Experiment H: Identification of an Unknown Organic Compound The objective of this lab was straightforward. We were given an unknown compound and we were to perform an IR spectroscopy and as well as NMR spectroscopy. With the IR spectroscopy‚ I was able to name the functional groups I have on my compound and further confirmed my assumptions by looking at the NMR spectroscopy after. The unknown number I was given was number 203. The molecular weight of the compound was 121. From the molecular weight
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Grainy and shiny white Becoming all liquid 125 Clear B. Melting point of unknown #42 1st trial Temperature (¡ÆC) Observation Unmelted Shiny light yellow crystal First liquid appear point 99 Grainy yellow Becoming all liquid 101 Clear 2nd trial Temperature (¡ÆC) Observation Unmelted Shiny light yellow crystal First liquid appear point 95 Grainy yellow Becoming all liquid 97 Clear C. Melting point of mixture (Unknown + Benzil) Temperature (¡ÆC) Observation Unmelted Shiny light yellow
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Amines are aliphatic and aromatic derivatives of ammonia. Amines‚ like ammonia‚ are weak bases (Kb = 10−4 to 10−6). This basicity is due to the unshared electron pair on the nitrogen atom. Classification and nomenclature of amines Amines are classified as primary‚ secondary‚ or tertiary based upon the number of carbon-containing groups that are attached to the nitrogen atom. Those amine compounds that have only one group attached to the nitrogen atom are primary‚ while those with two or three
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Reactions of amines Reaction of amines with acids – acids and amines form ammonium salts. R – NH2 + HCl → R – NH3+ + OH – Amine acid amine salt Example 1 CH3 – NH2 + HCl → CH3 – NH3 + Cl- Methylamine Methylammonium Example 2 CH3CH2 – NH3 + Cl → CH3CH2NH2 . HCl Ethylammonium Ethylamine Reaction of amine with water – when amines react with water‚ they produce hydroxide ( OH ) R – NH2 + H2O ⇄ R – NH3+ + OH- Amine water
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of biological system is usually preferred as the pH system‚ which determines the pH level of dilute aqueous solutions. In this laboratory‚ the data collected from the experiment will be used to graph the titration curves which help to identify an unknown amino acid. IntroductionAmino acids are simple monomers which are strung together to form proteins. Amino acids play a key cellular role in structure and function. Proteins themselves participate in nearly every physiological event in the cell. Since
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A Report of Experiment 1 Purification and Identification of An Unknown Mixture Aim To separate a mixture of a neutral (ester‚ alcohol‚ ketone‚ aldehyde or ether) and an acidic compound (phenol or carboxylic acid) or a neutral and a basic compound (amine)‚ and to identify the unknown mixture by physical (M.P. or B.P.) and spectroscopic methods (NMR‚ IR and MS). Method The mixture (sample number: 27) was dissolved in 200 mL of CH2Cl2 and then extracted with 10% NaOH. The acid was removed
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Hydrocarbon Derivative: Amines Amines are a type of hydrocarbon derivative‚ and they are used in many ways in society. Several companies use amines in products such as drugs and medicines. Also‚ in nature‚ amino acids help the body make proteins‚ and amines are found in many vitamins. For example‚ DOW Chemicals “plays an important role in commonly used products found around the world” by using amines in the manufacturing of energy drinks‚ detergents‚ insulin‚ etc. This is a very large industry
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Identification of Unknown Carbohydrates using various biochemical tests Date of experiment: 11/10/2012 Name of Student: Vicki Marshall Introduction A series of biochemical tests was carried out to identify unknown carbohydrates. There were six carbohydrates that needed to be identified; they have been randomly labelled A-F. The carbohydrates are glucose‚ fructose‚ maltose‚ lactose‚ sucrose and starch. There was six tests that were carried out to help identify them‚ these were: Iodine Test
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Increasing Fiber in Rice Pilaf Arcelay‚ Marilyn March 30‚ 2007 FOS 4041L Dr. Dixon Introduction Obesity is a word that everyone is currently familiar with. The media and health professionals have been working tirelessly to make the general public aware of its prevalence and detriments to society. With the staggering statistics of 32.2% prevalence in adults and a range of 13.9% to 18.9% prevalence in children and adolescents‚ these outstanding numbers stand
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flipped). Percent yield of the crude product was 67.75%. (What does this percentage mean?) The IR spectrum of purified product identified the Arene strand of 2969.71 indicating C-H stretch. Ester which indicated a C=O stretch of a 1750-1735. Aliphatic amines showed an absorption band of 1217.62 indicating a C-N stretch. (This makes no sense‚ look at the molecule you have and relate the points. Furthermore‚ you need to compare your results to a literature source) An example of a practical application would
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