Experiment 2 and 3: Synthesis of Aspirin and Determination of Melting Point A. Abstract Aspirin is the common name for the compound acetylsalicylic acid‚ widely used as a fever reducer and as a pain killer. The first part of the experiment aims to synthesize aspirin from the reaction of salicylic acid with acetic anhydride with the aid of phosphoric acid as a catalyst. The second part of the experiment aims to assess the purity of aspirin through the determination of its melting point and
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Synthesis of DEET Abstract: For this experiment m-toluic acid was reacted with thionyl chloride resulting in a nucleophilic acyl substitution which could then be used to create DEET with excess diethyl amine (Figure 1). This was done by adding diethyl amine drop wise using a seperatory funnel which resulted in a gas formation which was controlled with a condenser attached to a gas vacuum. The resulting mixture was then washed to remove excess acids and bases and rotovapped. DEET was synthesized
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Experiment 23: Synthesis of an Alkene April 5‚ 2013 Purpose: Results and Discussion The weight of our n-Butyl Bromide sample (actual yield) was 0.09g. The percent yield was found to be 4.38%. Only 0.09g of the theoretical 2.055g yield was obtained. The boiling point was 104° C‚ which is higher than the literature value of 101° C. This is due to the sample being somewhat impure‚ as impurities tend to increase boiling point. When IR spectroscopy was performed‚ there were no OH stretches
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Synthesis Essay In our world‚ we constantly encounter problems. There will be more significant and life-changing obstacles‚ and also many smaller‚ less threatening ones. But what matters most is not the size or relevance of those challenges‚ but instead‚ it is more important as to how one deals with the problem. Adversity of all different types and sizes reveals one’s character. One type of adversity‚ physical adversity‚ happens in various ways. In Mitch Albom’s book‚ Tuesdays with Morrie‚ Albom
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Tracey Thompson AP Lang Ms. Ransom 15 Dec‚ 2013 Synthesis Essay In 2013 a study by the US Department of Education showed that only 32 percent of American fourth-graders are reading at or above the proficiency of their grade level. One out of every 3 students in America have scored "below basic" on the National Assessment of Education Progress (NAEP) reading test. the United States was once the leading country in every aspect‚ including education‚ but now it has fallen behind to 17th place
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replication in a eukaryotic cell is more difficult. DNA of an eukaryotic cell is in chromatin form to fit into the small nucleus for the replication to occur‚ first the DNA should open. This is because it is harder for eukaryotes to carry out DNA synthesis. Replication of DNA in a prokaryote is different from a eukaryote. In a prokaryote they have a single origin where the replication process starts. Also eukaryotes synthesize the same time they are being transcribed‚ and ribosomes will be active
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Synthesis of Cyclohexanol Author: Ahmed Ayyash 06/06/13 Introduction: In this experiment‚ cyclohexanol was prepared from an initial cyclohexene. However‚ this occurred over a number of steps‚ these are out lined below. 1. Cyclohexene + aqueous acid cyclohexyl cation 2. cyclohexyl cation + hydrogen sulphate + water protonated cyclohexanol + cyclohexyl hydrogen sulphate 3. cyclohexyl hydrogen sulphate protonated cyclohexanol + HSO4 4. protonated cyclohexanol + HSO4
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Anthony Felix 10/27/11 Che12ALR Synthesis of Diphenylacetylene Observation of Results: 1‚2-dibromo-1‚2-diphenylethane | 0.204g | Diphenylacetylene | 0.087g | Theoretical yield | 0.107g | Percent yield | 81.3% | Melting point range of diphenylacetylene | 57- 60°C | Average melting point | 58.5°C | Average literature melting point | 60.0°C | Percent error of melting point | 2.5% | Calculations: Theoretical yield: Limiting reagent (LR) x M.W. (LR) x Mole to Mole ratio x M.W. (product)
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In the second separation of this experiment‚ the Erlenmeyer flask with the first filtrate was put into a beaker so the filtrate was in the beaker. The beaker was then heated on a hotplate until near boiling. After the whey protein had precipitated‚ a vacuum filter was used to filter out the whey. These proteins were then air-dried. A qualitative test was done to indicate that the sample extracted was the protein whey. Again‚ a small test tube was used and 2 mL of protein test solution was put in
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Synthesis Essay Four The minimum drinking age articles “Tempest in a Bottle”‚ by Shari Roan‚ “The Perils of Prohibition”‚ by Elizabeth M. Whelan‚ “The Minimum Legal Drinking Age: Facts and Fallacies” by Traci L. Toomey‚ Carolyn Rosenfeld‚ and Alexander Wagenaar‚ “De-Demonizing Rum: What’s Wrong with “Underage” Drinking?” by Andrew Stuttaford‚ are articles that represent why underage people shouldn’t be allowed to drink alcohol beverages. In the “Tempest in a Bottle”‚ by Shari Roan‚ explains
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