the liver‚ where it undergoes conjugation and excretion. Upon its separation from albumin on hepatocyte membrane‚ bilirubin binds to specific carriers and is intracellularly transferred to the site where it conjugates with glucuronic acid to form bilirubin diglucuronide and bilirubin monoglucuronide. During this process‚ the insoluble form of bilirubin is converted into its soluble form‚ known as conjugated or bound bilirubin. Upon conjugation‚ the bilirubin from hepatocytes is excreted
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Introduction: The theory behind the extraction of a solution containing benzoic acid‚ cellulose‚ and methyl orange involves many components pertaining to the fundamental ideas of solubility and polarity. Using the concepts of like dissolving like and acid base reactions‚ a solution of organic acid (benzoic acid)‚ a water soluble compound cellulose‚ and an organic soluble compound methyl orange‚ can be separated and benzoic acid can be isolated by a method of extraction. At the fundamental level‚
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of the number of moles of a substance there are in every cubic decimetre (litre) of solution‚ written as moles.dm-3 of M for short. • In this experiment you will find out how increasing the concentration of the acid solution changes the rate of the reaction between dilute hydrochloric acid and magnesium metal. • As the metal reacts with the acid‚ hydrogen gas is produced and the metal dissolves. To get an estimate of the rate of reaction‚ the time taken for a small piece of magnesium ribbon
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EXPERIMENT 11: DETERMINATION OF DISSOLVED OXYGEN IN A WATER SAMPLE (WINKLER METHOD) INTRODUCTION In an alkaline solution‚ dissolved oxygen will oxidize manganese(II) to the trivalent state. 8OH-(aq) + 4Mn2+(aq) + 2H2O(l) －－＞ 4Mn(OH)3(s) The analysis is completed by titrating the iodine produced from potassium iodide by manganese(III) hydroxide. 2Mn(OH)3(s) + 2I-(aq) + 6 H+(aq) －－＞ 2Mn2+(aq) + I2(aq) + 6H2O(l) Sodium thiosulphate is used as the titrant. Success of the method is critically
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Acids and Bases Q1.This question is about several Brønsted–Lowry acids and bases. (a) Define the term Brønsted–Lowry acid. ........................................................................................................................ ........................................................................................................................ (1) (b) Three equilibria are shown below. For each reaction‚ indicate whether the substance immediately above the box is acting
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Determination of Sulfate by Gravimetry Jose Luis E. De Guzman University of Santo Tomas‚ Sampaloc‚ Manila The determination of the percentage of sulfate in a sample is done as an instrument of learning a quantitative method of analysis‚ i.e.‚ of the gravimetric analysis. This type of analysis‚ which makes use of the weight of the samples was used for the experiment and required the precipitation of our analyte‚ SO4-2‚ and its filtration as a BaSO4 precipitate so as for weighing it. The weight
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Forming Methyl Orange an Azo Die Abstract: An synthetic azo dye was created by reaction of diazonium salt with N‚N-Dimethylanaline. The final product created was 4-dimethylaminoazobenzene-4-sulfonic acid‚ an orange clay-like substance. Sulfanilic acid was chemically manipulated by using sodium carbonate followed by cooled sodium nitrate and hydrochloric acid to form the diazonium salt used in the reaction. The products were washed in ethanol. The product was obtained at an 84% yield and was
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Determination of KHP – Acid - Base Titration For determining purity of unknown KHP‚ acid – base titration was used. Molarity of titrant in this case NaOH was standardized as 0.04958(±0.00011) M. Purity of unknown KHP was calculated as 35.88(±0.16) %. • Introduction Acid – base titration is typical method of determining unknown figures. Acid – base titration means that by using neutralization between acid and base. Abrupt changing of pH says whether procedure is done or not. pH indicators
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