"Grignard reaction preparation of benzoic acid lab report" Essays and Research Papers

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    Sn1 Reaction Lab Report

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    The effect of temperature on the reaction rate: As the temperature increases it provides more kinetic energy to the molecules allowing them to move faster and with more energy the molecules can overcome the activation energy barrier and therefore the reaction occurs faster. 5. Since the proposed mechanism is a SN1 reaction the reaction got faster as the polarity increased. This is because SN1 reactions work best with polar protic solvents as they stabilize the carbocation. Therefore‚ as seen

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    Lab Report: Acid-Base Titration Brianna Morrison Chemistry 111 October 11‚ 2010 Aim: To standardize a solution of the base sodium hydroxide using oxalic acid dihydrate as primary standard acid. Also to determine the amount of sodium hydroxide it takes to titrate a weighted sample of an unknown acid. Procedure: As outlined in instructions provided‚ no changes were made to the procedure. Data: Part A: Trial 1: Amount of H C O 2H O: 0.96 g Buret before titration: 3.6

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    because of the amount of time given in summer lab we had to save time and cut some days out. We were able to do this by being given our own Salicylic acid (SA) prepared for us instead of having to used wintergreen to make it and recrystallize it. In addition‚ we skipped the qualitative test of our purity for SA and Aspirin (ASA). The first part of this experiment is the preparation of ASA from SA were‚ we prepared our aspirin from the collected salicylic acid. A screw-capped vial was weighed empty to

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    Bromobenzene Reaction Lab

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    During the initiation and formation of the Grignard crushed magnesium was placed in a round bottomed flask with an iodine crystal with a bromobenzene solution with a stir bar. Once the stirring began‚ the solution turned brown and over time began to lighten up. The color change to brown indicated that the reaction began and this is why an iodine crystal was placed in the solution. The reaction started to boil due to its own reflux so heat didn’t need to be applied. Next the anhydrous ether solution

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    the value of the sum for Reaction 1 and Reaction 2’s change in temperature‚ compared to Reaction 3’s change in temperature. Reaction 1 was the dissolution of solid sodium hydroxide in water with a ΔH°rxn of -47047 J/mol‚ Reaction 2 was the neutralization of liquid sodium hydroxide with HCl with a ΔH°rxn of -31289 J/mol and Reaction 3 was the dissolution and neutralization of solid NaOH with HCl with a ΔH°rxn of -91000 J/mol. Consequently‚ the sum of Reaction 1 and Reaction 2 was -78336 J/mol‚ similar

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    Wittig Reaction Lab Report

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    by Georg Wittig in 1954‚ the Wittig reaction is a robust organic synthesis method for preparing stereospecific alkenes. In general‚ Wittig reactions involve an aldehyde or ketone and a Wittig reagent (triphenylphosphonium ylide) and result in the formation of an alkene product and triphenylphosphine oxide (side product). Stereospecific alkene products can be synthesized by adjusting the reaction reagents and conditions. In the 60 years since the Wittig reaction was discovered‚ many articles have

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    10-fold dilution of this ionic iron solution and 5 drops of concentrated HNO3 was made. This solution served as the source of ionic Iron for the remainder of the lab and was labeled “stock ionic Iron solution.” Next‚ a 50-mL aqueous ionic Iron and FerroZine® complex solution was prepared by adding 5.00mL stock ionic Iron‚ 3-mL of acetic acid buffer‚ 2-mL of 5% hydroxylamine hydrochloride‚ allowing five minutes for hydroxylamine to reduce Fe3+ to Fe2+‚ adding 2.5-mL of 0.01 M FerroZine® solution‚ and

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    Title: The affects of hydrogen peroxide on catalase reactions in animal and plant cells at different temperatures and states. Introduction: All living organisms in the kingdoms of life are composed of and depend on cells to function normally. Not all cells‚ however‚ are alike. There are two primary types of cells: eukaryotic and prokaryotic cells. Cells contain organelles‚ or tiny cellular structures‚ that carry out specific functions necessary for normal cellular operation. (Regina Bailey Updated

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    Thermite Background: Thermite is a powder made from aluminum powder and a metal oxide [usually iron oxide (Fe2O3‚ known as rust)]. The thermite reaction is a redox reaction‚ where Aluminum reduces the oxide of another metal. For example‚ when using iron oxide (as I did) the equation would be Fe2O3(s) + 2 Al(s) -> Al2O3(s) + 2 Fe(l). Black or blue iron oxide (Fe3O4) could also be used. Other examples of possible oxides are manganese thermite (MnO2)‚ Cr2O3‚ and copper thermite (CuO). Aluminum can

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    The purpose of the Weak Acid Dissociation experiment is to determine the dissociation constant of a weak acid experimentally by using acid-base titration with a strong base and stoichiometry. An acid-base titration is a method by which a basic (or acidic) solution of unknown concentration is reacted with an acidic (or basic) solution of known concentration. (1) The pH in acid-base titration is measured using a pH meter or color changing indicator‚ such as phenolphthalein‚ as the known solution is

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