A. Title – Acid-Base Extraction with Separatory Funnel B. Introduction – The main objective of the experiment was the extract an acid‚ a base‚ and a neutral compound from a 2:1:1 compound of benzoic acid‚ p-nitroaniline‚ and azobenzene. In theory‚ an extraction technique based on phase distribution should allow two immiscible solvents to separate with a portion of the solute distributed into each. Using a separatory funnel‚ acids were extracted with bases (NaOH)‚ and bases were extracted
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Purpose This experiment deals with separating substances. The objective was to become familiar with the methods of separating substances from one another using decantation‚ extraction‚ sublimation techniques. Brief Introduction This experiment was set to teach research students different methods of separating substances from one another. Materials that are not uniform in composition are set to be impure or heterogeneous and are called mixtures. The separation of the components of mixtures is
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Extraction of Caffeine from Tea Leaves Santos‚ Raphael‚ Samson‚ Nonia Carla‚ *Tabora‚ Brylle‚ Tan‚ Kate Michal Department of Biological Sciences‚ University of Santo Tomas‚ Manila‚ Philippines Abstract Tea leaves are natural products that are harvested from agriculture. Caffeine‚ on the other hand‚ is a stimulant that has been shown to speed up the time of reaction‚ increase alertness‚ and improve one’s concentration. What we did in this experiment was to extract the alkaloid caffeine content
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Preparation of SKEO The extraction of S. khuzistanica was performed by hydro distillation and clevenger apparatus for 5 hours. Once extraction was completed‚ the resulted essential oil was dehydrated using sodium sulfate (Merck). The essential oil was stored at temperature of 4ºC until using (12). In order to provide different concentrations of the extract‚ Dimethyl sulfoxide (DMSO) was used. Gas chromatography/mass spectrometry analysis of essential oil Isolation and measurement of the sample
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The central message of this advertisement is if you want to be strong like Popeye‚ eat their spinach. I can recall waking up Saturday morning watching the cartoon Popeye as a child. Popeye was always trying to impress Olive Oil. Popeye wasn’t the only one with eyes for Olive Oil‚ his nemesis‚ Pluto also had a very hostile interest towards Olive Oil as well. The cartoon would start out with Popeye planning something nice for Olive Oil‚ the day would be going perfectly. Pluto would notice Olive
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As the assistant to Michael Brune‚ the executive director of the Sierra Club‚ I am in full support of The Exploratory Fracking and Extraction act. I would like to express concerns associated with hydraulic fracturing‚ or fracking‚ on behalf of the Sierra Club. Critical problems that are commonly brought to attention are: contamination of water supplies‚ seismic activity caused by fracking‚ and it worsens the current condition of the climate. Fracking wells inject water‚ sand‚ and chemicals deep
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microfuge tube. Place this tube directly into liquid N2 to freeze plant tissue. 2) Remove tubes from the liquid N2 and quickly grind the plant tissue with a pestle. Add 300 L of Methanol 1%HCl and continue to grind the plant tissue. Allow extraction to occur overnight in a dark refrigerator. 3) Add 200 L Milli-Q H20 to each tube. Next‚ go to the fume hood and add 500 L of chloroform to each tube. Spin the tubes in a centrifuge set at the highest rpm for 2-5 minutes. 4) Return to
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Experiment 3: Isolation of Chlorophyll from Spinach and Chromatography Performed February 14th and 16th By Kyle Herzog Organic Chemistry 344 Section 807 Spring 2012 Objective: The purpose of the experiment is to extract pigments from spinach leaves and separate them by column and thin layer chromatography‚ determining Rf values for the pigments. Equations: Rf= Distance travelled by a given compound/Distance travelled by a solvent solution 1. Crude- 4.25/5.5= 0.773 2. Carotene-
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There has been much debate in recent years among politicians‚ military officials‚ and civilians on whether or not the U.S. should be fully withdrawn from Afghanistan‚ regardless of the country’s economic and military capabilities. There has also been a proposed timetable‚ which President Obama says is in effect and currently being executed‚ to have up to ninety percent of our military personnel out of the country by no later than 2014. It is imperative that we extract our forces out of Afghanistan
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Extraction of Caffeine from Tealeaves Perez‚ Albert Solomon K.*; Quiambao‚ Marie Angela C;.Pascua‚ Hanna Harriette R.; Patricio‚ Maria Roxanne DC.; 2-Chemistry‚ Department of Chemistry‚ College of Science University of Santo Tomas España St.‚ 1015‚ Manila Abstract Caffeine is soluble in both water and organic solvents‚ solid-liquid extraction and liquid-liquid extraction were used in the experimentation process. Caffeine was extracted using hot water‚ however‚ due to its
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