Every step in this experiment has reasons behind its application. One determines the masses of the crucible and barium chloride hydrate for obvious data collection and calculation purposed. The heating of the sample slowly for 10 minutes is done to remove the water from the sample. A constant mass for the sample must be obtained so therefore it must be done slowly because if not you may loose mass from the sample. At the point where the crystalline solid changes to a powdery solid the sample must
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ISE: The Determination of Chloride Unknown: #34 I. Purpose: In experiment V‚ “ISE: The Determination of Chloride”‚ the concentration of an Unknown Chloride solution‚ and the Wt% of NaCl in a sample of celery salt‚ were both determined. To determine the concentration of an Unknown Chloride solution‚ a Calibration plot is first prepared. The Calibration plot is made by first measuring a series of known concentrations of Cl- (with the same activity of the unknown solution) and obtaining
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Introduction This lab proposed the question of what happens when copper chloride and iron are combined and what is the balanced equation.By completing this lab‚ the goal was to determine the equation and product for the reaction of iron (Fe) and copper chloride (CuCl2). It was predicted either solid iron or solid copper would form. Methods To begin‚ 6.00026 grams of copper chloride was dissolved in 50ml of distilled water in order to have a solution with charged iron and chlorine atoms. Then‚ 6
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well as the density was calculated. The same process was performed to calculate the density of an unknown substance. The third part Section C 5-25% of sodium chloride was prepared by the instructor. For each percent concentration of sodium chloride a 25 mL was prepared. Weighing the graduated cylinder before and after the sodium chloride was transferred the density were calculation. Pre- Laboratory Questions: 1. A metal sphere weighing 15.45 g is added to 21.27 mL of water in a graduated cylinder
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Purity of Aspirin Objectives - To research‚ using various sources‚ the history of aspirin‚ its use in medicine‚ methods of synthesizing it and of measuring its purity - To compare the % purity of a branded aspirin tablet with a generic aspirin tablet - To compare 2 methods of composition analysis of the two types of aspirin Research
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Abstract The chloride present in an unknown soluble sample was precipitated into silver chloride through precipitation gravimetry. The colloidal silver chloride originally formed was converted to a crystalline solid by controlling certain parameters of the experiment such as temperature‚ pH of the solution‚ and concentration of AgNO3. Once the solid was large enough‚ it could be washed‚ filtered‚ and weighed. The percentage of chloride present was found to be 24.73695223 (±0.00000006) %.
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Gravimetric Analysis of a Chloride Salt CHEM 1001 Purpose: To illustrate typical techniques used in gravimetric analysis by determining quantitatively the chloride content in an unknown soluble salt. Theory: AgCl(s) is a very insoluble solid‚ yet still does have some solubility. Because of these traits‚ the following reaction is able to occur: Ag+(aq) + Cl−(aq) → AgCl(s) . This reaction is able to occur in both directions. When a soluble silver salt such as AgNO3 is added to a solution containing
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PREPARATION OF ASPIRIN AND DETERMINATION OF THE MELTING POINT Ferrer‚ Lara Melissa V. Faculty of Engineering University of Santo Tomas Manila‚ Philippines ABSTRACT This experiment involved three steps: synthesis of aspirin‚ isolation and purification‚ and the estimation of purity of the final product. The synthesis involved the reaction of salicylic acid and acetic anhydride in the presence of a catalyst‚ phosphoric acid‚ H3PO4. When the aspirin was prepared‚ it was isolated and filtered. The percentage
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The crude product (aspirin) was purified in the last lab‚ using recrystallization‚ in which we dissolved the crude product with hot ethanol. We then added 25 mL of water until the product reformed (the solution became cloudy white) and redissolved the solid with hot ethanol. The solution was allowed to cool for a week‚ and crystals of purified solid were formed. In order to analyze this purified product‚ we determined the melting point by placing a small sample of the aspirin in a capillary tube
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“The Synthesis of Zinc Chloride”‚ what a peculiar name for a lab that does not even involve synthesis. Synthesis‚ by definition‚ is when two elements are combined in a chemical reaction‚but that is not the case. In this lab we are combining zinc‚ an element‚ and hydrochloric acid‚ a compound‚ but combining a compound and an element is not synthesis‚ it is single replacement. We are taking zinc and hydrochloric acid and making zinc chloride and hydrogen‚ a single replacement‚ but what occurred during
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