CHEM 3125 Experiment 4: Multistep synthesis of tetraphenylcyclopentadienone Overall Synthesis: CHEMICALS: wk 1: thiamine hydrochloride (1 g/student)‚ 95% ethanol (8 mls/ student)‚ 2M NaOH (5 mls/student)‚ benzaldehyde (4 mls/student) wk 2: 95% ethanol (30 mls/student) wk 3: acetic acid (6 mls/student)‚ ammonium nitrate (1 g/student)‚ 0.1g/ml cupric acetate (1.5 mls/student)‚ dichloromethane (6 mls/ student)‚ 30% acetone in heptanes (3 mls/student)‚ 95% ethanol (20 mls/student) wk 4:
Premium Chemical reaction Chemistry Ethanol
and industrial applications. Citric Acid is one of the organic acids commonly used as a chelating agent. It is considered an excellent chelating agent that binds metals. It is used to remove lime scale from boilers and evaporators. It can be used to soften water‚ which makes it useful in soaps and laundry detergents. By chelating the metals in hard water‚ it lets these cleaners produce foam and work better without need for water softening devices. Citric acid is the active ingredient in some bathroom
Premium Water Acid
A. Title – Acid-Base Extraction with Separatory Funnel B. Introduction – The main objective of the experiment was the extract an acid‚ a base‚ and a neutral compound from a 2:1:1 compound of benzoic acid‚ p-nitroaniline‚ and azobenzene. In theory‚ an extraction technique based on phase distribution should allow two immiscible solvents to separate with a portion of the solute distributed into each. Using a separatory funnel‚ acids were extracted with bases (NaOH)‚ and bases were extracted
Premium Chlorine Sodium chloride Acid
Introduction The American Chemical Society databases were investigated through Scifinder Scholar Version X to find any information about Butyl 2-Cyano-(3‚5 dichloro-phenyl)-2-propenoate. There was no previous information present. Then‚ the microscale synthesis and characterization of Butyl 2-Cyano-(3‚5 dichloro-phenyl)-2-propenoate was conducted with the base catalyzed Knoevengael condensation of the butyl cyanoacetate and corresponding aldehyde (gkharas/235_14F/235_14F_Lab_2.pdf) and analysis. The elemental
Premium Thin layer chromatography Stoichiometry 3rd millennium
November 15‚ 2007 Synthesis of 1-Bromobutane Introduction: The purpose of this experiment is to synthesize 1-bromobutane from 1-butanol and sodium bromide. In order for this reaction to reach completion there are four major operations that need to be performed. The four major operations include refluxing‚ simple distillation‚ separation‚ and drying. To begin‚ in order for the compounds to react they will be dissolved in water and sulfuric acid will be added. The addition of sulfuric acid will then generate
Premium Distillation
Ethanoic Acid Advantages: Ethanoic acid is non-toxic and is a weak acid‚ meaning it will not do any damage to most surfaces as it does not corrode or bind to other metals‚ therefore can be easily removed through washing or rinsing it. Disadvantages: Ethanoic Acid is the slowest de-scaler of the three acids‚ and is therefore the least effective. It also may cause an unpleasant smell‚ and can have a negative effect on the taste of coffee meaning one would need to spend longer time rinsing and cleaning
Premium Acetic acid Acid Vinegar
AMINO ACIDS BY MEANS OF TITRATION CURVE ABSTRACT The aim of the experiment was to identify an unknown amino acid through acid-base titrations which was prepared in water to form an acidic solution. Each group prepared unknown amino acid hydrochloride. The pre-prepared basic solution was slowly added to the amino acid solution and pH change was closely observed using the pH meter. During these titrations the amino acid converted from cation to zwitterion to anion; zwitterion is an amino acid with
Premium Amino acid PH Acid
Acid Rain and its Chemistry Acid rain is a type of pollution that is becoming a major threat to our planet and is need of attention. Acid rain has significantly increased ever since the industrial revolution‚ and now around the world‚ countries like Russia‚ China‚ and those in Europe are facing increasing levels of acidity in their rain. Not only is it becoming more acidic but it is also spreading by the pumping of sulfuric gasses deeper into the atmosphere from of the use of taller smokestacks
Free Oxygen Acid rain Sulfuric acid
Acid Rain Definition: The term acid rain refers to what scientists call acid deposition. It is caused by airborne acidic pollutants and has highly destructive results. Scientists first discovered acid rain in 1852‚ when the English chemist Robert Agnus invented the term. From then until now‚ acid rain has been an issue of intense debate among scientists and policy makers. Acid rain‚ one of the most important environmental problems of all‚ cannot be seen. The invisible gases that cause acid
Premium Acid rain Pollution PH
The Effects of Acid Rain Bio-105 Abstract The effects of acid rain is damaging no matter how you look at the picture. Acid rain effects open areas more than forests due to the trees blocking some of the rain from hitting the ground. Acid rain is monitored by using emissions monitors. This helps figure out how much acid is in rainwater. Acid rain is harmful to fish by killing off entire species. Acid rain is harmful to living creatures‚ but many do not realize how toxic it can be to
Premium Sedimentary rock Rock Igneous rock