Organic Lab Part 2 Experiment 7: Diethyl n- Butylmalonate Lab Partner: Reference: Williamson K.L.‚ & Masters‚ K.M. (2011).”Diethyl n- Butylmalonate”. Macroscale and Microscale Organic Experiments ( 6th edition pp. 531-534)
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Abstract Separation of the compound ethanol from alcoholic beverages‚ such as vodka‚ involves the process of distillation. Distillation is the separation of volatile substances mixed with nonvolatile substances by boiling the mixture to alter the phase of the volatile substance. The researchers used the simple distillation set up to conduct the experiment. 25 ml of The Bar Vodka was used and 7 ml of distillate was collected before a temperature of 95 degrees Celsius was reached. Collected distillate
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Tetrapyrrole compounds: chlorophyll and heme groups By Erwin Lim 1. Tetrapyrrole compounds A tetrapyrrole compound is a chemical group that consists of four pyrroles that are joined together by covalent bonds‚ forming a porphyrin ring. They are naturally occurring pigments‚ which are used in many biological processes (Berg‚ 2009). The basic structure of a tetrapyrrole is as seen in Figure 1‚ while the basic structure of a pyrrole is as seen in Figure 2. Figure 1.Tetrapyrrole Compound (Berg‚ 2009)
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EXPERIMENT 1: REACTIONS OF ENOLATE IONS WITH CARBONYL GROUPS Aims In this experiment we used two techniques for the reactions of enolate ions with carbonyl groups. One technique used was Doebner reaction and the other technique used was Claisen-Schmidt reaction. Therefore the aim of this experiment is to synthesize trans p-methoxycinnamic acid and to synthesize dibenzalacetone via an aldol condensation reaction between acetone and benzaldehyde. The products would be recrystallized using ethanol
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Experiment 2: IDENTIFICATION OF UNKNOWNS BY TLC AND MP IN COMBINATION Introduction: Thin layer chromatography (TLC) is one of the most valuable techniques in organic chemistry. This is a best method of separating and identifying mixtures of two or more compounds. The separation is accomplished by the distribution of the mixture between two phases: one that is stationary and one that is moving or mobile. Chromatography works on the principle that different compounds will have different
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3/5/2011 EXPERIMENT EXPERIMENT 8 OBJECTIVES CONCEPTS REAGENTS PROCEDURE RESULTS DISCUSSION IR ANALYSIS 8 Objectives to differentiate various types of oxygen-bearing organic compounds to device a scheme to distinguish each functional group Analysis of Oxygen-bearing Organic Compounds alanx3@yahoo.com OBJECTIVES CONCEPTS REAGENTS PROCEDURE RESULTS DISCUSSION IR ANALYSIS to characterize an unknown sample through parallel chemical tests ARMSALCEDO ARMSALCEDO alanx3@yahoo
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Organic chemistry Organic chemistry is one of the ‘branches’ of chemistry and is seen as distinct from other branches‚ such as inorganic and physical chemistry. It can be described as the chemistry living processes (often referred to as biochemistry) but extends beyond that. It focuses almost entirely on the chemistry of covalently bonded carbon molecules and as well as life processes‚ it includes the chemistry of other types of compounds‚ including plastics‚ petrochemicals‚ drugs and paint
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constituent compounds discovered in past centuries - although not all aromatic compounds known today share the same distinction (many are in fact‚ odorless or even unpleasant)‚ they are the principle components in such pleasant smelling substances as cinnamon‚ licorice‚ wintergreen‚ clove & vanilla CLASSIFICATION – - also known as arenes‚ many aromatic compounds possess the benzene ring functional group: G’s FG = aromatic compound or arene benzene ring or aryl grp - other compounds which do
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www.igcse.at.ua ORGANIC CHEMISTRY OIL and its many useful PRODUCTS The origin of oil Crude oil is formed from organic material of the remains of plant and animal organisms that lived millions of years ago. These remains form sediments eg at the bottom of seas‚ and become buried under layers of sedimentary rock. They decay‚ without air (oxygen)‚ under the action of heat and pressure to form crude oil over millions of years. It is a fossil fuel because it is formed from
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Organic Chemistry/Biochemistry 1: Compounds Important to Life • Biologists classify compounds into organic compounds and inorganic compounds. Organic Compound: a compound that is derived from living things and contains carbon Inorganic Compound: a compound generally derived nonliving things • Water Water is an inorganic molecule with unique properties that make it one of the most important compounds for living things. In the water molecule (H2O)‚ the hydrogen and oxygen atoms bond
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