Steam Distillation Purpose: To use steam distillation to purify heat sensitive‚ natural products‚ like essential oils. Procedure Please refer to: Williamson‚ Macroscale &Microscale Organic Experiments 4th Ed.‚ pgs.98-109 Results Table 1.1: Steam distillation Drop # (every third drop) Temperature (ºC) Addition of 0.5 mL water 1 100.3 Water added 2 100.5 3 100.5 Water added 4 100.6 Water added 5 100.6 6 100.6 Water added 7 100.6 8 100.6 Water added 9 100.3 10 100.6
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Cheryl Baclit Chem 234 Experiment 4: Steam Distillation Introduction The purpose of this experiment is to extract Eugenol from Cloves using steam distillation as a purification technique and to transfer Eugenol from the aqueous phase to the MeCl2 phase. With steam distillation‚ the boiling point of a mixture of immiscible liquids is lower than the boiling points of the individual components. Water from the steam is one of the components of an immiscible liquid mixture. The vapor pressures of
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All about Distillation Distillation is a process that is used to purify a lot of substances on a domestic as well as commercial basis. It is very interesting to know about the process in detail as it is a natural process. The story begins when a liquid or solid state of mater responds to the heat in environment. The heat makes the liquid state or solid state of matter to convert into gas state. Liquid Gas (Vaporization) Solids
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Loreta Grazhees TA: Titas Friday 11:50 - 3:55 February 9‚ 2018 Nitration Of Toluene When reacting Toluene with (NO2+) the end goal is to generate an ortho-‚ para-‚ and/or meta-nitrotoluene. This lab will help guide you in the direction to predict the regioselectivity and activation vs. deactivating powers of the nitro-group. Gas Chromatography will be used to analyze compounds that can be vaporized without being decomposed. GC is also used to check the purity of a substance‚ and separating the
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In experiment 5‚ distillation method was used to divide hexane and toluene from a mixture (50:50) of hexane and toluene. Hexane was separated from toluene and was observed from the gas chromatography‚ it showed that hexane increased from 0.0.873 to 0.886 moles. Once the mixture of toluene and hexane hit 70 degrees in the experiment‚ the distillate was used for the gas chromatography. Hexane was higher in the distillate stage. The first drop of condensation appeared at 79°C. The volume of the distillate
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8.2.1 (iv) Fractional Distillation of Crude Oil By Blake Turner – Year 11 Fractional Distillation of Crude Oil Introduction Crude oil is the term for "unprocessed" oil‚ the stuff that comes out of the ground. It is also known as petroleum. Crude oil is a fossil fuel‚ meaning that it was made naturally from decaying plants and animals living in ancient seas millions of years ago -- most places you can find crude oil were once sea beds. Crude oils vary in colour‚ from clear to tar-black‚
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EXECUTIVE SUMMARY: The main objective of this project was to carry out a design on the Propane distillation column for a process that produces 1‚3 Butadiene. The raw materials used are Butane‚ Oxygen and Water and the process capacity is 100 000 tonnes per annum nominal. In the previous work it was stated that the plant is located in China. The main location of the plant is in the capital city of the Gansu Provence‚ Lanzhou. This was decided as the location over other provinces due to the excellent
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plants. In this experiment‚ the essential oil eugenol was isolated from ground cloves using steam distillation techniques. Eugenol had a high boiling point‚ but it was isolated at a lower temperature by performing a co-distillation with water‚ a process known as steam distillation. This technique allowed the desired material to be distilled at a lower temperature than 100℃. The point of the steam distillation was to use an azeotrope to isolate the organic compound from a solid. The azeotrope was the
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The Extraction of Bio-ethanol from Apple (Malus domesticus) and Banana (Musa accuminata Colla) Peelings through the Process of Fermentation and Distillation Abstract Apple (Malus domesticus) and banana (Musa accuminata Colla) peelings are common household waste products. This study sought to extract bioethanol from these two peelings and to compare which sample can produce more bioethanol. About 400 grams of apple and banana peeling was obtained from the 1 kilogram bought from the supermarket
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Distillation Alcoholic distillation is basically the process of separation the more volatile component‚ alcohol‚ from the less volatile component‚ water‚ from a water/alcohol solution‚ by heating the solution and condensing and collecting the alcohol rich vapours released‚ as a high alcohol strength liquid (spirit). The starting material for most distillations‚ such as wine for brandy and beer for whisky‚ are usually weak alcoholic solutions (5%-7% v/v ethanol) This seems counter intuitive
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