the forming Butyl 2-Cyano-(3‚5 dichloro-phenyl)-2-propenoate. The analyses that were used to prove its composition and structure include; IR spectroscopy‚ thin layer chromatography (TLC)‚ and CHN analysis. A radical copolymerization reaction was conducted‚ with the initiation by radical initiator 1‚1’-azobiscyclohexanecarbonitrile. CHN analysis‚ IR spectroscopy‚ and Proton NMR analysis were used to prove its composition and structure. 1. Introduction The American Chemical Society databases were investigated
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1680-1600 1600-1400 2250-2100 1740-1720 1725-1705 1725-1700 1750-1730 1700-1640 1810 and 1760 1300-1000 Intensity s m m m s s s m w w m-w m-w m-w s s s s s s s Alkanes -CH3 -CH2Alkenes (stretch) (bend) (bend) (stretch) CHARACTERISTIC INFRARED FREQUENCIES (bend) Aromatic (stretch) (out-of-plane bend) Alkyne Aldehyde C=C C C C=O (stretch) Alkene (stretch) Aromatic (stretch) Alkyne (stretch) Aldehyde (stretch) Ketone (acyclic) Carboxylic Acid Ester Amide Anhydride Alcohols‚ ethers
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Multistep Synthesis of Tetraphenylcyclopentadienone Author: Instructor: Date work performed: 10.18.2012--10.25.2012 Date work submitted: 11.01.2012 Abstract: The aim of this experiment was to perform a multistep synthesis to form tetraphenylcyclopentadienone. The first step of the reactions was to synthesize benzoin from the condensation of benzaldehyde. A yield of 28.91% benzoin was obtained. The MP of benzoin was 127O-130O C and the IR spectra displayed a carbonyl peak at 3415 cm-1
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order to synthesize our metal complexes‚ we were able to make both Copper and Ruthenium metals. From this‚ we combined each metal complex with DMSO by refluxing the compound. The metal complexes were analyzed through their melting point and IR spectroscopy to determine whether the metal bonded to a Sulfur atom or an Oxygen atom of the DMSO. After analyzing the IR spectrum‚ it was determined that S=O shifted to a lower wavenumber in CuCl2~2DMSO and that S=O shifted to a higher wavenumber in RuCl2~4DMSO
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product was then distilled using a Hickman still and characterized using infrared spectroscopy. The percent yield of isopentyl acetate was 61.52%. This may have been low due to not all of the condensed product being removed from the Hickman still‚ some product being lost during transfer of the product from the reaction tube into the Hickman still‚ or the loss of some product due to evaporation during distillation. Infrared spectrum analysis of the product indicated that the product was isopentyl
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Infrared Spectroscopy Aim: To obtain IR spectra of know solid sample and liquid sample using the following sample preparing technique: Prepare solid IR sample using Solid Pellet Samplin Technique Use IR is used to identify functional groups. 5 major functional groups easily identified by IR spectroscopy: 1. C=O 2. C–O 3. OH 4. Phenols 5. C–H Instrument details Type of spectrophotometer: Nicolet 380 FT-IR spectroscopy‚ Nicolet Avatar 360 & Thermo Scientific iS10 FT-IR Spectrometer
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Abstract Soil reflectance spectroscopy is a well known technique to assess soil properties rapidly and quantitatively both in point (Spectroscopy) and image (Imaging Spectroscopy (IS)) domains. The quantitative approach has been developed in the past two decades by many researchers and many papers have been published on this subject in the scientific literature. Basically‚ the quantitative approach has been adopted from other disciplines (e.g. food‚ textile‚ pharmaceutical); whereas the mapping
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the metal becomes warm‚ although its appearance doesn’t change. As it heats up‚ it begins to glow dull red‚ then orange‚ brilliant yellow‚ and finally white. How do we explain this? When the metal is at room temperature‚ it emits only invisible infrared radiation. As
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Background NMR spectroscopy is a well established method for structure determination of various organic molecules ranging from small molecules all the way up to large bio-molecules such as proteins‚ DNA and polysaccharides. The chemical environment surrounding each atom as well their proximity to other atoms in a molecule can be studied with various experiments‚ enabling high-resolution 3D-structure determinations as well as verification of the chemical structure. NMR spectroscopy is well suited
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carriedout for the degradation of fabric dyes from aqueous solution using Chara and Chara beads are discussed below.Various analytical techniques like UV-Vis‚ FTIR spectroscopy were used to confirm the decolorization as UV-Vis spectroscopy; FT-IR spectroscopy and toxicity bioassay were truly used [14]. Also‚ Fourier transform infrared spectroscopy (FT-IR) is widely used to confirm the product obtained after decolorization of dye degradation experiments [15]. It helps in determination of reaction
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