8: Synthesis of Adipic Acid Performed November 8th & 10th By Jennifer Seitz Organic Chemistry 344 Section 803 Fall 2011 Objective: The purpose of this experiment was to synthesize adipic acid from cyclohexanol via an oxidation reaction that was catalyzed by sulfuric acid. Purity of the product was assessed by measuring the melting point. Physical Properties/Structures: Name | Formula | Molecular Weight (g/mol) | Boiling Point (0C) | Melting Point(0C) | Density(g/mL) | Hazards
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Acetic acid (glacial) 100% suitable for use as excipient EMPROVE® exp Ph Eur‚BP‚JP‚USP‚E 260 For general questions please contact our Customer Service: Merck KGaA Frankfurter Str. 250 64293 Darmstadt Germany Phone: +49 6151 72-0 Fax: +49 6151 72 2000 01 March 2014 Product number Packaging Qty/Pk 1000562500 Glass bottle 2.5 l 1000569025 Plastic container 25 l 1000569190 Plastic barrel 190 l Accessories 101595 Chemizorb® H+ Absorbent and neutralizer for spilled acids‚ with indicator
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The acid-base titration curves help to find the pKa‚ Ka‚ and pH at equivalent point. At the beginning pH for HCl is 1.90 which is lower than the 3.28 for acetic acid; thus‚ strong acid (HCl) means lower pH and weak acid (acetic acid) means higher pH. Then at the equivalent point for the titration HCl-NaOH the pH is 7‚ which mans that is neutral‚ in other words there are enough NaOH mmol to neutralize the HCl mmol present; also‚ the solution contains only water and NaCl the salt derived from the titration
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DETERMINATION OF FRUIT ACIDS BY TITRATION AND CALCULATION OF THE SUGAR/ACID RATIO It is the sugar/acid ratio which contributes towards giving many fruits their characteristic flavour and so is an indicator of commercial and organoleptic ripeness. At the beginning of the ripening process the sugar/acid ratio is low‚ because of low sugar content and high fruit acid content‚ this makes the fruit taste sour. During the ripening process the fruit acids are degraded‚ the sugar content increases and
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Synthesis of benzilic acid from benzoin utilizing a multi-step reaction. Names: Arian Karim TA Name: Sayantan Das Lab Day & Time: Thursday 7:30-11:40 Lab Section #: Abstract The main purpose of this experiment was to synthesize benzilic acid from benzoin. This requires a multistep synthesis with benzyl as an intermediate product. The first step required HNO3 as an oxidizing agent and the second step required KOH and HCl. The percentage yields of benzil and benzilic acid were 59.5% and 21
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October 9‚ 2013 Partner(s): Acetylsalicylic Acid Synthesis Theory. This experiment was carried out to see how the hydroxyl group on the benzene ring in salicylic acid reacts with acetic anhydride to form an ester‚ and to make aspirin. Synthesis of Acetylsalicylic Acid occurs by protonation of carbonyl (C=O) group‚ and a nucleophilic attack of OH on the acetic anhydride. The ferric chloride test and melting point were used to test the purity of the results. A hypothesized recovery rater of above
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Depression and Anxiety Sarah Gartin COM/155 March 17‚ 2013 Tressa Cook Gray [APA style looks good!] Depression and Anxiety Depression and anxiety are two common disorders that many Americans deal with day in and day out. So‚ individual Americans may ask‚ are we anxious‚ or are we depressed? Anxiety and depression are thought of as two distinct disorders. However‚ in this world‚ many people suffer from both conditions. Knowing the similarities‚ differences‚ treatments‚ and prevention/reduction
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Crystallization of Benzoic Acid Purpose: The purpose of this experiment is to purify benzoic acid by crystallization. Procedure: 1. 0.5g impure benzoic acid was placed in a 50mL Erlenmeyer flask. 15mL of water was added and the mixture was heated to a boil on a hot plate. 0.5mL of water was added to the flask‚ while swirling the flask. The mixture was boiled until the benzoic acid completely dissolved. The total volume of water used was recorded. The black solid that remain in the dissolved
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Acids And BAses Acids And BAses 8.1 8.2 8.3 8.4 18.1 18.2 18.3 18.4 18.5 Theories of acids and bases Properties of acids and bases Strong and weak acids & bases The pH scale Calculations involving acids and bases (AHL) Buffer solutions (AHL) Salt hydrolysis (AHL) Acid-base titrations (AHL) Indicators (AHL) 8 8.1 THeORies OF Acids And BAses 8.1.1 Define acids and bases according to the Brønsted–Lowry and Lewis theories. 8.1.2 Deduce whether or not a species could act as a Brønsted–Lowry
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Tablets I. Introduction An acid-base titration is a method of neutralizing strong acids. Unbeknownst to many‚ acid-base titrations occur on a daily basis. Our stomachs use acid to help us digest our food – approximately .155 hydrochloric acid (HCl) with a pH of 2-3. When too much of this acid is formed in the stomach‚ heartburn and other discomfort occurs. This is when people grab for their antacids; these are bases that neutralize the excess acid in the stomach. Calcium carbonate
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