PREPARATION OF BIODIESEL FROM WASTE COOKING OIL In partial fulfillment of the requirements for the award of the degree of Bachelor of Engineering in Mechanical Engineering Submitted by Ritesh Shukla Pankaj Singh Bais Ciby Ninan Ankush Deshmukh Under the guidance of Prof. SUSHANT S. SATPUTALEY (Assistant Professor of Mechanical Engineering) Academic Year 2010-11 Department of Mechanical Engineering ST. VINCENT
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Chris CXXXX Organic Chemistry Lab Dr. Lyn XXXX 2 February 2012 Esterification of Isopentyl Alcohol to Isopentyl Acetate Procedure The technique for esterification that was employed in the experiment was to use a reflux apparatus (Figure 1) while heating in order to evaporate out water to drive our reaction into the product favored direction. The starting material of isopentyl alcohol (1.0 mL) and excess glacial acetic acid(1.5 mL‚ 17.6M) were eppendorf pipetted into a 5 mL conical vile. This
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(1977) Agbalumo pectin; Extraction and Properties 21. Institute of food Technology (I.F.T). (1959) Pectin standardization: Final Report of the I.F.T Committee‚ J 22. Speiser‚ R. and Eddy‚ C.R (1946) Effect of Molecular weight and Method of de-esterification on the gelling 23. Hills C.H Moltern‚ H.H Nutting‚ G.C and Speiser‚ R (1949)
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CH 223 - Organic Chemistry Laboratory I Experiment #6 - Column and Thin-Layer Chromatography (TLC) of a Spinach Extract Pre-Lab Assignment (1) List 5 ways that TLC can be used in an organic chemistry lab experiment. To identify an unknown‚ to monitor the course of a reaction and assess the purity of its product‚ to determine the best solvent for a column chromatography separation‚ to determine the somposition of each fraction from a column chromatography separation‚ and to determine whether
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HOW TO GET A HACK LICENSE Driving an NYC Yellow cab is an excellent way to earn money. At the end of every shift‚ even when a fare pays with a credit card - you go home with cash in your hand! Getting your NYC TLC yellow cab licenses is not difficult. From start to finish‚ there are five procedures that average one month to complete and $500 in fees. If you are ambitious‚ the five steps can be completed with in a two week time period. If you are a full-time university student‚ willing
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Micro-extraction of urine and/or stomach contents and analysis by TLC Abstract Thin Layer Chromatography (TLC) is one of the oldest chromatographic techniques used for the identification of compounds and for determination of the presence of trace impurities. The aim of the experiment was to determine two unknown samples (X and Y) by comparing results to the known standard drugs‚ of which there was five‚ using a specific TLC method. The same technique was used for the determination of
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Thin-layer Chromatogragaphy : Analysis of Drug Components CHEM221 Date experiment performed : January 20‚ 2014Date Submitted : January 27‚ 2014 Introduction This laboratory has its first objective to familiarize with the thin layer chromatography (TLC) technique. Second‚ each student has to identify the unknown components by comparing it to one of the tree dissolved liquid analgesics: Acetaminophen‚ Aspirin and Caffeine. Finally‚ calculating the Rf value by measuring the mobile and stationary phase
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The progress of the reaction was monitored in my case using two TLC plate. It first started off with the spotting of Standard benzoin and benzil which were provided in the lab and followed by the addition of the reaction mixture at once it starts changing colour/boiling‚ then at 10 and 20 mins into the reflux. Once all the necessary steps were spotted‚ the TLC plate was placed in in a beaker containing CH₂Cl₂(methylene chloride)‚ which was used as the developing solvent in this experiment. To check
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Chromatography – Analyzing Analgesics by TLC and Isolation of β-Carotene by Column Chromatography Introduction/Background: Flavonoids are an important group of additives that can be defined as pure substances either natural‚ extracted from raw materials or synthetic. Chromatography is the separation of two or more compounds or ions caused by their molecular interactions with two phases – one moving and one stationary (Weldegirma 2012). Three types of chromatography are used
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eluate were collected‚ this process is the column chromatography (CC). The purity of the components was determined by using the thin layer chromatography (TLC). Ultraviolet spectroscopy and iodine staining were used to visualize the developed TLC plate and the Retention Factor was measured. Keywords: Chromatography‚ column chromatography‚ TLC and visualizing agent‚ elution‚ capsicum frutescens Introduction Chromatography can be defined as the separation of a mixture‚ in which the mixture is
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