1.0 Calibration of Volumetric Glassware 1.1 Introduction: Calibration is the process by which a stated measure such as the volume of a container is checked for accuracy. In general‚ measurements of mass can be determined more precisely and accurately than measurements of volume. Therefore‚ the mass of the liquid contained or dispensed by the glassware will be measured and the corresponding volume calculated using the density of the liquid. However‚ a relatively small change in temperature
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9 Experiment A Volumetric Analysis A titrimetric analysis requires the careful addition of titrant. • To prepare and standardize a sodium hydroxide solution • To determine the molar concentration of a strong acid Objectives The following techniques are used in the Experimental Procedure Techniques 2 4 16b 16a 90 80 5 16c 6 13c 15a 15b ! A chemical analysis that is performed primarily with the aid of volumetric glassware (e.g.‚ pipets‚
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Experiment 2 CALIBRATION OF A PIPETTE Introduction An ordinary laboratory pipette may be expected to deliver its nominal volume with good precision and good accuracy if it is used in the way recommended. In this experiment we investigate the precision and accuracy of such a pipette by making accurate determinations of the mass of water it delivers in repeated operations. Materials 10.0-cm3 pipette‚ 50-cm3 beaker‚ thermometer‚ pipette filler‚ graph paper. Procedure
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NO | ANSWER | MARK | 1 :( i )( ii ) ( iii ) ( iv )2 :( i )( ii )( iii )3 )4 )5 ) ( i )( ii )( iii )( iv )6 )7 ) i )ii ) iii )8 )9 )10 )i ) ii )iii)11 ) | A reagent is highly serves as a reference material in all volumetric & mass titrimetric method.A reagent solution of accurately known concentration. * End point-point at which the reaction is observed to be complete and there is permenant colour change at the end of titration. * Equivalent point-point at which an equivalent amount of
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Chem-102 Lab Dr. Sobhi Experiment #3: Spectrophotometric Determination of Tartrazine Purpose The objectives of this lab include- illustrating the use of the spectrophotometer in chemical analysis‚ and generating a standard‚ or calibration curve‚ then using that curve to determine the value of an unknown substance. The spectrophotometer is one of the most powerful tools used in chemistry to find the concentration of substances in solution. It compares the colors of a known and an unknown solution
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Part A- Additive Volumes First‚ obtain a dry 10 mL volumetric flask that includes a stopper with it and weight on a digital scale. Be sure to get the mass at the closest milligram. Then‚ pour DI water to the calibration mark of the flask. Place the stopper back and weigh it again on the same digital scale. Once recorded‚ it is okay to pour this water down the drain. Observations: Mass of Empty Flask Mass of DI Water Filled Flask 15.114 g 25.048 g Now‚ put 100 mL of ethanol in a beaker and
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Objective: Find the percentage of iron in a given sample through titration. EDTA CONCENTRATION 0.02060 M Mass of Ferric Salt 1.8193 g Burette Readings ( in mL) Trial 1 Trial 2 Trial 3 Final 42.19 21.29 39.69 Initial 23.35 2.61 21.21 Endpoint Volume 18.85 18.6 18.47 Average of the endpoint volumes V= 18.64 mL % Fe ± Sv 11.78% ± 0.19313 Calculations: sV= {[(v1 – V)^2 + (v2 – V)^2 + (v3 – V)^2]/2}^(1/2) {[(18.85 – 18.64)^2 + (18.6 – 18.64)^2 + (18.47
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VOLUMETRIC ANALYSIS 1. In volumetric analysis‚ the volume of a reagent needed to react with analyte is measured. 2. In a titration‚ increments of the reagent solution -the titrant-are added to the analyte until their reaction is complete. 3. The most common titrations are based on: - acid-base - oxidation-reduction - complex formation and - precipitation reactions 1. Methods of determining when the analyte has been consumed include: - detecting a sudden change in
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Experiment 9 and 10: Volumetric/Vinegar Analysis Abstract: The goal of the experiment that was conducted was to figure out both the molar concentration of NaOH and the standard mole ratio of the NaOH solution. In order to find the concentration of the NaOH solution‚ volumetric analysis was used. In volumetric analysis‚ a titration mechanism was utilized in order to find the reaction that the base will end up having with KHC8H4O4
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Lab 1: Calibration of Pipettes and Burettes Names TA Name‚ Thursday Lab: 1:40 P.M. - 4:10 P.M. Aim: This experiment sought to gather data regarding water volume gathered in glassware‚ then to statistically analyze the data‚ focusing on average and standard deviation‚ along with relative error gleaned from linear regression. Introduction: This experiment was divided into two parts. For part one of the experiment‚ 25 mL were transferred from a glass pipette to a tarred beaker and weighed
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