Nitration and Purification of Bromobenzene Abstract: An electrophilic aromatic substitution reaction was performed on bromobenzene with nitric acid producing both 2-bromonitrobenzene and 4-bromonitrobenzene. Products of the reaction were purified through multiple recrystallizations and column chromatography creating multiple crops of a yellow powder. The percent yield of products was determined to be 51%. The melting point of Crop 1 was found to be 110-115 °C‚ and Crop 2 was found to be 37-90
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Experiment C: Identification and Separation of Dyes by TLC Pre-lab Properties: Ethyl acetate‚ ethanol‚ silica‚ azobenzene‚ azulene‚ 4-(p-nitrophenylazo) resorcinol‚ methyl red‚ bromocresol green (solubilities in water and ethanol) Purpose: To identify compounds from an unknown mixture using TLC Up to 100% of missed points can be recovered from this lab Watch the video: http://www.youtube.com/watch?v=e99nsCAsJrw (MIT) TLC plates are near the main hood DO NOT BREAK CAPILLARY TUBES Keep spots small
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Music Appreciation April 30‚ 2013 “The Separation” The separation of church music and secular music during the Baroque period was the beginning of something new. Many people had no idea that the instruments they used during the Renaissance period could do more than they had been doing with them. This brought a new meaning of music and life into the world. It was a great change for music‚ instruments‚ and even people. Church music‚ also known as sacred music‚ was well known in the Renaissance
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CHAPTER 6 MECHANICAL-PHYSICAL SEPARATION PROCESSES Introduction Separation Processes Many chemical processes materials and biological substances occur as mixtures of different components in the gas‚ liquid‚ or solid phase. In order to separate or remove one or more of the component from its original mixture‚ it must be contacted with another phase. The two-phase pair can be gas-liquid‚ gas-solid‚ liquid‚ or liquid-solid. Absorption When the two contacting phases are a gas and a liquid
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Introduction ESTERS are compounds derived from the reaction of a organic acid with an alcohol. Acid + Phenol/alcohol --> ester + water R--C=O + R’--OH ----> R--C=O + H2O | | C-OH C-O-R’ Esters are the compounds that give fruits their characteristic flavours and odours. ie. methyl salycilate is "Oil of Wintergreen". http://www.petrik.com/PUBLIC/library/misc/glossary_of_org_chem.htm#ESTERS Aim To synthesise the ester 3-methylbutyl ethanoate( isopentyl acetate) and to identify the product
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Study of Water Purification Methods Water is the most essential component of life on Earth. In the United States‚ the average person uses about 75 gallons per day of freshwater. Most of this water is pre-treated in facilities and comes out of the tap clean and ready for drinking‚ a fact many take for granted. If you are camping and hiking you won’t always have access to this source of healthy‚ potable water. Unfortunately‚ many water sources in the wilderness include microorganisms‚ bacteria
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The Isolation‚ purification and identification of Proteins assayed From Bovine Liver Using SDS Gel Electrophoresis‚ Mass Spectroscopy and Western Blotting Abstract The purpose of the experiment was to isolate and recognize varying protein solubilization and assaying methods by using bovine liver protein. The experiment implicated the impact of different types of solvents like ethanol‚ water‚ PBS‚ PBS+1% Triton x-100‚ and PBS+2% SDS on protein solubilization. Bradford and Ghosh/Dumbroff
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of experiment‚ we would generally see a decreasing trend for the total activity‚ total amount of protein‚ and percent yield and an increasing trend for specific activity and fold purification. These trends come about naturally when performing multiple purification steps. To determine the success of each purification step‚ the more important factors to look at are the total activity units‚ total protein amount‚ and percent yield. Looking at our purification table (table 7) our purifications were
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CONTENT INTRODUCTION WATER PURIFICATION BY NANOPARTICLES NANOPARTICLES IN WASTE WATER TREATMENT MATERIALS AND METHODS CONCLUSION REFERENCES INTRODUCTION WATER PURIFICATION: It is the process of removing undesirable chemicals‚ biological contaminants‚ suspended solids and gases from contaminated water. NEED: The goal of this process is to produce water fit for a specific purpose
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Chem 2203 Sec 026 27/September/2013 Experiment 3B: Fractional Semi-microscale Distillation Separation of Hexane and Toluene. Objective: The main goal of this lab is to learn how separation of binary liquid mixtures is performed. Especially when the two liquids have boiling points varying by about 30° C. Hexane can be separated from toluene in this experiment because of the difference in their boiling points. Since toluene has a higher boiling point‚ it will left at the bottom while the hexane
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