conducted to determine the identity of an unknown aldehyde or ketone. The tests include a Tollens test‚ a Schiff test‚ an iodoform test‚ and a derivative melting point test. The data of the first three tests was inconclusive. The final derivative melting point test was utilized to successfully determine that the unknown was the ketone‚ Propiophenone. Introduction: Qualitative analysis is a method or series of methods used to determine the identity of an unknown compound (1). It is imperative that
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The purpose of this experiment was to identify one ketone with Thin Layer Chromatography and one using NMR spectrometry. We will do this by making 2‚ 4 a DNPH derivative and checking the melting points. Theory: By Using specific methods of compounds detection‚ we can match an unknown compound with a known compound because similar compounds will display similar characteristics. In this experiment‚ identifications of the unknown ketone was accomplished using thin layer chromatography‚ melting
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Flavoring Agents made from Aldehydes and Ketones Peter Konn Mountain State University Chemistry 302 7/31/12 Abstract This paper looks to delve into the chemistry behind ketones and aldehydes as well as related compounds. The endeavor involved looking into the way their bonding influences how they react. It also considers the simple physical properties of these compounds including their reaction with other compounds‚ chemical structures and formulas. The paper also looked to
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Identifying an Unknown Aldehyde or Ketone Introduction The purpose of this lab is to identify an unknown aldehyde or ketone substance using chemical tests. The chemical tests used in this experiment are solubility‚ Schiff‚ Bisulfite‚ and Iodoform tests. Also‚ a 2‚4-dinitrophenylhydrazone derivative synthesis reaction will be completed from which a melting point will be obtained. The chemical test results and the melting point analysis will be compared to the table of compounds given to find the
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Aldehyde and Ketone 1. ALDEHYDE Definition: An aldehyde is an organic compound containing a formyl group. This functional group‚ with the structure R-CHO‚ consists of a carbonyl center (a carbon double bonded to oxygen) bonded to hydrogen and an R group‚ which is any generic alkyl or side chain. The group without R is called the aldehyde group or formyl group. Aldehydes differ from ketones in that the carbonyl is placed at the end of a carbon skeleton rather than between two carbon atoms
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ALDEHYDES AND KETONES Abstract Aldehydes and Ketones have certain characteristics in common. However‚ both couldn’t exist in the same compound. Some test for the presence of aldehyde was made for this experiment. These tests includes Tollen’s test‚ Benedict’s Test‚ 2-4-dinitrophenylhydrazine and Schiff’s test. All the tests conduted yielded same results‚ that is‚ formalin and benzaldehyde are aldehyde-containing compounds while acetone is a ketone. On the other hand‚ effect of acid concentration
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Aldehydes‚ Ketones and Saccharides Aldehydes – contains a carbonyl group at the end of the carbon chain. – RCOH Ketones – contains a carbonyl group in the middle of the carbon chain. – RCOR * 2‚4-dinitrophenylhydrazine Test - Test for Carbonyl group * Sodium Bisulfate Test- Test for Aldehydes and Methy Ketones * White precipitate * Ketones with more than 2 carbon – non-reactive * Ketones with 2 carbons – slightly reactive * Schiff’s
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Analysis of Alcohols‚ Aldehydes and Ketones Karl Wayne Mancao‚ Raphaell Mordeno‚ Andres Pastrana III*‚ and Shannen Peñaverde Department of Biology‚ University of Santo Tomas‚ Manila‚ Philippines Abstract The proponents have done several tests for identifying alcohols‚ aldehydes and ketones. These tests are Dichromate test‚ Tollens test‚ Lucas test‚ DNPH test and Iodoform test. Three samples got positive result in dichromate test and one in Tollens test. Lucas test got one sample that has
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D. REACTIONS OF ALDEHYDES AND KETONES WITH SODIUM HYDROXIDE (By: Mary Deo Luigi J. Mabunay 1N-3) Objective: To determine the reactions of Aldehydes and Ketones when combined with Sodium Hydroxide. Process: * Obtain 5 clean and dry test tubes * Put 2mL of 40% NaOH solution to test tubes 1‚ 2 and 3 and on test tubes 4 and 5‚ put 10% NaOH solution * Add 10 drops of the following solution: * Tube 1: formaldehyde * Tube 2: benzaldehyde * Tube 3: acetaldehyde
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Reactions of Carbonyls-Aldehyde/Ketone Analysis: Introduction: The carbonyl group is a rich source of many important reactions in organic chemistry‚ with two fundamental properties that are primarily responsible for its diverse chemistry. The first is the polarization of the. Carbon-oxygen pi bond‚ owing to the relatively high electro negativity. The second property of a carbonyl function is to increase the acidity of the alpha-hydrogen atoms‚ which are the hydrogen’s
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