Chemistry Laboratory - CH 201 (2010-2011) Experiment 4B Column and Thin-Layer Chromatography of Capsicum Frutescens L. Pigments John Cyril Abanto*‚ Vernalyn Abarintos and Clarice Gail Abella Department of Chemistry‚ College of Science University of Santo Tomas‚ Espana Street‚ Manila 1050 Date Submitted: September‚ 2010 ____________________________________________________________ _________________________________ Abstract: The experiment was done to separate and analyze the components
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A Fight for Freedom for Journalists “A First Amendment Blind Spot” was published in The Wall Street Journal by Theodore J. Boutrous Jr. The author is a partner of the Gibson‚ Dunn and Crutcher LLP. He is also the co-chair of the International Women’s Media Foundation. Moreover‚ he was denominated by the National Law Journal as one of 100 most influential lawyers in America (“Theodore J. Boutrous‚ Jr.‚ JD Biography”). In “A First Amendment Blind Spot”‚ Theodore J. Boutrous Jr. draws the attention
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To: Wesley Clark From: Lizzie Heath Date: March 4‚ 2013 Subject: Thin-Layer Chromatographic Analysis of Drug Components (Experiment #15) The purpose of this experiment is to determine the components of an unknown drug and identify it as one of six (6) commercial drugs by using thin-layer chromatography. I added approximately a quarter of a tablet of acetaminophen‚ aspirin‚ caffeine‚ ibuprofen‚ salicylamide‚ and the unknown (#19) to separate test tubes containing 2.5mL of dichloromethane
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The First Experience for a Wisdom Tooth Extraction Just a year ago‚ I got my wisdom tooth pulled for the first time. My wisdom tooth had started to ache on last New Year ‘s day. Normally‚ I celebrate New Year’s day with special food‚ but I was no time for that because of an excruciating pain. Unfortunately‚ my husband and I didn’t know a good doctor in this city‚ and we couldn’t contact friend who knows well regional information because it was a big holiday! At the long time‚ I found a dentist
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Introduction Chromatography is a technique used to separate a mixture into its individual components. In this experiment‚ chromatography is done by using a thin layer chromatography (TLC) plate and filter paper. The word ‘chromatography’ itself means the separation of colours. However‚ nowadays‚ both coloured and colourless compound are used in chromatography by various methods. In chromatography‚ the separation process of mixture is mainly based upon the polarity and molecular weight of sample
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the Extraction lab is to separate and purify benzoic acid‚ 2-naphthol‚ and naphthalene. These organic solids are purified by partitioning the solid in 2 immiscible solvents‚ diethyl ether and sodium bicarbonate or sodium hydroxide. II. Significance a. The significance of the Extraction lab is to purify Acetanilide benzoic acid‚ 2-naphthol‚ and naphthalene by determining the partition coefficient. This value is determined by dividing the solubility of the given solute in the extraction solvent
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As we know‚ the TLC is a separation technique that has two phases: the stationary phase and mobile phase. The stationary phase is silica gel (SiO2) which is very polar compound‚ while the mobile phase is 0.5% acetic acid which has less polar. Also‚ as we know‚ the compound will rather to stay with stationary phase or travel with mobile phase depend on its polarity. The result show as that the polarity of the solvent is the key factor for the compound to travel with it or stay in stationary phase
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sugar molecules are produced. In this experiment‚ trials were conducted to test hypothesis of whether all 40 circular spinach leaves would arise or stay at ground level in differential water temperature’s. Using a fluorescent light source gave us another perspective to keep in mind for it could be an advantage or loss to new current predications. Later in discussion‚ relationship to this experience among two other will
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January 24‚ 2013 TLC Analysis of Analgesic Drugs Introduction: The purpose of this lab was to determine the composition of four different over-the-counter drugs (Anacin‚ Bufferin‚ Excedrin‚ and Tylenol). These compositions were determined by using the method of thin-layer chromatography (TLC) of the four over-the-counter drugs‚ which were then compared to four different components of drugs (acetaminophen‚ aspirin‚ caffeine‚ and salicylamide). Experiment Scheme1:
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compounds (those with the lowest boiling point) will vaporize first (i.e. be converted to gases)‚ leaving the higher-boiling compounds behind in the mixture. By isolating the vapor produced at different temperatures and condensing them (i.e.‚ converting gases to liquids)‚ you can effectively separate and purify compounds based on their boiling points. While there are multiple factors that contribute to the efficiency of distillation‚ the first‚ most obvious is the boiling points of the compounds themselves
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