in the 100 mL beaker‚ heated it up to separate the sodium chloride and benzoic acid from the insoluble sand‚ then poured out the benzoic acid and sodium chloride into a separate cup and allowed I to chill in an ice bath for approximately five minutes. I dried up the sand and calculated the net weight for that. I poured the benzoic acid and sodium chloride mixture into a filtered funnel that caught the majority of the benzoic acid and allowed the sodium chloride to drain through to the cup. I allowed
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General College Chemistry LabPaq / Published by: Hands-On Labs‚ Inc. sales@HOLscience.com / www.HOLscience.com / Toll Free 866.206.0773 A Laboratory Manual of Small-Scale Experiments for the Independent Study of General College Chemistry 50-0123-CK-02 LabPaq® is a registered trademark of Hands-On Labs‚ Inc. (HOL). The LabPaq referenced in this manual is produced by Hands-On Labs‚ Inc. which holds and reserves all copyrights on the intellectual properties associated with the LabPaq’s
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The Stereochemistry of Bromine Addition: Bromination of trans-Cinnamic Acid Pitak Chuawong Objectives 1. To perform bromination of trans-‐cinnamic acid 2. To investigate stereochemistry of bromination reaction Introduction Alkenes undergo electrophilic addition to give alkyl halides. When bromine is used as a
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Raquel Johnson October 19‚ 2014 Solids: Recrystallization and Melting Points Organic Chemistry 2423 Lab Report: Recrystallization Abstract: The purpose of this lab was to purify an unknown compound by recrystallization. Taking an unknown compound and identifying it by purifying it from its impurities through the use of hot gravity filtration. Then to determine the unknown you were to take the melting point. An unknown compound was recrystallized from hot water to produce 0.99 grams (67% recovery)
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During the initiation and formation of the Grignard crushed magnesium was placed in a round bottomed flask with an iodine crystal with a bromobenzene solution with a stir bar. Once the stirring began‚ the solution turned brown and over time began to lighten up. The color change to brown indicated that the reaction began and this is why an iodine crystal was placed in the solution. The reaction started to boil due to its own reflux so heat didn’t need to be applied. Next the anhydrous ether solution
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The purpose of this lab was for students to familiarize and perfect the simple distillation method to produce 4-Methylcyclohexene and to gain experience using an IR spectroscopy to characterize the product of the reaction in favor of equilibrium. B. Results and Discussion: C. Experimental: 24 mL of 4-methylcyclohexanol‚ 5mL of phosphoric acid‚ and 1mL of concentrated sulfuric acid was added to a 250 mL round bottom flask and mixed thoroughly with a magnetic stirrer. A simple distillation
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solubility/miscibility behavior observed in procedure A-D. For part A of the procedure we worked with the solubility of solid compounds in various solvents. The three solid compounds that were worked with during this procedure were benzophenone‚ malonic acid‚ and biphenyl. These three solids were then mixed with water (highly polar)‚ methyl alcohol (intermediately polar)‚ and hexanes (nonpolar). When benzophenone is mixed with water the results turned out to be insoluble because benzophenone is a pure
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Taylor Durham Nutrition 101 Mr. Oropallo Lab Report #2: Fat Extraction From Food What is a triglyceride? Draw its structure. A molecule that contains three fatty acids attached at the oxygen atoms of glycerol. What are the differences between saturated and unsaturated fats? Drawn an example of each. If all bonds are single‚ the fatty acid molecule is saturated. If there is a double bond among the carbon atoms‚ the fatty acid molecule is unsaturated. What form does each of these fats take at
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Experiment 28: The reaction of Butanols with Hydrobromic Acid Pre-lab Objective: The objective of this experiment is to synthesize 1-bromobutane and 2-bromobutane with different catalyst:substrate ratios to determine which ratio is the most economically favorable. Discussion: In this experiment‚ 1-butanol or 2-butanol will be converted to the corresponding alkyl bromide with HBR‚ while using sulfuric acid as a catalyst. The sulfuric acid will accelerate the chemical reaction with being consumed
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Acid Determination of Vitamin C Tablets and Salt Solutions Chem 1290-016 03-05-2010 ------------------------------------------------- Purpose: The purpose of this lab was to use acid-base titrations to find the mass percent of ascorbic acid in a Vitamin C tablet. A known concentration of sodium hydroxide was used and the value found was compared to the stated amount of ascorbic acid listed on the vitamin container. Also in this lab the acidity of different salt solutions were tested using
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