"Experiment 55 a separation and purification scheme" Essays and Research Papers

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    Separation

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    TEACHER’S GUIDE CHEMISTRY TOPIC: OBSERVATIONS AND EXPERIMENTS USEFUL TIPS: Student’s experiments can be done in groups. Groups can be given different mixtures. Each group then carry out their own experiment‚ makes a write up of their procedure and presents to the rest of the class together with the samples obtained. UNIT 1: MIXTURES AND PURE SUBSTANCES This unit is suitable for senior one (S1) BRIEF DESCRIPTION OF THE UNIT: This unit deals with: • Methods of separating

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    Nitration and Purification of Bromobenzene Abstract: An electrophilic aromatic substitution reaction was performed on bromobenzene with nitric acid producing both 2-bromonitrobenzene and 4-bromonitrobenzene. Products of the reaction were purified through multiple recrystallizations and column chromatography creating multiple crops of a yellow powder. The percent yield of products was determined to be 51%. The melting point of Crop 1 was found to be 110-115 °C‚ and Crop 2 was found to be 37-90

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    Chemistry Investigatory Project To determine minimum amount of Bleaching Powder Required to disinfect different samples of Water. INDEX I. Introduction o Purification of Water o History of Water Purification o Bleaching Powder II. Experiment o Aim o Requirements o Theory o Procedure o Observations o Result o Precautions Introduction 98% of the Earth’s water is present in the oceans with an average salinity of 3.5%. The remainder of the

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    Purification of Infliximab[3] begins at Stage 1 with the filtration of the harvest material using a spin filter. The harvest is then clarified and undergoes 3 main chromatographic steps. Firstly‚ at Stage 2‚ the direct protein capture by Protein A affinity chromatography helps to remove a large majority of the impurities whicn include viruses and media components. At Stage 3‚ prior to cation exchange chromatography‚ the purified material in the eluted stream is then subjected to freezing‚ thawing

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    mummion assignment Task 1 – purification Aim We were given a sample of mummion in the form of dried mud from a lake; the aim of the practical was to purify the sample and separate it from the insoluble impurities into the form of mummion salt. Context A long time ago mummion was used to preserve the bodies of ‘mummies’ in ancient Egypt‚ mummion along with other naturally occurring preservatives was used to treat the organs before the bodies were wrapped. This purification practical happens very often

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    Experiment C: Identification and Separation of Dyes by TLC Pre-lab Properties: Ethyl acetate‚ ethanol‚ silica‚ azobenzene‚ azulene‚ 4-(p-nitrophenylazo) resorcinol‚ methyl red‚ bromocresol green (solubilities in water and ethanol) Purpose: To identify compounds from an unknown mixture using TLC Up to 100% of missed points can be recovered from this lab Watch the video: http://www.youtube.com/watch?v=e99nsCAsJrw (MIT) TLC plates are near the main hood DO NOT BREAK CAPILLARY TUBES Keep spots small

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    The Separation

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    Music Appreciation April 30‚ 2013 “The Separation” The separation of church music and secular music during the Baroque period was the beginning of something new. Many people had no idea that the instruments they used during the Renaissance period could do more than they had been doing with them. This brought a new meaning of music and life into the world. It was a great change for music‚ instruments‚ and even people. Church music‚ also known as sacred music‚ was well known in the Renaissance

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    separation

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    CHAPTER 6 MECHANICAL-PHYSICAL SEPARATION PROCESSES Introduction Separation Processes Many chemical processes materials and biological substances occur as mixtures of different components in the gas‚ liquid‚ or solid phase. In order to separate or remove one or more of the component from its original mixture‚ it must be contacted with another phase. The two-phase pair can be gas-liquid‚ gas-solid‚ liquid‚ or liquid-solid. Absorption When the two contacting phases are a gas and a liquid

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    Purification of an Ester

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    Introduction ESTERS are compounds derived from the reaction of a organic acid with an alcohol. Acid + Phenol/alcohol --> ester + water R--C=O + R’--OH ----> R--C=O + H2O | | C-OH C-O-R’ Esters are the compounds that give fruits their characteristic flavours and odours. ie. methyl salycilate is "Oil of Wintergreen". http://www.petrik.com/PUBLIC/library/misc/glossary_of_org_chem.htm#ESTERS Aim To synthesise the ester 3-methylbutyl ethanoate( isopentyl acetate) and to identify the product

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    Chem 2203 Sec 026 27/September/2013 Experiment 3B: Fractional Semi-microscale Distillation Separation of Hexane and Toluene. Objective: The main goal of this lab is to learn how separation of binary liquid mixtures is performed. Especially when the two liquids have boiling points varying by about 30° C. Hexane can be separated from toluene in this experiment because of the difference in their boiling points. Since toluene has a higher boiling point‚ it will left at the bottom while the hexane

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