Experiment 2: IDENTIFICATION OF UNKNOWNS BY TLC AND MP IN COMBINATION Introduction: Thin layer chromatography (TLC) is one of the most valuable techniques in organic chemistry. This is a best method of separating and identifying mixtures of two or more compounds. The separation is accomplished by the distribution of the mixture between two phases: one that is stationary and one that is moving or mobile. Chromatography works on the principle that different compounds will have different
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EXPERIMENT 1: REACTIONS OF ENOLATE IONS WITH CARBONYL GROUPS Aims In this experiment we used two techniques for the reactions of enolate ions with carbonyl groups. One technique used was Doebner reaction and the other technique used was Claisen-Schmidt reaction. Therefore the aim of this experiment is to synthesize trans p-methoxycinnamic acid and to synthesize dibenzalacetone via an aldol condensation reaction between acetone and benzaldehyde. The products would be recrystallized using ethanol
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Lab Report Experiment 1 & 2 CHM-101 Amele Takpara Partner: Jessamyn Dupree ------------------------------------------------- Experiment 1 ------------------------------------------------- (Pre-Lab Questions) 1. In the design of a Bunsen burner‚ explain the purpose of a. the gas control valve The gas control valve regulates the rate at which methane enters the burner. b. and the air vents. The air vents control the rate at which air enters the burner 2. Why is a luminous
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Physical Properties of Organic Molecules Abstract Identifying the physical properties of compounds can be useful in several ways. It helps us to determine the structure of certain compounds‚ the purity of substances and if a substance is not pure we can figure out how to separate contaminating substances from a compound. In this experiment‚ I learned how to determine a solid’s melting point and why some melting point ranges may be broader than others.
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The vapor pressure of a liquid is the equilibrium pressure of gas molecules from that liquid (i.e.‚ the results of evaporation) above the liquid itself. A glass of water placed in an open room will evaporate completely (and thus never reach equilibrium); however‚ if a cover is placed on the glass‚ the space above the liquid will eventually contain a constant amount of water vapor. How much water vapor is present depends on the temperature‚ but not on the amount of liquid that is present at equilibrium
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Jessica Robins Lab 3: Properties of Organic Compounds Introduction Distillation is a physical process used to separate chemicals from a mixture by how easy they vaporize. The temperature rises unit it reaches the temperature of the lowest boiling substance in the mixture while the other contents of the mixture remain in their original phase (until the most volatile substance has all boiled off) as it’s heated. Hot vapor results and passes into a condenser and is then converted to a liquid
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process of distillation. Distillation is the separation of volatile substances mixed with nonvolatile substances by boiling the mixture to alter the phase of the volatile substance. The researchers used the simple distillation set up to conduct the experiment. 25 ml of The Bar Vodka was used and 7 ml of distillate was collected before a temperature of 95 degrees Celsius was reached. Collected distillate was then subjected to a flammability test to confirm ethanol content. The percent ethanol was computed
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case osmosis will cause more water to move out of the cell than will move in the cell and the cell will shrink. In this case‚ we say that the solution is “hypertonic”. Learn more about osmosis and diffusion from Chapter 3 of your textbook. CELERY EXPERIMENT We can place celery in three different water solutions to observe the effects of osmosis on the celery stalks. Salt will serve as our solute to
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EXPERIMENT 5 REDOX TITRATION: TITRATION USING SODIUM THIOSULPHATE Objectives 1. 2. To prepare a standard solution of potassium iodate for use to determine the concentration of sodium thiosulphate solution accurately. To acquire the proper techniques of carrying out a titration. Introduction Redox titrations using sodium thiosulphate as a reducing agent is known as iodometric titration since it is used specifically to titrate iodine. The reaction involved is: I2 + 2Na2S2O3 I2 + 2S2O322NaI + Na2S4O6
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Experiment #1: Introduction to Experimentation Submitted by: Neann Klara M. De Jesus BS Psychology II Submitted to: Dr. Geraldine E. Tria ABSTRACT SUMMARY The first experiment done by the class was called “Introduction to Experimentation”. Its main objective is to give basic knowledge about some of the logic of experimentation. The class was divided into groups of 2. In each group there was an experimenter (E) and a subject (S). The experimenter instructed
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