purpose of this experiment was to isolate the aromatic hydroxyl compound‚ eugenol from crushed cloves using steam distillation. After conducting the distillation‚ the expected two layers were not visible in the centrifuge tube. Subsequently‚ the extraction and evaporation did not produce the expected oil. This result is probably due to the collection of only water vapor during distillation. From another group’s data‚ 3.80% of the oil was recovered from the cloves in which the major component is eugenol
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eugenol in the basic aqueous layer‚ and acetyleugenol in the organic layer. The basic aqueous layer can be acidified to re-extract eugenol from it. And the organic layer can be dried and concentrated to yield acetyleugenol The principle of steam distillation is based on the fact that two immiscible liquids will boil at a lower temperature than the boiling points of either pure component‚ because the total vapor pressure of the heterogeneous mixture is simply the sum of the vapor pressures of the individual
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Results | 9-11 | 6) Discussion | 12 | 7) Conclusion | 13-14 | 8) References | 15 | ABSTRACT This experiment is about steam distillation by using Dalton’s Law. The objectives of this experiment are to demonstrate a separation of a mixture by using steam distillation and next to prove that Dalton’ Law and ideal gas law are applicable in steam distillation. Dalton’s Law; While Ideal Gas Law; This experiment is conducted by placing 2mL of Turpentine and 15mL of water into
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Distillation of Alcoholic Beverages Pamela Mallari*‚ Symon Manuel‚ Katherine Merene and Charlene Mondelo Department of Chemistry‚ University of Santo Tomas‚ Manila‚ Philippines Abstract Distillation is a physical process used to separate chemicals from a mixture by the difference in how easily they vaporize. This experiment aims to (1) compare the efficiency of simple and fractional distillation‚ (2) distill and calculate the % of ethanol and (3) determine the % loss in distillation. Two
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therefore then allowing toluene particles to separate in the later fractions when temperature is over 105 degrees Celsius. Lastly‚ it is concluded that fractional distillation is a more effective method as opposed to simple distillation because in fraction 7 of the simple‚ there was only around 36% toluene consumption versus a 96% in the fractional distillation. This is also due to the fact that using a fractionating column makes the samples more pure because it works better at separating the first couple
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Comparing between the simple and fractional distillation‚ the fractional distillations for both n-propanol and acetone provided a better distillation. The data and graphs support the statement since the fractional graphs provided a steeper slope than the simple distillation. The steeper slope represent how fast the mixture are separated throughout the distillations. For example‚ the simple distillation for acetone the slope initially started at about 20 mL at about 65.5℃ and ended at about 30 mL
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Distillation of Alcohol Beverages Abstract Distillation is a process wherein a liquid is heated until its boiling point while the resultant hot vapors are subsequently captured and cooled‚ and the condensed vapors are collected. Among the many types of distillations‚ the fractional method or technique of distillation was used in this experiment. A step by step procedure was followed and an amount of 3.33 % of ethanol was obtained from the sample wine‚ Mateus Rose‚ which was used. Further
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Municipal Solid Waste Andrew McClarren Final Project Outline EGEE 439 April 12‚ 2015 Introduction Through the years‚ especially in the most recent few decades‚ the use and creation of biomass has been under study and practice as to maximize how much it can benefit society as well as the planet as a whole. Biomasses are being used around the world for a magnitude of purposes. So what exactly is a biomass and what can they be used for? Biomasses are any materials and matters derived from
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Name of the Experiment: Simple Distillation (Semimicroscale Procedure.) Abstract: Distillation is a method of process of separating 1:1 mixture based on differences in their volatilities in a boiling liquid mixture. Distillation is done with the use of simple distillation apparatus shown in Figure 1. In this experiment‚ simple distillation process was used to determine the identities of the unknown compounds in the solution through the obtained boiling points. The list of probable unknown volatile
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Steam Distillation Purpose: To use steam distillation to purify heat sensitive‚ natural products‚ like essential oils. Procedure Please refer to: Williamson‚ Macroscale &Microscale Organic Experiments 4th Ed.‚ pgs.98-109 Results Table 1.1: Steam distillation Drop # (every third drop) Temperature (ºC) Addition of 0.5 mL water 1 100.3 Water added 2 100.5 3 100.5 Water added 4 100.6 Water added 5 100.6 6 100.6 Water added 7 100.6 8 100.6 Water added 9 100.3 10 100.6
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