Acetylsalicylic Acid (Aspirin) Synthesis Telow‚ AJV Sumicad‚ CJ‚ Tavanlar‚ EMMT‚ Chem 40.1‚ Institute of Chemistry‚ University of the Philippines Los Baños I. Introduction Organic synthesis is the process where a desired organic compound is constructed or prepared from commercially available materials. The objective of organic synthesis is to design the simplest synthetic routes to a molecule. Aspirin‚ also known as acetylsalicylic acid is as salicylate drug often used as analgesic
Free Aspirin Acetic acid Carboxylic acid
Stereochemistry of Butenedioic Acid Objective: To study the interconversion of two geometric isomers‚ maleic acid (cis isomer) to fumaric acid (trans isomers)‚ the differences in physical properties between this pair of cis-trans isomers and determine the stereochemistry of addition of bromine to butenedioic acid. Chemicals and Apparatus: 2 grams of maleic acid‚ 10 cm3 of concentrated hydrochloric acid‚ 10 cm3 of bromine water[1]‚ one 50 cm3 beaker‚ one 100 cm3 beaker‚ one 250 cm3
Premium Carboxylic acid Hydrogen Chemistry
The unknown carboxylic acid’s melting point was 108°C according to the Mel-Temp machine. The melting point is the temperature at which a solid precipitate changes into its liquid form upon heating. The melting point of benzoic acid‚ the aromatic carboxylic acid was 122°C. Thus‚ the product contained impurities which caused the solid to melt at a lower temperature than the actual temperature. Pure solids typically melt at higher temperatures while impure solids melt at lower temperatures. This is
Premium Temperature Water Liquid
AMINO ACIDS BY MEANS OF TITRATION CURVE ABSTRACT The aim of the experiment was to identify an unknown amino acid through acid-base titrations which was prepared in water to form an acidic solution. Each group prepared unknown amino acid hydrochloride. The pre-prepared basic solution was slowly added to the amino acid solution and pH change was closely observed using the pH meter. During these titrations the amino acid converted from cation to zwitterion to anion; zwitterion is an amino acid with
Premium Amino acid PH Acid
Recrystallization of Benzoic Acid Objective To purify benzoic acid by recrystallization and gain experience with a basic organic laboratory techniques. Background Products of chemical reactions are often contaminated with impurities. One method for purifying chemicals‚ recrystallization‚ takes advantage of the differences in the solubilities of the desired products and the impurities and the tendency for the slow formation of crystals to exclude impurities from the crystalline solid. HC HC
Premium Crystal Chemistry Solid
steps of the citric acid cycle. Differentiate between citric acid cycle and glyoxylate cycle. Relate citric acid cycle as energy source. The Central Role of the Citric Acid Cycle 3 processes play central roles in aerobic metabolism. The citric acid cycle. Electron transport . Oxidative phosphorylation. Metabolism consists of: Catabolism: the oxidative breakdown of nutrients. Anabolism: the reductive synthesis of biomolecules. • The citric acid cycle is amphibolic
Premium Citric acid cycle Metabolism
multi-step purification of benzoic acid after performing the extraction from a mixture containing benzoic acid‚ cellulose‚ and methyl orange. Recrystallization was done to remove impurities from the sample. The amount of BA recovered during recrystallization is much less than the extracted amount of BA. The difference between the pure and impure samples was observed by comparison of melting points. It was found that impure samples will have a lower and wider melting point range. The experiment performed
Premium Solubility Chemistry Temperature
Lewis Acids and BasesLewis acids and bases play an important role in chemical reactions because‚ except oxidation-reduction reactions‚ almost every reaction could be categorized as an acid-base reaction. Bases in water solutions show certain specific characteristics: bitter taste‚ feel slippery‚ and turn litmus paper blue. Acids in water solutions show these most common characteristics: sour taste‚ react with metals‚ and turn litmus paper red. The understanding of chemical reactions‚ such as acid
Premium Hydrogen PH Base
Title: Estimation of Ascorbic acid Aim: To determine the ascorbic acid content of canned apple and orange juice To determine the volume of canned juice necessary to provide 75mg of Vitamin C Introduction: For the estimation of ascorbic acid‚ the method used involved the titration of the ascorbic acid‚ in the presence of a redox indicator 2‚6-dichlorophenol-indophenol (DCPIP) which acts as both an oxidant so as to oxidise the ascorbic acid to dehydroascorbic acid‚ and it acts as an indicator
Premium Vitamin C Ascorbic acid Vinegar
The Depression Anxiety and Stress Scale (DASS): The study of Validity and Reliability Ahmet AKIN* Bayram ÇET‹N** Abstract This study investigated the validity and reliability of the Turkish version of the Depression Anxiety Stress Scale (DASS). The sample of the study consisted of 590 university students‚ 121 English teachers and 136 emotionally disturbed individuals who sought treatment in various clinics and counseling centers. Factor loadings of the scale ranged from .39 to .88. Findings
Premium Psychometrics Factor analysis Reliability