Experiment 1: Purification of Benzoic Acid by Recrystallization III. Introduction Purification - physical separation of impurities and by-products from an impure sample pure substance. *Distillation- for liquid compounds‚ *Recrystallization- solid compounds Recrystallization - precipitation of a solid cpd. from a saturated solution in the form of crystals through cooling or evaporation -7 steps: 1) selecting the appropriate solvent 2) dissolving the solute 3) decolorizing the
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Carboxylic acids are compounds which contain a carboxyl group‚ -COOH group‚ where the -COOH group is attached either to a hydrogen atom or to an alkyl group. One of the example of carboxylic acid is benzoic acid( benzene carboxylic acid) which has a benzene connected to the carboxyl carboxyl group‚ -COOH group. It has a formula of C6H5COOH. The carbon atom of a carboxyl group has a high oxidation state. Therefore‚ that many of the chemical reactions used for their preparation are oxidations. In
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Wang Experiment #4 Recrystallization of Pure Phthalic Acid‚ Benzoic Acid and Napthalene Introduction Recrystallization is a important method in purifying organic compounds which are solid. It is an effective method that is important to be familiar with that is essential in the industrial chemical world. This experiment will allow students to be familiarized with the technique of recrystallization by working with phtalic acid‚ benzoic acid and naphthalene from appropriate organic solvents. Experimental
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Megan Wierzbowski Organic II Laboratory Wed. 11-1:50 Title: Grignard Reaction with a Ketone: Triphenylmethanol Part 1 Objective: The goal of this experiment is to learn to make Grignard reagents. The reactions of the Grignard reagents with ketones form tertiary alcohols. These reagents are highly air- and moisture-sensitive materials. We will observe the formation of the Grignard reagents‚ which magnesium metal is transformed into organometallic salts. Experimental Procedure:
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The obtained mass of benzocaine and benzoic acid mixture was measured to be 2.075 grams. Following being dried for a week the mass of benzocaine was recorded to be 0.250 grams‚ and benzoic acid was recorded to be 0.600 grams. The melting point range of benzocaine was measured to be 89.5°C-91.5°C‚ while benzoic acid’s melting point range was measured to be 129°C-131.3°C. The percent mass recovered was calculated to be 40.96% for the experiment. Table 1 illustrates the collected information. Starting
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Unit 4B Task 2 Title Recrystallization of benzoic Acid Aim Equipment 1. Erlenmeyer flask 2. Graduated cylinder 3. Hot plate 4. Small beaker 5. Ice bath (if necessary) 6. Filter paper 7. Buchner funnel 8. Spatula 9. Weighing machine Method 1. Weighing paper was used to weigh approximately 1.00g of ‘impure Benzoic acid to produce re crystallization’. 2. Moved it to a 125ml Erlenmeyer flask. 3. Poured approximately 20ml of distilled water by using a graduated cylinder
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Acid Rain Lab Report Introduction: The problem was to see how crushed chalk and whole chalk weather differently. The independent variables are The temperature of the liquids The surface area of the chalk‚ crushed vs whole The dependant variable was the weathering of the chalk; this was calculated by measuring the foam reactant. Procedure: Part B- For the two partners recording data with the room temperature liquids‚ the materials where collected first. Two of the graduated
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E XPE RIME NT 4 . 5 Reactions of acids Aim To investigate and compare some reactions of a strong acid‚ hydrochloric acid‚ and a weak acid‚ ethanoic acid (common name‚ acetic acid) Equipment Dropper bottles containing: • 0.1 M hydrochloric acid‚ HCl • 0.1 M ethanoic acid (acetic acid)‚ CH3COOH • 0.1 M sodium hydroxide‚ NaOH • 1 M hydrochloric acid‚ HCl • 1 M ethanoic acid (acetic acid)‚ CH3COOH • universal indicator solution • limewater (calcium hydroxide‚ Ca(OH)2) Marble chips (calcium carbonate
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Acid Rain Lab #1 Chem. 1 20 February 2016 Concordia University Texas Angelina Luna angelinaluna97@yahoo.com Chem 1- Sect C Acid Rain Lab #1 Professor Koeck Abstract In this experiment our main objective was to create three gaseous oxides CO₂‚ SO₂ and NO₂ by using data that was collected using a pH sensor which was connected to a laptop with LoggerPro and Vernier. We created the gases by bubbling each gas into the water to create the three acidic solutions we were looking for. Once that
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Lab Report Acids and Alkalis: Chemistry of Neutralization and Salt Formation Introduction: An acid is a group of chemicals. Acids are positively charged ions‚ they are liquid and are solutions of pure compounds in water. If you want to know if something is an acid‚ you can test it by using litmus paper. Acids will turn litmus paper red‚ whilst alkalis will turn it blue. Alkalis are negatively charged ions and are usually solid. Aim: To find out how much of different acids is needed to neutralize
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