Synthesis of Benzoin Date of Experiment: 1-26-15 Chelsea Price Lab Partner: Joey Simmons Abstract: In this experiment‚ benzoin was synthesized from benzaldehyde‚ using thiamine hydrochloric acid as a catalyst. The thiamine HCl was deprotonated by sodium hydroxide and acted as a nucleophile to attack the benzaldehyde. A water-cooled condenser was used to heat the solution at reflux. Vacuum filtration was used to wash and dry the product. The benzoin product was recrystallized
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Cited: Aguilar‚ Andrea. "Synthesis of Aspirin Part B."CourseHero. N.p.. Web. 7 Mar 2014. . "aspirin." PubChem. National Center for Biotechnology Information. Web. 7 Mar 2014.
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Materials & Methods Synthesis Procedure of PDA@MT Polydopamine is synthesized through covalent polymerization similar to melanin biosynthesis‚ with DA oxidized to dopamine quinone‚ then further oxidized to DHI‚ which undergoes deprotonation and cross-linking via Michael addition to form PDA. A solution was prepared to synthesize PDA by mixing 90 mL of water‚ 40 mL of ethanol‚ and 3 mL of ammonia solution in a 300 mL beaker. After stirring for 30 minutes at 37°C‚ a solution of 500 mg of DA dissolved
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1. What is the more formal chemical name for aspirin? Acetylsalicylic acid 2. Using your data from Experiment 2‚ how can you be sure you synthesized aspirin? By using the colors as a guide‚ we can compare the Acetylsalicylic acid + 8 mL FeCl3 to the Aspirin Crystals from Experiment 1 + 8 mL FeCl3 in order to see if it synthesized. 3. Would you say that your synthesized aspirin is relatively pure? How can you tell? One way that the purity of aspirin can be judged is by it’s color as pure
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School December 13‚ 2011 Formal Lab Report Introduction: This lab addresses how people’s metabolism directly affects their performance when faced with a situation that involves exercise for one‚ and two minutes. Using and understanding Cellular Respiration is something you will need to learn before you can fully grasp this Formal (Lee‚ Susan. Bio Home. N.p.‚ 15 Feb. 2005. Web. 9 Dec. 2011. <http://biology.clc.uc.edu/courses/bio104/cellresp.htm>.) Lab Report. First of all‚ you will need
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Angelina Mass-Valderrama CHM1032 summer ‘12 Graphing and Estimating Formal Lab Report Introduction: Today scientists put acquired data into a form of a graph. This said graph is designed to help make predictions and furthermore‚ study and understand the experiment and its contents at hand. The Graphing and Estimating lab involves just that. The lab is designed to collect data from several tests involving burn time of a candle. Oxygen‚ O2‚ is a kind of gas. A lot of the air we breathe
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Experiment 23: Synthesis of an Alkene April 5‚ 2013 Purpose: Results and Discussion The weight of our n-Butyl Bromide sample (actual yield) was 0.09g. The percent yield was found to be 4.38%. Only 0.09g of the theoretical 2.055g yield was obtained. The boiling point was 104° C‚ which is higher than the literature value of 101° C. This is due to the sample being somewhat impure‚ as impurities tend to increase boiling point. When IR spectroscopy was performed‚ there were no OH stretches
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Spectrophotometric Determination of Equilibrium Formal Report Matt DeLuca The Department of Chemistry‚ SUNY College at Brockport Brockport‚ NY 14420 CHM 206.04 Abstract: The main objective of this experiment was incorporating the use of spectrophotometry in an attempt to study the position of equilibrium. Furthermore‚ after the completion of this experiment‚ the formation of the equilibrium constant of the iron thiocyanate complex
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shows a reaction with a primary alcohol. Usually primary alcohols form primary carbocation. However‚ primary carbocations are too unstable to form as intermediates‚ so they can undergo a rearrangement or E2 mechanism. A rearrangement occurs when an alkyl group or a hydrogen on the neighboring carbon of the carbocation shift to delocalize the positive charge to result in a more stable carbocation. A rearrangement almost always occurs whenever a carbocation can form a more stable molecule. An E2 mechanism
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High Performance Liquid Chromatography Analysis of Aspirin Problem: Was aspirin (acetylsalicylic acid) successfully synthesized? Are there impurities or by-products present in the synthesized aspirin? How pure is the synthesized aspirin? Introduction: In the last experiment‚ aspirin was synthesized followed by characterization of the product using several different techniques. Melting point was a test that provided information about the identity and purity of the aspirin product. The iron(III)chloride
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