6. FIRST DERIVATIVE ZERO CROSSING METHOD 6.1. ABSTRACT: Simple‚ specific‚ accurate and precise 1st order derivative zero-crossing spectroscopic method was developed for simultaneous determination of PHENYLEPHRINE and EBASTINE from their binary mixture. In this 1st derivative zero-crossing spectroscopic method the amplitudes of the 1st order derivative of the spectra of the binary mixture containing PHE and EBS were measured at 252.2 nm (zero crossing of EBS) for determination of PHE and at 274.8
Premium Chemistry Ethanol Chemical reaction
. Yes‚ comparably to TLC plate 2 and 3. The benzophenone is more neutral but as the same time its nonpolar‚ being that Silica gel in TLC 2 was polar and the solvent ethyl acetate-hexane is non-polar it moved relatively with the solvent. The stationary phase in TLC 3‚ alumina is non polar and the solvent ethyl acetate is polar so from the ideal that polar does not attract non-polar benzophenone stick stronger to alumina non-polar rather than moving up with polar solvent ethyl acetate as it did in
Premium Oxygen Solvent Acid
Name: __________________________ Date: _____________ 1.|Complete the table and use the result to estimate the limit. x|||||||f(x)|||||||| A)|–0.076923| B)|0.423077| C)|0.298077| D)|0.548077| E)|–0.451923| 2.|Determine the following limit. (Hint: Use the graph of the function.)| A)|6| B)|5| C)|1| D)|4| E)|does not exist| 3.|A graph of is shown and a c-value is given. For this problem‚ use the graph to find .| A)|0| B)|–10| C)|–5| D)|15| E)|does not exist| 4.|Use
Premium Mathematics Economics Molecule
Chromatographic conditions Shimadzu VP-ODS column is (250 mm x 4.6 mm i.d.‚ 5 µm particle size)‚ Shimadzu‚ Kyoto‚ Japan. The mobile phase consisted of a mixture of 0.3% TEA‚ 10% n-propanol in a solution of 0.1 M SDS adjusted to pH 2.8 using 0.02 M orthophosphoric acid. It was pumped at a flow rate of 1 mL min-1. The column was kept at ambient temperature and the wavelength of the detector was at 225 nm. Standard solutions Stock solutions of LVD‚ CBD and ETC containing to 1.0 mg mL-1 were prepared
Premium Chemistry Chromatography Analytical chemistry
Anionic Exchange Ion Chromatography to Detect the Anions Concentrations in the water Samples Narendra Boppana‚ Nasser Ali‚ Martin Chavez‚ Sear Introduction: Ion Exchange Chromatography is a process where the ionic exchange occurs in between the stationary phase and the sample in the mobile phase‚ by using this ionic exchange phenomenon it is easy to separate the compounds. Ionic exchange depends on the electrical properties
Premium Ion Chemistry Atom
unknown compound. In this experiment‚ chromatography and titration were performed to identify the unknown amino acid. Within experimental error‚ the results were consistent with the reference literature cited in this report. Experimental Thin Layer Chromatography The amino acid standards used in this experiment were Alanine‚ Glycine‚ Serine‚ and Histidine. These standards and the unknown were separated by performing a method of chromatography. Thin layer chromatography (TLC) was performed by using a mobile
Premium
Institute of Technology MSc in Oil & Gas Technology “CONTRACT LAW” “THE INTERPRETATION OF LEGAL TERMS ABOUT CONTRACTUAL OBLIGATIONS OF THE PARTIES IN AN OIL OR GAS EXPLORATION/EXTRACTION CONTRACT” Authors: Andreou Christos Georgiou Manolis Kakanis Iordanis Skarvelas Stathis Supervisor: Pr. K. Kalambouka November 2012 ABSTRACT The purpose of this assignment is to identify the contractual obligations of the parties in oil and gas exploration and extraction contracts. The
Premium Petroleum Natural gas Contract
Chromatography of Food Dye Chem 180-DL3 Abstract: The goal of this experiment was to use different dyes to determine the Rf value. Chromatography is done to determine the presence of a mixture in a substance. In this experiment different dyes were used such as McCormick food coloring‚ M&M’s‚ Kool-Aid‚ and the dyes that came with the lab kit. Experiment and Observation: In this experiment a 50mL beaker was filled with luke warm water and a pinch of salt water was dissolved in it
Premium Food coloring E number
Objectives: To use the process of chromatography to separate plant pigments. To compare the plant pigments found in spinach and red leaf lettuce leaves. Hypotheses: I believe the spinach leaf in the acetone will have a higher pigment of chlorophyll a and the red leaf lettuce will have a higher pigment of anthocyanin. I believe the spinach leaf in distilled water will have a higher pigment of chlorophyll a and the red leaf lettuce will have a higher pigment of anthocyanin. Discussion Questions:
Premium Chlorophyll Photosynthesis
Serratiopeptidase drug was purchased from MARS Therapeutics & Chemicals limited‚ Hyderabad‚ India. The standard drug Fenofibrate was purchased from USV limited‚ Himachal Pradesh‚ India. Assay kits for serum Total Cholesterol (TC)‚ Triglycerides (TGL)‚ High density lipoproteins were purchased from Erba Mannheim‚ Transasia Bio-Medicals limited‚ Himachal Pradesh‚ India. All other chemicals were of analytical grade. The experiment was conducted using [12] male Albino Wistar rats (150-200g)‚ at about
Premium Chromatography Acetic acid Aspirin