Grignard Synthesis of Tirphenylmethanol David Szuminsky Organic Chemistry Lab II Shaopeng Zhang Monday 1PM 2/10/14 & 2/24/14 - Abstract A sample of triphenylmethanol was prepared using Grignard synthesis techniques. Reflux was used in order to speed up the reaction and the final product was purified using recrystallization methods. The percent recovery and percent yield were 80.46% and 47.526%‚ respectively. A melting point range of 85-87oC was obtained from
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Identifying Organic Compounds Joe Harris 11/12/07 1. Background Organic compounds are‚ by definition‚ any chemical compound containing carbon. These compounds include carbohydrates‚ polysaccharides‚ lipids‚ proteins‚ and nucleic acids. Each one of these compounds has a different purpose. Carbohydrates give energy to cells when consumed. Lipids are basically the
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Introduction The purpose of this lab is to determine which pigments in a plant support or effect photosynthesis‚ based on starch production‚ which wavelengths of light are involved in photosynthesis‚ and identify plant pigments found in a plant leaf by means of paper chromatography. Life on Earth is dependent entirely on the energy from the Sun‚ not only to keep the planet at a suitable temperature but also to provide the energy required to sustain life. The energy of the Sun‚ in the form of
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Who Took Jerell’s iPod? Lab Purpose: Standardized Tests The purpose of testing the organic nutrients (vegetable oil‚ glucose‚ starch‚ powdered egg white) with each of the different indicators (brown paper towel‚ benedicts‚ iodine‚ biurets) was to determine the color it would turn with positive traces of the nutrient. The purpose of testing just the Distilled H2O was to determine the color it would turn with negative traces. Nutrient in the Different Foods The purpose of testing each of the
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Analysis – Synthesising Aspirin results After recrystallisation differences between the crude and purified aspirin were noted. The impure (crude) aspirin was powered and fluffy with small clumps and was slightly yellow in colour whereas the pure aspirin has a less fluffy crystalline powder and was whiter. This showed distinct differences in the two substances but similarities were also apparent showing aspirin‚ in some level‚ was created. Before recrystallisation the crude aspirin could of included
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Lab #4 The Synthesis of Organic Polymers CHM2123‚ Section C October 21‚ 2014 Introduction: Organic polymers are macromolecules that are composed of smaller molecules called monomers. There are two main groups of polymers: natural polymers and unnatural (synthetic) polymers. Natural polymers include proteins such as cellulose and starch and are a necessity for our existence. On the other hand‚ synthetic polymers such as the polycarbonate in our lab goggles
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TENS 2146 Electric Devices and Measurements Lab 3 Current and Voltage This report was prepared by: L. Wall Fall 2009 Prof. R. Alba-Flores Team Members: J. White‚ L. Wall Conducted on: September 17‚ 2009 Submitted on : September 24‚ 2009 Abstract: In this lab students experimented with light emitting diodes. The student built a basic circuit with two LED’s and resistors in parallel. The results showed that the voltage is the same in parallel. The items that were in series had the
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BCH3015 Organic Chemistry Name: Chun Ka Yuen (52180145) Group: C Date of experiment: 30/3/2012 Date of report: 3/4/2012 Experiment 5: Polymers Aim: This experiment is to prepare polymeric materials including polystyrene‚ Nylon6‚ 10‚ and cellulose triacetate. Introduction: A polymer consists of repeating subunits in the form of –A-A-A-A-A- or A-B-A-B-A-B-‚ where A and B are different subunits. These sub-units are typically connected
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Lab Report #1 Title: Synthesis of Divanillin Abstract: The purpose of this experiment was to synthesize divanillin. This was done via the oxidative dimerization of two equivalents of vanillin‚ using enzyme horseradish peroxidase as the catalyst. Procedure: Lab Handout: Nishimura‚ R.T.; Giammanco‚ C.H.; Vosburg‚ D.A. J. Chem Educ. 2010‚ 87‚ 526-527. Discussion: Mechanism: Reaction 2 Vanillin H2O2 Divanillin 2 H2O
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Safety Precautions for Synthesis of Acetic Anhydride Acetic Anhydride Acetic anhydride is an irritant and also flammable‚ therefore gloves and goggles should be worn at all times during the experiment. It is reactive to water‚ so in the case of fire‚ alcohol foam or carbon dioxide is preferred to use as an extinguisher. This chemical has harmful fumes and use of a fume hood is strongly recommended. Sulphuric and Salicylic Acid These acids may irritate the skin in high concentrations. Take
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