EXPERIMENT 10 POTENTIOMETRIC REDOX TITRATION BAUTISTA ‚ Anne Judith LARIN‚ Michelle V. OBJECTIVES At the end of the experiment‚ the student should be able to: 1.Construct a potentiometric redox titration curve 2.Determine the % Fe in a sample by potentiometric redox titration INTRODUCTION Potentiometry definition indicator electrode reference electrode Potentiometric titration applications general procedure similarities with redox titration INTRODUCTION Determining the endpoint
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Theo Victor Cavite Chem 28.1 Melanie Bucsit-Carpio September 14‚ 2012 Spectrophotometric Determination of Iron in Aqueous Solutions as a Complex of 1‚10-Phenanthroline Introduction From the previous classical method of concentration determination of an unknown sample‚ this experiment now deals with the instrumental one. Unknown concentrations of iron in solutions were determined by measuring their corresponding absorbances through spectrophotometry. A spectrophotometer measures the amount
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Experiment V02 An analysis of aspirin tablets Procedure a. Weigh accurately a definite number of aspirin tablets (two or three tablets weighing no more than 1.5 g) into a 250 cm3 conical flask. Initiate the hydrolysis of the aspirin by adding 25 cm3 of 1.0 M sodium hydroxide by pipette‚ diluting with approximately the same volume of distilled water. Warm the flask over a tripod and gauze for ten minutes to complete the hydrolysis. b. Cool the reaction mixture and transfer with washings to
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Eric Wu 117 Experiment 1.6: Determination of Density Abstract: The purpose of the experiment was to determine if density is an intensive or extensive property of matter. The experiment proves that density is an intensive property. The density of an object remains the same no matter how much of it is present. The density is an intensive property because mass and volume changes at the same rate. Introduction: This experiment was designed to determine if density is an intensive or extensive
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DETERMINATION OF THE SOLUBILITY PRODUCT CONSTANT OF CALCIUM HYDROXIDE ABSTRACT This experiment aimed to determine the solubility product constant (Ksp) of Ca(OH)2 as well as to evaluate the effects of common and non-common ions on its solubility. Ca(OH)2 solids were dissolved in eight various media: distilled water‚ 1.0 M KCl‚ 0.5 M KCl‚ 0.1 M KCl‚ 0.05 M KCl‚ 0.005 M KCl‚ 0.001 M KCl‚ and 0.1 M Ca(NO3)2. The concentration of dissociated OH- concentrations was determined by means of titrimetric
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Experiment #5: Esterification of Methyl Benzoate from Benzoic Acid October 28‚ 2010 Abstract: This experiment was conducted to synthesize methyl benzoate from benzoic acid and methanol by using the Fischer esterification method. Methanol (12.5ml) and Benzoic acid (4.9 grams) are heated together in the presence of concentrated sulfuric acid (1.5ml) until equilibrium is achieved. A reflux apparatus is set up for 1 hour to carry out the reaction at the boiling point of the solvent (Methanol
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Monica Perez Experiment 8: Acetylsalicylic Acid Experiment 01/25/2013 CHM Lab- 2211 Sec 0016 Instructor: Jennifer Reed Introduction: Commonly used as Aspirin‚ acetylsalicylic acid is an analgesic (pain reliever)‚ which is one of the products of the esterification reaction between salicylic acid and acetic anhydride. This esterification occurs since the hydroxyl group from the salicylic acid reacts with acetic anhydride to form an ester. In this experiment‚ we will be able to recreate
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Lab 2: Spectrophotometric Determination of Iron In Vitamin Tablets Objectives: - To determine the amount of iron in a generic vitamin tablet on a per tablet (in grams) basis. - To prepare standards using a pre-made iron solution to help determine the iron content in our generic vitamin tablets - Determine absorbances of our vitamin tablets and standards using the spectrophotometer Method: 1. Mass three vitamin tablets that contain iron 2. Place each vitamin in a 125-mL Erlenmeyer flask
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Tacula‚ Jassy Camille D.S. Activity 11 Acids and Bases I. Objectives * To identify some acids and some bases which are used in common household products. * To construct an operational definition of an acid and a base‚ using the characteristic properties of those substances. II. Procedure A. For acids * Place 2ml each of dilute acetic acid‚ hydrochloric acid‚ sulfuric acid‚ carbonated drink (colorless) and calamansi juice extract in
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Experiment #10 & #11 The Synthesis of Cobalt Oxalate Hydrate The Synthesis of a Nitrite Complex February 5‚ 2012 Chemistry 1211L - 146 - Spring 2012 Procedure The Synthesis of Cobalt Oxalate Hydrate Place 100 ml of distilled water in a 250-ml (or 400-ml) beaker. Add 1.26g of oxalic acid dihydrate (H2C2O4.2H2O) and 1 ml of concentrated ammonia. Stir the mixture until the solid has dissolved completely. Dissolve 2.34 g of cobalt chloride hexahydrate (CoCl2.6H2O) in 100 ml of water
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