Spectrophotometric Methods: The Determination of Iron The goal of this laboratory experiment was the quantitative spectrophotometric determination of Fe (II) by using a calibration plot‚ which obeyed the Beer-Lambert Law. In order to determine the Fe (II) concentration‚ a series of solutions of known concentrations were made. The solutions were analyzed by the Ocean Optics spectrophotometer in order to determine their absorbance. The concentration of the unknown Fe (II) was determined by the “eye-ball”
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Experiment A Spectroscopic determination of Iron with Phenanthroline Unknown # 2 Mass of Mohr’s Salt: 0.2040 1. 5mL of 6M acetic acid was measured and transferred into a 100mL volumetric flask with a pipette and diluted to the mark. Concentration = [0.2040(±0.0001)g/100(±0.08)mL]*[(1mol/392.16g)/(1L/1000mL)] = 0.005202(±0.09382%) = 0.005202(±0.000005)mol/L 2. 10mL of the above stock solution was transferred to a 250 mL volumetric flask and diluted to the mark. Concentration
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Eric Wu 117 Experiment 1.6: Determination of Density Abstract: The purpose of the experiment was to determine if density is an intensive or extensive property of matter. The experiment proves that density is an intensive property. The density of an object remains the same no matter how much of it is present. The density is an intensive property because mass and volume changes at the same rate. Introduction: This experiment was designed to determine if density is an intensive or extensive
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Title: Determination of Iron in Natural water by Spectrophotometry. Aim: To determine the iron in natural water by spectrophotometry. Abstract: The iron in natural water was determined by utilizing spectrophotometric analysis. That was done by measuring the absorbance of five Fe(oPH)2+3 standards at 510 nm. From that information‚ a calibration curve was plotted and used to find the amount of Fe2+ that was in two unknown water samples based on the absorbance readings obtained with them at 510nm. The
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EXPERIMENT : Iron in Breakfast Cereal by Atomic Absorption Spectroscopy OBJECTIVES : 1) To determine the actual iron content of different brands of cereals 2) To compare the experimental results with the values listed on the manufacturer’s labels. INTRODUCTION : Iron is one of the important minerals that is required for our bodies to function properly. Most of the iron in our body is found in the blood such as haemoglobin‚ approximately 60 -70% of the human body’s iron is found
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Determination of Iron by Reaction with Permanganate-A Redox Titration Purpose: The purpose of this experiment was to find the percentage of iron in an unknown iron oxide sample which could be determined through titration with a standard solution of potassium permanganate. Success in this analysis requires careful preparation and attention to detail. Performing this experiment also provides practice at titrations. The overall reaction is: 8H+(aq) + MnO4-(aq) + 5e- Mn2+(aq) + 4H2O Theory:
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Abstract: The purpose of this experiment was to determine the percentage purity of the iron(II) salt in an unknown sample. We performed titrations using Potassium permanganate which is a strong oxidizing agent‚ with unknown sample dissolved in deionized water. The result of the experiment was a 99.5% purity for the anhydrous iron (II) ammonium sulfate. Introduction: In this experiment‚ oxidation/reduction (or redox) will be used in the titration analysis of an iron compound. We will use potassium
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Lab 2: Spectrophotometric Determination of Iron In Vitamin Tablets Objectives: - To determine the amount of iron in a generic vitamin tablet on a per tablet (in grams) basis. - To prepare standards using a pre-made iron solution to help determine the iron content in our generic vitamin tablets - Determine absorbances of our vitamin tablets and standards using the spectrophotometer Method: 1. Mass three vitamin tablets that contain iron 2. Place each vitamin in a 125-mL Erlenmeyer flask
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Experiment 4A: Determination of a Partition Coefficient for Benzoic Acid in Methylene Chloride and Water Experiment 4B: Solvent Extraction I: Acid-Base Extraction Using the System Benzoic Acid‚ Methylene Chloride‚ and Sodium Bicarbonate Solution Objective A: To accustom participants (students) to general procedures that are used to obtain a partition coefficient at the microscale level. We will gain experience in such practices as the transfer of microliter volumes of solutions with a Pasteur filter
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Theo Victor Cavite Chem 28.1 Melanie Bucsit-Carpio September 14‚ 2012 Spectrophotometric Determination of Iron in Aqueous Solutions as a Complex of 1‚10-Phenanthroline Introduction From the previous classical method of concentration determination of an unknown sample‚ this experiment now deals with the instrumental one. Unknown concentrations of iron in solutions were determined by measuring their corresponding absorbances through spectrophotometry. A spectrophotometer measures the amount
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