Lab 3: Grignard Synthesis Objective: The goal of this lab is to synthesize a Grignard reagent from bromobenzene and magnesium metal in diethyl ether. This same Grignard reagent would then be used to prepare a tertiary alcohol and then purify and characterize the product. Table of Reagents: Name Chemical formula Melting Point Boiling Point Density Safety Hazards Diethyl ether C4H10O -116.3°C 34.6°C 0.7134 g/ml Flammable Bromobenzene C6H5Br -30.6°C 156°C 1.5 g/ml
Premium Diethyl ether Alcohol Magnesium
Social scientists have studied it‚ lawyers have tried to fix it and post-feminist society is over it. But women are still outnumbered by men in math‚ science and engineering fields. Most overt discrimination against women in the sciences has been reduced or eliminated in recent decades through legal‚ academic‚ corporate and government measures. But a climate that is less than fully friendly to women remains‚ and its texture is often still so taken for granted that it tends to be invisible. The
Free Gender
Synthesis of Acetanilide By: Rick Whitely April 9‚ 2013 Organic Chemistry Lab 1; Professor J. Hutchison Recrystallization is a common method of purifying organic substances through the differences in solubility at different temperature. In this experiment‚ acetanilide was produced by acetylation of aniline with acetic anhydride. The crude acetanilide was dissolved in a solvent in a heated water bath. The solution was cooled slowly in an ice bath as crystals form out. As the compound crystallizes
Premium Amine Oxygen Acetic acid
Abstract – This multi-step synthesis uses aniline as the starting reagent to synthesize five compounds employing several reactions such as acetylation‚ diazo coupling‚ nitration‚ bromination‚ and hydrolysis. The isolated products were analyzed with TLC and spectral data that determined most products were pure while some had a few impurities indicated by GC‚ LC‚ and a wide melting point range was shown for products 2 and 3. The presence of water in product 2 and 7 was indicated by the IR. Acetanilide
Premium Chemistry Chemical reaction Oxygen
Synthesis of Acetaminophen Lab Report Bijal Patel‚ 20467049 Partner: Poojan Parikh T.A.’s: Long Pu CHEM 123L‚ Section: 006‚ Rm: ESC 149 Tuesday February 4‚ 2013‚ 2:30pm-5:20pm Experiment Done: Tuesday January 22‚ 2013 Introduction Acetaminophen was first introduced in 1955 (Richman‚ 2004). It is an over-the-counter drug that relieves pain and reduced fevers. Acetaminophen is considered an alternate to aspirin since it does not irritate the stomach (Richman‚ 2004). It also has very
Premium Functional group Chemistry Carboxylic acid
A Synthesis of Safrole and o-Safrole W.H. Perkin & V.M. Trikojus J. Chem. Soc. 1663 (1927) HTML by Rhodium No direct synthesis of safrole has been recorded‚ the most recent attempt being that of Baker and Robinson (JCS‚ 1925‚ 127‚ 1424)‚ who distilled the product of the action of silver oxide and water upon gamma-piperonylpropyltrimethylammonium iodide‚ but obtained isosafrole‚ the double bond moving into the position of greater stability. Kawai (Sci. Papers Inst. Phys. Chem. Res.‚ 1925‚ 3‚ 263)
Premium Sodium Ethanol Sodium sulfate
countries and could result in criminal charges being filed. If carried out by individuals unskilled at chemistry they could result in serious bodily harm. MDMA ("Ecstasy") is a semi-synthetic compound which can be made relatively easily from available precursors. Synthesis instructions exist which can be followed by an amateur with very little knowledge of chemistry. However‚ people with less than 2 years of college chemistry experience would probably not be capable of sucessfully synthesizing MDMA‚ and
Premium Sodium borohydride Chemistry Chemical reaction
Synthesis of Phenacetin from para-Acetamidophenol Aims: To determine how phenacetin from acetamidophenol (known as paracetamol) is synthesized using Sodium Ethoxide Iodine‚ which is the Williamson Ether synthesis. Experimental: Sodium metal was patted dry to remove any oil and was cat into small pieces. A dry 100cm3 round bottom flask was placed on a cork ring‚ on a balance and tarred sodium metal (0.6g) was placed into the flask. The flask was then attached to the dry reflux condenser
Premium Distillation Temperature
is . . . Can we? From what I observed is happening now‚ instead of being the country’s biggest hope‚ we seem to be one of its burdens. There’s pre-marital sex‚ prostitution‚ juvenile delinquencies‚ and the list goes on and on. However‚ one of the biggest problems our teenagers are facing is . . . laziness. I‚ myself‚ as a teenager‚ admit that. And we all know that laziness is not an illness. Now what are the reasons why teenagers today are lazy? According to Sara Broers from her article Why are
Premium Adolescence Educational psychology Psychology
Gay/Lesbian Families Adoption is an extremely sensitive subject‚(insert dash) especially for individuals who are Gay or Lesbian. There is much controversy on the topic. There are a variety of ways to which it isn’t possible for a couple to adopt. Infertility is becoming a greater problem in our time. In Gerald P. Mallon’s article‚ “Assessing Lesbian and Gay Prospective Foster and Adoptive Families: A Focus on the Home Study Process‚” in 2007. He introduces a few different ways gay men and lesbian
Premium Homosexuality Adoption Foster care