RECRYSTALLIZATION OF ACETANILIDE ABSTRACT Recrystallization is the primary method for purifying solid organic compounds through the differences in solubility at different temperatures. In this experiment‚ a suitable solvent was first determined. Acetanilide was produced by acetylation of aniline with acetic anhydride. The crude acetanilide was dissolved in a solvent in a heating water bath. The hot solution was filtered and the filtrate‚ cooled slowly in an ice bath as crystals started forming
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Writing Practical Reports Aim: To observe what happens during and after a chemical reaction. Equipment: Concentrated nitric acid in a glass dropping bottle Small pieces of Copper 250ml Beaker 2 M Lead nitrate in a dropping bottle 2 M Potassium iodide in a dropping bottle 2 M Copper sulfate in a dropping bottle 2 M Sodium hydroxide in a dropping bottle 2 M Hydrochloric acid in a dropping bottle 4 Pyrex test tubes Test tube rack Spatula Bunsen burner‚ gauze
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of the reaction: The effect of the temperature of the reaction on the activity of the purified enzyme was carried out by make the enzymatic reaction for 10 minutes at different temperature 25‚30‚35‚40‚45‚50‚60 and 70°C using an enzyme protein 0.1mg/reaction mixture and substrate concentration of 15 mg/reaction mixture‚ using a control of previously heated enzyme solution in the reaction. The data recorded in (table 27) and (figure 29) illustrate the effect of temperature of the reaction on the pectinase
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even something inanimate like sound could affect so much of biological processes. The movement of energy through matter produces sound. Sound is a mechanical wave that travels in waves and has the ability to move particles. Noise pollution is the result of the rapid and loud buzzing of a city‚ factory‚ piece of machinery‚ etc. The vibrations caused by energy vibrate the air particles around it and produce sound waves. These
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In this laboratory voltmeters where utilized to take reading of three different electrochemical reactions: Pb/Zn‚ Pb/Cu‚ and Zn/Cu. A salt bridge was placed between two reactions containing metal strips in separate aq solutions. The salt bridge was placed in order to balance the reaction. The voltage measurements for Pb/Zn‚ Pb/Cu‚ and Zn/Cu where .595 V‚ .479 V‚ and 1.072 V accordingly. The values obtained where then used to determine the voltage value for the reduction half. The resulting cell potential
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Measuring Human Reaction Time Name: Prerna Mohan Date: November 3‚ 2017 Team members: Allison Fitzgerald‚ Isabella Federico 1. Objectives The objective of this lab is to measure each individual’s reaction time using a ruler. 2. Method and Equation: We will apply free fall kinematics to find our own reaction time. An object in free fall is an object in motion where gravity is the sole force acting upon it. If we drop an object from a certain distance‚ the object will experience constant
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Carrington Lucas Spring 2013 Essay 1 Found Object Essay As I stumble my way through life‚ I found the one thing that the thing that is very important to me my family. Nothing compares how greatly family impacts people. I can’t imagine myself having a career that doesn’t involve helping my family or others’. I want family to be a part of my life‚ regardless if I am being an orthodontist for children or working in finance making sure that families are financially stable. There are many reasons
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The environmental factors that effected the rate of enzyme reactions were the enzyme concentration‚ pH‚ and temperature. These environmental factors help enzymes break down the poisonous chemicals into harmless substance. When we tested the liver with 2ml of hydrogen peroxide for a normal reaction it showed that it was exothermic. We added more hydrogen peroxide and the reaction rate of the liver was 3. We learned that the catalase is reusable because the liver reacted both times when we put in
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the value of the sum for Reaction 1 and Reaction 2’s change in temperature‚ compared to Reaction 3’s change in temperature. Reaction 1 was the dissolution of solid sodium hydroxide in water with a ΔH°rxn of -47047 J/mol‚ Reaction 2 was the neutralization of liquid sodium hydroxide with HCl with a ΔH°rxn of -31289 J/mol and Reaction 3 was the dissolution and neutralization of solid NaOH with HCl with a ΔH°rxn of -91000 J/mol. Consequently‚ the sum of Reaction 1 and Reaction 2 was -78336 J/mol‚ similar
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Grignard Reaction: Synthesis of Triphenylmethanol Hai Liu TA: Ara Austin Mondays: 11:30-2:20 Abstract: In this experiment‚ phenylmagnesium bromide‚ a Grignard reagent was synthesized from bromobenzene and magnesium strips in a diethyl ether solvent. The Grignard reagent was then converted to triphenylmethanol‚ a tertiary alcohol with HCl. The reaction for phenylmagnesium bromide was: The reaction for Grignard to triphenylmethanol was: In the formation of the Grignard reagent
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