Mona Vaidya 02/04/2014 CHE 317 Laboratory Experiment #1: Simple Distillation of Two Volatile Liquids Containing Non-Volatile Impurities Introduction: Simple distillation is a commonly used method to separate and purify the mixtures of organic liquids into their original components. Mixtures of two miscible liquids with two different boiling points were separated. Therefore‚ it can be said that the two organic compounds are separated by exploiting the different boiling temperatures of the liquids
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Distillation Purpose: To conduct the distillation process‚ simple or fractional. Procedure: 1. Add 5ml of 20% ethanol: water mix to the distillation flask. 2. Add 23 stir bar 3. Make sure that the thermometer bulb is just below the Claisen Head‚ carefully. Be very gentle with the thermometers and take care not to break them. 4. Label 3 vials‚ 1‚2‚ and 3. 5. Place receiving vial 1 on ice to collect the distillate 6. Start the distillation by piling up hot sand around the distillation flask with
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Comparing between the simple and fractional distillation‚ the fractional distillations for both n-propanol and acetone provided a better distillation. The data and graphs support the statement since the fractional graphs provided a steeper slope than the simple distillation. The steeper slope represent how fast the mixture are separated throughout the distillations. For example‚ the simple distillation for acetone the slope initially started at about 20 mL at about 65.5℃ and ended at about 30 mL
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Discussion: Extraction and crystallization- The purpose of this lab was to extract and crystallize compounds in a mixture using acids and bases. 1 gram of the unknown was dissolved into 30 mL of ethyl acetate. The mixture was then transferred to a separatory funnel. Using aqueous solutions of different pH we were able to separate organic acids‚ bases and neutral compounds from each other. Using three 10 mL portions of HCl‚ we reacted the HCl with the base in solution. This made it possible to
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Identity as “neutral spirits so distilled‚ or so treated after distillation with charcoal or other materials‚ as to be without distinctive character‚ aroma‚ taste‚ or color.” As Vodka is a neutral spirit‚ it means that it can be obtained by the distillation of any product with fermentable carbohydrates on it‚ like grains (rye‚ corn or wheat) or products like potatoes‚ beets or sugar beets; even grapes. Nowadays‚ most Vodka is obtained from grain. To get Vodka‚ a neutral spirit‚ (without the character
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Name: Leung Chun Wai Student no.: G20554292 Topic: (NT3048) Smoke extraction design for large space such as atrium 1. INTRODUCTION Atrium inside a building is an old architectural concept for about two thousand years. This concept has been developed and extended to modern buildings. Current trend of atrium design provides an ‘ideal’ external environment to the occupants with a large undivided space. The major problem for fires in atrium is hot and toxic gases accumulating and go down in the atrium
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DNA EXTRACTION In extracting chromatin from the cells of wheat germ there are seven steps to follow. The optimal cell to use would be the polyploidal eukaryotic. Eukaryotes have nucleus membrane-bound organelles‚ while prokaryotic does not. The polyploidal eukaryotic cell has DNA that is held in the nucleus while the prokaryote has DNA that floats freely around the cell. The DNA of eukaryotes is more complex and extensive than the other. Prokaryote is a bacterial cell that
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governed. An organisational structure is the process of arranging people and other resources to work together to accomplish a goal (Schermerhorn‚ 2011). However‚ what happens when there is no organisational structure? This is the theme of the “Valve Steams Ahead” case study in which this report is assessing. Using peer-reviewed sources and other research‚ an analysis will be made of Valve Software’s operations regarding their flat‚ unstructured organisational structure. This report will examine Valve’s
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Objective: To extract caffeine from tea powder using polar - nonpolar solvent extraction technique. Theory: The technique used to separate an organic compound from a mixture of compounds is called Extraction. Extraction process selectively dissolves one or more of the mixture compounds into a suitable solvent. The solution of these dissolved compounds is referred to as the Extract. Here the organic solvent dichloromethane is used to extract caffeine from an aqueous extract of tea leaves
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Much can be learned from studying an organisms DNA. The first step to doing this is extracting DNA from cells. In this experiment‚ you will isolate DNA from the cells of fruit. Materials (1) 10 mL Graduated Cylinder(2) 100 mL Beakers15 cm Cheesecloth1 Resealable Bag1 Rubber Band (Large. Contains latex pleasewear gloves when handling if you have a latex allergy).Standing Test TubeWooden Stir StickFresh‚ Soft Fruit (e.g.‚ Grapes‚ Strawberries‚ Banana‚ etc.) ScissorsDNA Extraction SolutionIce Cold EthanolYou
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