BSc Pharmaceutical Technology Practical - No 5 Preparation of a Primary Standard Solution Aim: to prepare a standard solution of pure silver nitrate and use it to determine the concentration of chloride ions in a sample of tap water and another sample of bottled water. Chemicals: * High grade purity silver nitrate * Potassium chromate indicator * Tap water * Bottled water * Distilled water Apparatus: * Laboratory oven * Dessicator * Conical flask
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TABLE OF CONTENTS 1. IA (Alkaline Metals) 1.1. H………………………………………………………………………..2 1.2. Li………………………………………………………………………..2 1.3. Na………………………………………………………………………2 1.4. K………………………………………………………………………..3 1.5. Rb………………………………………………………………………3 1.6. Cs………………………………………………………………………3 1.7. Fr……………………………………………………………………….4 1. IIA (Alkaline Earth Metals) 2.8. Be………………………………………………………………………4 2.9. Mg………………………………………………………………………4 2.10. Ca………………………………………………………………………4
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Experiment 7 Gooch filter crucible or fritted-glass funnel Mother liquor- liquid from which a substance precipitates or crystallizes Filtrate- liquid that passes through the filter Slurry- suspension of solid in liquid Calcium ion can be analyzed by precipitation with oxalate in basic solution to form CaC2O4.H2O The precipitate is soluble in acidic solution because the oxalate anion is a weak base CaC2O4.H2O (calcium oxalate monohydrate ; MW = 146 g/mol) Equation: Ca2+(aq) + C2O42-(aq)
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experiment‚ we are going to make a battery by making an electron current between the metals Zinc and Copper. We aim two study the voltaic cells and the transfer of electrons from the metal to the ion. The tendency for the electrons to flow from one chemical to another‚ such as from the zinc metal to the copper ion as shown here‚ is something that can be channeled and controlled. Channeling the flow of electrons is what we will take up in this experiment. Research question How would changing the shape
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PAGE © UCLES 2012 9701/36/O/N/12 3 1 You are to determine the concentration of aqueous copper(II) sulfate by titration. The concentration of Cu2+ ions in a solution can be found by reaction with an excess of aqueous iodide ions to produce iodine. The amount of iodine formed can be found by titration with thiosulfate ions‚ S2O32–. For Examiner’s Use FB 1 is aqueous copper(II) sulfate‚ CuSO4. FB 2 is 0.100 mol dm–3 sodium thiosulfate‚ Na2S2O3. FB 3 is aqueous potassium iodide
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source of oxalate ion and its content in the fruit varies during different stages. Oxalate ion are extracted from the fruit by holding pulp with dilute H2SO4. The Oxalate ions are estimated volumetrically by titrating the solution with standard KMnO4 solution. OBJECTIVE OF PROJECT In this project‚ we will learn the test the presence of oxalate ions in the guava fruit and how its amount varies during different stages of ripening. THEORY Oxalate ions are extracted
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structures Shapes of molecules of methane‚ ammonia and water Shapes of some other molecules Influence of the nature of electron pairs on bond angles in molecules of methane‚ ammonia and water Shapes of some polyatomic ions Shapes of molecules with multiple bonds Molecular crystals of buckminsterfullerene (C60) 23.1 – 23.7 Summary 1 Examples of covalent molecules with non-octet structures are as follows: Molecule Electron diagram F BF3 B F F SF4
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xa.yimg.com/kq/groups/9534928/992196434/name/1.pdf by WE GORDON - Cited by 8 - Related articles reaction of sulfamic acid with nitrites is practically instan- taneous‚ and only ... differences between the sulfamate ion and the sulfate or chloride ions (12). T. [PDF] Method 9010C - US Environmental Protection Agency www.epa.gov/osw/hazard/testmethods/sw846/pdfs/9010c.pdf the distillation‚ nitrate and nitrite will form nitrous acid‚ which will react with some organic
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Conclusion: The purpose of this lab was to synthesize and purify aspirin. The theoretical yield was calculated to 3.766g. The actual yield of pure aspirin was 2.863g with a yield of 76%. The percent yield indicates that our synthesis was a success but the yield is low and indicates that some of the aspirin was lost during synthesis. Some reasons for loss can result from human error such as loosing product from sticking on the spatula and the Buchner funnel and several weighings. Also‚ when transferring
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Ind. Eng. Chem. Res. 1994‚33‚1687-1691 1687 Synthesis of Triphenyl Phosphate and Benzyl Benzoate with Phase-Transfer Catalyst in Heterogeneous Liquid-Liquid Reaction System S a t o r u Asai‚’ Hidemi Nakamura‚ Mitsunori Tanabe‚ and Kenji Sakamoto Department of Chemical Engineering‚ University of Osaka Prefecture‚ Sakai‚ Osaka 593‚Japan The synthetic reactions of triphenyl phosphate from diphenylphosphoryl chloride and sodium phenoxide and of benzyl benzoate from benzyl chloride and sodium
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