concentration of aqueous copper(II) sulfate by titration. The concentration of Cu2+ ions in a solution can be found by reaction with an excess of aqueous iodide ions to produce iodine. The amount of iodine formed can be found by titration with thiosulfate ions‚ S2O32–. For Examiner’s Use FB 1 is aqueous copper(II) sulfate‚ CuSO4. FB 2 is 0.100 mol dm–3 sodium thiosulfate‚ Na2S2O3. FB 3 is aqueous potassium iodide‚ KI. starch indicator Read through the instructions carefully before starting
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than titrating directly with standard iodide‚ because a high concentration of I- is needed to form the I3- complex. In this type of analysis‚ excess iodide is added to the oxidizing agent‚ and the triiodine is titrated with stand thiosulfate. This indirect analysis finds the number of moles of ascorbic acid based on the known number of moles of IO3- and subtracting half the amount of moles of the thiosulfate solution. II: Equations: Iodate with Iodide: IO3- + 8I- + 6H+ 3I3- + 3H2O Thiosulfate
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together 31. Prepare the solution to be analyzed by placing it in a clean Erlenmeyer flask or beaker 32. Dissolve a single tablet in 500 mL of distilled water in a conical flask and add about 150 mL of distilled water‚ 5 mL of 0.6 mol L−1 potassium iodide‚ 5 mL of 1 molL−1 hydrochloric acid and 1 mL of starch indicator Solution. 33. Use the buret to deliver a stream of titrant to within a couple of mL of your expected endpoint. 34. Use a wash bottle to rinse the sides of the flask and the tip of the
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of valence electron(s) between atoms. It is a type of chemical bond that generates two oppositely charged ions (Larsen‚ 2010). Element that have a positive ion are able to bond with elements with negative ions. This is because the elements share the electrons so that the ionization becomes neutral and both atoms become stable. Materials: 1. Cards with elements and positive or negative ions. 2. Reference Tables for Physical Setting/CHEMISTRY 2011 Edition: Periodic Table of the Elements 3. Bond
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many atoms there are in each molecule (Wikipedia). Ionic compounds are basically defined as being compounds where two or more ions are held next to each other by electrical attraction. One of the ions has a positive charge called a cation and the other has a negative charge called an anion. Cations are usually metal atoms and anions are either nonmetals or polyatomic ions. Usually‚ when we have ionic compounds‚ they form large crystals that you can see with the naked eye (4). A covalent compound
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precipitation reactions‚ as well as to identify spectator ions‚ perception reactions and solubility of different compounds. Experiment and Observations In this experiment I was using a 96-well plate to add two drops of the following solutions into seven wells in rows A through E: cobalt (II) nitrate‚ copper (II) nitrate‚ iron (III) nitrate‚ barium nitrate‚ and nickel (II) nitrate. Afterward‚ two drops of each of sodium phosphate‚ sodium iodide‚ sodium sulfate‚ sodium chloride‚ sodium bicarbonate‚
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monochloride solution from a burette and mix. Then add about 5 mL of a 2.5% solution of mercuric acetate in glacial acetic acid‚ which will act to catalyse the reaction. Insert the stopper which has been previously moistened with a solution of potassium iodide. Keep in a dark place for 3 minutes to allow the unsaturated fatty acid residues of the
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NITROSYL CHLORIDE 657 NITROSYL CHLORIDE [2696-92-6] Formula: ClNO; MW 65.459 Structure: Cl—N=O. bent molecule‚ N—O bond distance 1.139Å and N—Cl bond distance 1.975Å Uses Nitrosyl chloride is an important component of aqua regia. It is an oxidizing agent in organic synthesis. It also is used as a catalyst. Physical Properties Yellow gas; heavier than air‚ density 2.3 (air=1); gas density 2.872 g/L; liquefies at –5.55°C; liquid density 1.273 g/mL; freezes at –59.4°C; critical temperature 167°C;
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Experiment IV Solubility of Dissolved Oxygen Purpose To demonstrate the effect of partial pressure‚ temperature and salinity on the solubility of dissolved oxygen and to demonstrate the interference of nitrite in dissolved oxygen analysis by the Winkler Method. To demonstrate the use of the oxygen electrode and the difference between activity and concentration. References 1. Mancy‚ K. H.‚ Jaffe‚ T.‚ "Analysis of Dissolved Oxygen in Natural and Waste Water‚" USDHEW Public Health Service
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People believe that trouble is far away but it is here to stay and cannot be redirected any way that you may wish Net ionic equations are equations that show only the soluble‚ strong electrolytes reacting (these are represented as ions) and omit the spectator ions‚ which go through the reaction unchanged. When you encounter net ionic equations on the SAT II Chemistry test‚ you’ll need to remember the following solubility rules‚ so memorize them! Also keep in mind that net ionic equations‚ which
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